Process for production of heat sensitive dispersions or emulsions

• US 5,927,852 A
• Filed: 12/01/1997
• Issued: 07/27/1999
• Est. Priority Date: 12/01/1997
• Status: Expired due to Fees

• Current Assignee: 3M Company
• Original Assignee: 3M Company
• Inventors: Serafin, Mark
• Primary Examiner(s): SOOHOO, TONY GLEN
• Application Number:
  US08/980,526
• Time in Patent Office: 603 Days
• Field of Search: 366/144, 366/145, 366/162.4, 366/152.1, 366/182.2, 366/182.1, 366/173.2, 366/173.1, 137/14, 137/334, 137/3, 137/4
• US Class Current: 366/144
• CPC Class Codes: B01F 23/41 Emulsifying
• CPC Class Codes: B01F 23/56 by introducing solids in liquids, e.g. dispersing or dissolving
• CPC Class Codes: B01F 25/23 Mixing by intersecting jets
• CPC Class Codes: B01F 25/4323 using elements provided with a plurality of channels or using a plurality of tubes which can either be placed between common spaces or collectors

Abstract

The invention is an apparatus and process for making multi-phase mixtures. The apparatus includes a high pressure pump, at least two high pressure mixing zones in series, and a high pressure heat exchanger located before the last high pressure mixing zone.

Claims

1. A process of making multi-phase mixtures comprising the steps of:

a) pressurizing components of the mixture

b) passing the components through a first high pressure mixing zone,

c) after passing the components through the first mixing zone, passing the pressurized components through a heat exchanger to cool the components, and

d) after passing the pressurized components through the heat exchanger, forcing the pressurized mixture through a last high pressure mixing zone, wherein the process is characterized in that no repressurization step occurs between steps b) and d).

2. The process of claim 1 wherein the high pressure mixing zones comprise impinging two or more streams of the components upon each other.

3. The process of claim 2 wherein each of the impinging streams pass through a nozzle and the nozzles of the last high pressure mixing zone are smaller than the nozzles of the first high pressure mixing zone.

4. The process of claim 2 wherein each of the impinging streams pass through a nozzle and the distance from the exit of the nozzle to the point of impingement is less than two times the diameter of the nozzle.

5. The process of claim 4 wherein the distance from the exit of the nozzle to the point of impingement is less than the diameter of the nozzle.

6. The process of claim 1 wherein the components are recycled through the process by introducing the mixture exiting the last high pressure mixing zone into the first high pressure mixing zone under pressure.

7. The process of claim 1 wherein the components are cooled before the pressurizing step (a).

8. The process of claim 1 wherein the components are further cooled after passing through the last high pressure mixing zone.

9. The process of claim 1 wherein the components comprise a polymeric binder, a pigment and a carrier liquid.

10. The process of claim 9 wherein the pigment is a magnetic pigment.

11. An apparatus for preparing mixtures comprising

a high pressure pump which pressurizes components of the mixture,

a first high pressure mixing zone in which the components are mixed by flowing through the first zone,

a high pressure heat exchanger in which the components are cooled after passing through the first high pressure mixing zone, and

a last high pressure mixing zone in which the components are mixed by flowing through the second zone.

12. The apparatus of claim 11 in which the high pressure mixing zones comprise at least two nozzles and a region where the components passing through the nozzles can impinge upon each other.

13. The apparatus of claim 12 in which the nozzles in the last high pressure mixing zone are smaller than the nozzles in the first high pressure mixing zone.

14. The apparatus of claim 12 in which the distance from the exit of the nozzle to the point of impingement is less than two times the diameter of the nozzle.

15. The apparatus of claim 12 in which the distance from the exit of the nozzle to the point of impingement is less than the diameter of the nozzle.

16. The apparatus of claim 11 further comprising a low pressure heat exchanger after the last high pressure mixing zone.

17. The apparatus of claim 11 further comprising a heat exchanger before the high pressure pump.