Process for the final evaporation of black liquor

• US 5,944,950 A
• Filed: 06/27/1997
• Issued: 08/31/1999
• Est. Priority Date: 10/20/1994
• Status: Expired due to Term

• Current Assignee: Metso Fiber Karlstad AB (Neles Oyj)
• Original Assignee: Kvaerner Pulping AB (Akastor ASA)
• Inventors: Wennberg, Olle, Olausson, Lars
• Primary Examiner(s): Manoharan, Virginia
• Application Number:
  US08/817,586
• Time in Patent Office: 795 Days
• Field of Search: 159/47.3, 159/49.21, 159/27.4, 159/17.1, 159/172, 159/DIG. 8, 159/24.1, 159/24.3, 159/20.1, 159/13.2, 162/30.11, 162/47, 202/173, 202/174
• US Class Current: 159/47.3
• CPC Class Codes: B01D 1/26 Multiple-effect evaporating
• CPC Class Codes: D21C 11/10 Concentrating spent liquor by evaporation evaporators B01D
• CPC Class Codes: Y10S 159/08 Multieffect or multistage
• CPC Class Codes: Y10S 203/16 Combination

Abstract

The process for the final evaporation has at least two evaporation appliances. These appliances are coupled in series with respect to the black liquor and in parallel with the live steam (primary steam), which drives the evaporation, and with the secondary steam that is generated by the evaporation. The pressure of the primary steam that is supplied to the appliance(s) where the liquor concentration is at the highest concentration is greater than the pressure of the primary steam supplied to the other appliances where the liquor concentration is not so high.

Claims

1. A process for a final evaporation of black liquor, comprising the steps of:

supplying a black liquor to a first evaporation appliance to a second and a third evaporation appliance in series, the first evaporation appliance having a first concentration of solids and the second evaporation appliance having a second concentration of solids, the first concentration being greater than the second concentration;

connecting a primary steam carrying member of the second evaporation appliance to the third evaporation appliance in parallel;

connecting a secondary steam carrying member of the first evaporation appliance to the second evaporation appliance so that the first and second evaporation appliances are in open fluid communication;

supplying a first primary steam to the first evaporation appliance at a first maximum pressure and a first temperature;

supplying a second primary steam to the second evaporation appliance at a second maximum pressure and a second temperature, the first maximum pressure being greater than the second maximum pressure and the first temperature being greater than the second temperature;

driving an evaporation process with the first and second primary steam; and

generating a first secondary steam by the evaporation process in the first evaporation appliance and generating a second secondary steam by the evaporation process in the second evaporation appliance, the first secondary steam having a first secondary steam pressure and the second secondary steam having a second secondary steam pressure, the first secondary steam pressure being identical to the second secondary steam pressure so that a resulting difference in temperature between a steam side and a liquor side of the first evaporation appliance is equal to or greater than a temperature difference between a steam side and a liquor side of the second evaporation appliance.

2. The process according to claim 1 wherein the process comprises passing black liquor through the second evaporation appliance and then passing the black liquor through the first evaporation appliance and feeding the first primary steam to the first evaporation appliance and feeding the second primary steam to the second evaporation appliance.

3. The process according to claim 2 wherein the process further comprises the steps of providing a pulp mill containing a low pressure steam having a pressure, the first maximum pressure of the first primary steam being greater than the pressure of the low pressure steam.

4. The process according to claim 1 wherein the process further comprises the step of concentrating the black liquor supplied to the first evaporation appliance so that a dry substance content of the black liquor exceeds 70% when the black liquor leaves the first evaporation appliance.

5. The process according to claim 1 wherein the process further comprises the step of evaporating the black liquor according to a falling film technique by permitting the black liquor to fall downwardly through the first and second evaporation appliances.

6. The process according to claim 5 wherein the process further comprises the steps of providing a heat exchanger having tubes disposed therein for shearing the falling film disposed on an inside of the tubes.

7. The process according to claim 1 wherein the process further comprises the step of increasing the steam pressure of the first and second primary steam by providing a steam ejector containing a driving steam having a pressure that is greater than the pressures of the first and second primary steam.

8. The process according to claim 1 wherein the method further comprises increasing the pressure of the first and second primary steam with a mechanical compressor.

9. A process for a final evaporation of black liquor, comprising the steps of:

coupling a black liquor carrying member of a first evaporation appliance to a second and a third evaporation appliance in series;

connecting a primary steam carrying member of the second evaporation appliance to the third evaporation appliance in parallel;

connecting a secondary steam carrying member of the first evaporation appliance to the second evaporation appliance so that the first and second evaporation appliances are in open fluid communication;

supplying a first primary steam to the first evaporation appliance at a first maximum pressure and a first temperature;

supplying a second primary steam to the second evaporation appliance at a second maximum pressure and a second temperature, the first maximum pressure being greater than the second maximum pressure and the first temperature being greater than the second temperature;

supplying a pulp mill in operative engagement with the second evaporation appliance, the pulp mill containing a low pressure steam having a pressure, the first maximum pressure of the first primary steam being greater than the pressure of the low pressure steam;

driving an evaporation process with the first and second primary steam;

generating a first secondary steam by the evaporation process in the first evaporation appliance and generating a second secondary steam by the evaporation process in the second evaporation appliance, the first secondary steam having a first secondary steam pressure and the second secondary steam having a second secondary steam pressure, the first secondary steam pressure being identical to the second secondary steam pressure;

passing black liquor through the second evaporation appliance and then passing the black liquor through the first evaporation appliance and feeding the first primary steam to the first evaporation appliance and feeding the second primary steam to the second evaporation appliance; and

setting the low pressure steam to about four bar.

10. The process according to claim 9 wherein the method further comprises setting the pressure of the secondary steam to a value that is greater than 0.7 bar and setting a condensation temperature of the secondary steam that is greater than 115 Celsius.