Ultrasonic sensors for on-line monitoring of castings and molding processes at elevated temperatures

• US 5,951,163 A
• Filed: 10/16/1996
• Issued: 09/14/1999
• Est. Priority Date: 10/16/1996
• Status: Expired due to Term

• Current Assignee: National Research Council Canada
• Original Assignee: National Research Council Canada
• Inventors: Wang, Hao, Cao, Bin, Loong, Chee Ang, Nguyen, Ky Thanh, Jen, Cheng-Kuei
• Primary Examiner(s): Williams, Hezron
• Assistant Examiner(s): MILLER, ROSE MARY
• Application Number:
  US08/733,113
• Time in Patent Office: 1,063 Days
• Field of Search: 73/597, 73/598, 73/599, 73/600, 73/644, 73/628, 73/632, 374/117, 374/118, 374/119, 374/139
• US Class Current: 374/119
• CPC Class Codes: B22D 17/32 Controlling equipment
• CPC Class Codes: B22D 2/006 for the temperature of the molten metal measuring temperature in general G01K
• CPC Class Codes: B29C 2945/7604 Temperature
• CPC Class Codes: B29C 2945/7605 Viscosity
• CPC Class Codes: B29C 2945/76083 Position
• CPC Class Codes: B29C 2945/76103 shrinkage, dilation, dimensional change, warpage
• CPC Class Codes: B29C 2945/76287 Moulding material
• CPC Class Codes: B29C 2945/76301 auxiliary fluids introduced into the cavity
• CPC Class Codes: B29C 2945/76381 Injection
• CPC Class Codes: B29C 2945/76474 Ultrasonic
• CPC Class Codes: B29C 2948/92085 Velocity
• CPC Class Codes: B29C 2948/92171 Distortion, shrinkage, dilatation, swell or warpage
• CPC Class Codes: B29C 2948/922 Viscosity; Melt flow index [MFI]; Molecular weight
• CPC Class Codes: B29C 2948/92209 Temperature
• CPC Class Codes: B29C 2948/92285 Surface properties
• CPC Class Codes: B29C 45/1642 having a "sandwich" structure B29C45/1603 takes precedence
• CPC Class Codes: B29C 45/1704 the fluid being introduced into the interior of the injected material which is still in a molten state, e.g. for producing hollow articles B29C45/1732 and B29C45/1734 take precedence; injection blow-moulding B29C49/06
• CPC Class Codes: B29C 45/76 Measuring, controlling or regulating measuring in general G01; controlling or regulating in general G05
• CPC Class Codes: B29C 45/78 of temperature
• CPC Class Codes: B29C 48/0011 combined with compression moulding
• CPC Class Codes: B29C 48/06 : Rod-shaped
• CPC Class Codes: B29C 48/92 : Measuring, controlling or regulating
• CPC Class Codes: G01K 11/24 : of the velocity of propagation of sound
• CPC Class Codes: G01N 2291/011 : Velocity or travel time
• CPC Class Codes: G01N 2291/015 : Attenuation, scattering
• CPC Class Codes: G01N 2291/0252 : Melting, molten solids
• CPC Class Codes: G01N 2291/02836 : Flow rate, liquid level
• CPC Class Codes: G01N 2291/02854 : Length, thickness
• CPC Class Codes: G01N 2291/02881 : Temperature
• CPC Class Codes: G01N 2291/0422 : Shear waves, transverse waves, horizontally polarised waves
• CPC Class Codes: G01N 29/07 : by measuring propagation velocity or propagation time of acoustic waves
• CPC Class Codes: G01N 29/228 : related to high temperature conditions
• CPC Class Codes: G01N 29/2462 : Probes with waveguides, e.g. SAW devices

Abstract

Ultrasonic sensors and associated methods for on-line monitoring of material properties for die casting, molding and extrusion processes at elevated temperatures are disclosed. The sensors include the use of ultrasonic waveguides embedded in the processing machines and piezoelectric ultrasonic transducers. The sensors are operated in the reflection geometry in which one side access of the processing machines is required. The monitoring parameters are the flow front, gap development and temperature of the materials being processed and filled in the cavities of the die in casting processes and the mold in injection molding, and the temperature and viscosity of the molten polymers in the polymer extrusion machines. Piezoelectric ultrasonic transducers made of high Curie temperature materials, fabricated by sol-gel techniques and directly deposited on top of the ultrasonic waveguides or the external walls of the shot sleeve of the die caster, die of the die caster, mold of the injection molding machine or barrel of the extruder are also used.

Claims

1. An apparatus for monitoring a mass of molten material in a cavity, comprising:

an array of buffer rods, each buffer rod having a proximal end extending into said cavity and a distal end extending outside said cavity;

an ultrasonic transducer operable in the reflection mode mounted on the distal end of each said buffer rod;

means for energizing said transducers so that they emit pulses of ultrasonic energy into the molten material through said buffer rods;

receiving means for receiving return pulses from said transducers;

axially spaced reflection means in said buffer rods at the proximal end thereof for reflecting pulses emitted by said transducers; and

a computer for analyzing said return pulses to derive data therefrom pertaining the state of the molten material, said computer being programmed to calculate the velocity of said return pulses reflected from said axially spaced means and derive therefrom the temperature of said buffer rods between said axially spaced means.

2. An apparatus as claimed in claim 1, further comprising a multiplexer for sequentially connecting said respective transducers to said energizing means and said receiving means.

3. An apparatus as claimed in claim 1, wherein each said buffer rod comprises a central axial core surrounded by a cladding sleeve.

4. An apparatus as claimed in claim 1, further comprising a cooling jacket surrounding each said transducer at the distal end of said buffer rods.

5. An apparatus as claimed in claim 1, wherein an ultrasonic coupling material is located between each said transducer and the distal end of each buffer rod.

6. An apparatus as claimed in claim 1, wherein said ultrasonic transducers are operable in the longitudinal wave mode.

7. An apparatus as claimed in claim 1, wherein said ultrasonic transducers are operable in the shear wave mode.

8. An apparatus as claimed in claim 1, wherein said computer is programmed to derive from said travel time of said return pulses additional information pertaining to surface disturbance arid solidification of the molten material.

9. An apparatus as claimed in claim 1, wherein said computer is programmed to additionally derive the viscosity of the molten material from said travel time of said return pulses and the degree of their attenuation.

10. An apparatus as claimed in claim 1, wherein said computer is programmed to additionally derive from the amplitude variation of the return pulses, information pertaining to the flow and gap development of the molten material.

11. An apparatus as claimed in claim 1, wherein said axially spaced means are transverse slots.

12. An apparatus as claimed in claim 1, wherein said respective ultrasonic transducers are directly fabricated onto the distal ends of the buffer rods.

13. An apparatus as claimed in claim 12, wherein said ultrasonic transducers are sol-gel fabricated thick film piezo-electric transducers.

14. An apparatus for measuring the temperature of a mass of molten material in a cavity, comprising:

at least one buffer rod, the or each buffer rod having a proximal end for extending into the cavity and a distal end for extending outside the cavity;

an ultrasonic transducer operable in the reflection mode mounted on the distal end of the or each said buffer rod;

means for energizing the or each said transducer to emit pulses of ultrasonic energy into die molten material through the or each said buffer rod;

receiving means for receiving return pulses from the or each said transducer; and

axially spaced reflection means in the or each said buffer rod at the proximal end thereof for reflecting pulses emitted by the or each said transducer to permit the temperature of the or each said buffer rod between said axially spaced means to be derived from the travel times of the return pulses reflected from said axially spaced means.

15. An apparatus as claimed in claim 14, wherein said axially spaced means are transverse slits.

16. An apparatus as claimed in claim 15, comprising at least three axially spaced said transverse slits.

17. An apparatus as claimed in claim 16, wherein said buffer rods comprise a central axial core surrounded by a cladding sleeve.

18. An apparatus as claimed in claim 17, wherein said transducers are directly fabricated onto the distal end of said respective buffer rods.

19. An apparatus as claimed in claim 18 wherein said transducers comprise piezo-electric particles dispersed in a sol-gel solution coated onto the distal ends of said buffer rods.

20. An apparatus as claimed in claim 19, wherein said piezo-electric particles are selected from the group consisting of lithium tantalate and niobium tantalate.

21. An apparatus as claimed in claim 14, comprising an array of said buffer rods.