Miniaturized ion mobility spectrometer sensor cell

• US 5,965,882 A
• Filed: 10/07/1997
• Issued: 10/12/1999
• Est. Priority Date: 10/07/1997
• Status: Expired due to Term

• Current Assignee: Hanger Solutions, LLC (IP Investments Group LLC)
• Original Assignee: Raytheon Company (Rtx Corporation)
• Inventors: Megerle, Clifford A., Townsend, Carl W., Linder, Jacques F.
• Primary Examiner(s): Berman, Jack I.
• Application Number:
  US08/946,115
• Time in Patent Office: 735 Days
• Field of Search: 250/287
• US Class Current: 250/287
• CPC Class Codes: G01N 27/622 Ion mobility spectrometry

Abstract

An improved ion mobility spectrometer for detecting chemical warfare agents and hazardous vapors. The ion mobility spectrometer has an improved sensor cell that includes a heated air flow assembly, an ionization assembly and a field electrode and detector assembly printed circuit assembly. The heated air flow assembly includes a cover with an air inlet, an ambient temperature sensor, a thin-film heater element, a heater frame, a heated air sensor, and a heater channel formed therein. The ionization assembly comprises a nuclear ionization source attached to a holder, a lid, and an ionization channel formed therein that is coupled to the heater channel. The field electrode and detector assembly printed circuit assembly comprises a field electrode printed circuit board, a detector electrode printed circuit board, and detector electronics. The field electrode printed circuit board has a plurality of field electrodes disposed on a bottom surface thereof. A gasket is disposed between the field electrode and detector electrode printed circuit boards. The detector electrode printed circuit board has a plurality of detector electrodes disposed on a top surface thereof. The detector electronics processes current outputs of the detector electrodes to generate a histogram of ion currents that identify mobilities of chemical species tested by the ion mobility spectrometer.

Claims

1. A sensor cell for use in an ion mobility spectrometer, said sensor cell comprising:

a heated air flow assembly comprising an ambient temperature sensor and a thin heater channel and having a thin-film heater element disposed on an interior surface of the channel;

an ionization assembly; and

a field electrode and detector assembly printed circuit assembly.

2. The sensor cell of claim 1 wherein the heated air flow assembly further comprises:

a cover having an air inlet;

a heater frame for holding the thin-film heater element;

a heated air sensor; and

a heater channel.

3. The sensor cell of claim 2 wherein the ionization assembly comprises:

a nuclear ionization source attached to a holder;

a lid separating the nuclear ionization source from the heated air flow assembly; and

an ionization channel coupled to the heater channel.

4. The sensor cell of claim 1 wherein the field electrode and detector assembly printed circuit assembly comprises:

a field electrode printed circuit board comprising a plurality of field electrodes;

a detector electrode printed circuit board comprising a plurality of detector electrodes disposed adjacent to and separated from the plurality of field electrodes;

a gasket disposed between the field electrode and detector electrode printed circuit boards; and

detector electronics coupled to the plurality of detector electrodes for processing current outputs thereof to generate a histogram of ion currents.

5. The sensor cell of claim 2 wherein the thin-film surface heater element comprises a tantalum heater element.

6. The sensor cell of claim 3 wherein the nuclear ionization source comprises Americium-241 foil.

7. The sensor cell of claim 3 wherein the gasket comprises a Teflon gasket.

8. The sensor cell of claim 2 wherein the temperature sensors comprise thermistors.

9. A sensor cell for use in an ion mobility spectrometer, said sensor cell comprising:

a cover having an air inlet therein;

an ambient temperature sensor attached to the cover;

a thin-film heater element attached to an interior surface of the cover;

a heater frame attached to the cover that forms a thin heater channel through the upper portion of the sensor cell;

a heated air sensor disposed in the heater channel downstream of the thin-film surface heater element;

a nuclear ionization source attached to a holder;

a lid attached to the holder that forms walls of the heater channel and an ionization channel;

a field electrode printed circuit board disposed adjacent to the holder having an opening therein that permits heated air to pass by the nuclear ionization source and has a plurality of field electrodes disposed on a bottom surface thereof;

a detector electrode printed circuit board having plurality of detector electrodes disposed on a top surface thereof, an air outlet formed therein, and detector electronics disposed thereon, that processes current outputs of the detector electrodes to generate a histogram of ion currents that identify mobilities of chemical species tested by the ion mobility spectrometer; and

a gasket disposed between the field electrode printed circuit board and the detector electrode printed circuit board that forms outer walls of the ionization channel.

10. The sensor cell of claim 9 wherein the thin-film surface heater element comprises a tantalum heater element.

11. The sensor cell of claim 9 wherein the nuclear ionization source comprises Americium-241 foil.

12. The sensor cell of claim 9 wherein the gasket comprises a Teflon gasket.

13. The sensor cell of claim 9 wherein the temperature sensors comprise thermistors.

14. An ion mobility spectrometer comprising:

a sensor cell comprising;

a cover having an air inlet therein;

an ambient temperature sensor attached to the cover;

a thin-film heater element attached to an interior surface of the cover;

a heater frame attached to the cover that forms a thin heater channel through the upper portion of the sensor cell;

a heated air sensor disposed in the heater channel downstream of the thin-film surface heater element;

a nuclear ionization source attached to a holder;

a lid attached to the holder that forms walls of the heater channel and an ionization channel;

a field electrode printed circuit board disposed adjacent to the holder having an opening therein that permits heated air to pass by the nuclear ionization source and has a plurality of field electrodes disposed on a bottom surface thereof;

a detector electrode printed circuit board having plurality of detector electrodes disposed on a top surface thereof, an air outlet formed therein, and detector electronics disposed thereon, that processes current outputs of the detector electrodes to generate histogram of ion currents that identify mobilities of chemical species tested by the ion mobility spectrometer; and

a gasket disposed between the field electrode printed circuit board and the detector electrode printed circuit board that forms outer walls of the ionization channel.

15. The spectrometer of claim 14 wherein the thin-film surface heater element comprises a tantalum heater element.

16. The spectrometer of claim 14 wherein the nuclear ionization source comprises Americium-241 foil.

17. The spectrometer of claim 14 wherein the gasket comprises a Teflon gasket.

18. The spectrometer of claim 14 wherein the temperature sensors comprise thermistors.