Acoustic method for determining the static gel strength of a cement slurry

• US 5,992,223 A
• Filed: 10/09/1997
• Issued: 11/30/1999
• Est. Priority Date: 07/14/1997
• Status: Expired due to Term

• Current Assignee: Chandler Instruments Co. LLC (Ametek Incorporated)
• Original Assignee: Chandler Engineering Company
• Inventors: Sabins, Fred L., Maki, Voldi
• Primary Examiner(s): BROCK, MICHAEL J
• Application Number:
  US08/947,691
• Time in Patent Office: 782 Days
• Field of Search: 73/54.03, 73/54.41, 73/61.49, 73/64.42, 73/64.53, 73/599, 73/597
• US Class Current: 73/64.42
• CPC Class Codes: G01N 2291/0251 Solidification, icing, curing composites, polymerisation
• CPC Class Codes: G01N 2291/02863 Electric or magnetic parameters
• CPC Class Codes: G01N 2291/02872 Pressure
• CPC Class Codes: G01N 2291/048 Transmission, i.e. analysed material between transmitter and receiver
• CPC Class Codes: G01N 2291/102 one emitter, one receiver
• CPC Class Codes: G01N 29/032 by measuring attenuation of acoustic waves

Abstract

An acoustic method and system for determining the static gel strength of one or more cement slurry samples at wellbore temperatures and pressures. The cement slurry sample to be tested is maintained in a static condition inside an acoustic pressure vessel at a controlled temperature and pressure. A first transducer generates an acoustic signal which is transmitted through the sample. A second transducer measures and records the amplitude of the acoustic signal after it transits the sample. This data is then processed and the static gel strength of the sample is determined according to a predetermined relationship relating signal amplitude to static gel strength.

Claims

1. An acoustic method for determining the static gel strength of a cement slurry sample, comprising the steps of:

(a) maintaining said sample in a static condition at a controlled temperature and pressure;

(b) transmitting an acoustic signal through said sample;

(c) measuring the amplitude of said acoustic signal as it transits said sample to obtain signal attenuation data;

(d) repeating steps (b) and (c) at a predetermined number of time points, thereby producing a predetermined number of amplitude measurements;

(e) calculating from said predetermined number of amplitude measurements at least one value representative of a derivative; and

,

(f) calculating a static gel strength of said sample by using at least one of said at least one values representative of a derivative.

2. The method according to claim 1 wherein said acoustic signal is an ultrasonic signal.

3. The method according to claim 2 wherein said ultrasonic signal is a high frequency signal in the range from about 100-600 kHz.

4. The method according to claim 1 further comprising pulsing said acoustic signal over time and repetitively performing steps (c) through (f) to obtain a time history of the static gel strength of said sample.

5. The method according to claim 1 further comprising comparing the static gel strength of said sample to an arbitrary value and determining the time when the static gel strength reaches said arbitrary value.

6. The method according to claim 5 wherein said arbitrary value represents the point at which signal amplitude begins to increase to indicate the onset of static gel strength development.

7. The method according to claim 5 wherein said arbitrary value represents the point at which signal amplitude reaches a maximum rate of increase to indicate a specific gel strength.

8. The method according to claim 1 wherein step (c) includes filtering said acoustic signal with a filter centered at 500 kHz to eliminate all frequencies outside a desired frequency range.

9. The method according to claim 1 further comprising simultaneously performing steps (a) through (c) upon multiple cement slurry samples and transmitting said signal attenuation data to a central processor which performs steps (d) through (f).

10. The method according to claim 1 further comprising simultaneously measuring the time required for said acoustic signal to transit said sample and determining the compressive strength of said sample using a predetermined relationship.

11. A system for determining the static gel strength of a cement slurry sample according to claim 1, comprising:

(a) an acoustic pressure vessel to maintain said sample in a static condition at a controlled temperature and pressure;

(b) a first transducer to transmit an acoustic signal through said sample;

(c) a second transducer to record the amplitude of said acoustic signal after it transits said sample to obtain signal attenuation data; and

(d) a data processor for determining the static gel strength of said sample according to the method of claim 1, wherein at least steps (e) and (f) of claim 1 are encoded as computer instructions with said data processor.

12. The system according to claim 11 wherein said first transducer is operable to transmit a high frequency ultrasonic acoustic signal in the range from about 100-600 kHz.

13. The system according to claim 11 further comprising a filter centered at 500 kHz to eliminate all frequencies outside a desired frequency range.

14. The system according to claim 11 further comprising a plurality of said acoustic pressure vessels and first and second transducers connected to said data processor to enable the simultaneous testing of multiple slurry samples.

15. A method for determining the static gel strength of a cement slurry sample, comprising the steps of:

(a) maintaining said sample in a static condition at a controlled temperature and pressure;

(b) transmitting an acoustic signal through said sample;

(c) measuring the amplitude of said acoustic signal as it transits said sample to obtain signal attenuation data;

(d) repeating steps (b) and (c) at a predetermined number of time points to obtain a predetermined number of amplitude measurements and a same predetermined number of corresponding time points, said amplitude measurements and time points together comprising an amplitude curve;

(e) identifying, from within said amplitude curve, a region containing a plurality of amplitude measurements, wherein said amplitude curve is at least approximately linear; and

,

(f) using at least two of said amplitude measurements within said approximately linear region to calculate an estimate of said static gel strength.

16. A method according to claim 15, wherein step (f) includes the steps of:

(f1) selecting a first amplitude measurement from said at least two amplitude measurement,

(f2) selecting a second amplitude measurement from said at least two amplitude measurements,

(f3) calibrating a linear equation to said amplitude curve by associating a first predetermined static gel strength value with said first selected amplitude measurement, and, associating a second predetermined static gel strength value with said second selected amplitude measurement, and,

(f4) estimating a static gel strength using said calibrated linear equation.

17. A method for determining the static gel strength of a cement slurry sample, comprising the steps of:

(a) maintaining said sample in a static condition at a controlled temperature and pressure;

(b) transmitting an acoustic signal through said sample;

(c) measuring an amplitude value of said acoustic signal as it transits said sample to obtain signal attenuation data;

(d) repeating steps (b) and (c) at a predetermined number of time points to obtain a predetermined number of amplitude values and a same predetermined number of corresponding time points, said amplitude values and time points together comprising an amplitude curve;

(e) identifying at least one amplitude value proximate to an inflection point of said amplitude curve;

(f) calculating a static gel strength of said sample by using at least one of said at least one amplitude values proximate to an inflection point.

18. A method according to claim 17, wherein step (f) includes the steps of:

(f1) selecting one of said at least one identified amplitude values,

(f2) identifying a time point associated with said selected amplitude value,

(f3) estimating a derivative of said amplitude curve for at least one time point different from said identified time point,

(f4) choosing from among said at least one derivatives a maximum derivative,

(f5) selecting a particular amplitude associated with said maximum derivative,

(f6) calibrating a linear equation to said amplitude curve by associating a first predetermined static gel strength value with said selected identified amplitude value, and, associating a second predetermined static gel strength value with said selected particular amplitude value, and,

(f7) estimating a static gel strength using said calibrated linear equation.

19. An acoustic method for determining the static gel strength of a cement slurry sample, comprising the steps of:

(a) maintaining said sample in a static condition at a controlled temperature and pressure;

(b) transmitting an acoustic signal through said sample;

(c) measuring the amplitude of said acoustic signal as it transits said sample to obtain signal attenuation data; and

(d) calculating, according to a predetermined relationship relating signal attenuation to static gel strength, the static gel strength of said sample.