Weathered reef-building coral material

• US 6,033,730 A
• Filed: 06/12/1998
• Issued: 03/07/2000
• Est. Priority Date: 10/15/1997
• Status: Expired due to Term

• Current Assignee: Coral Biotech KK
• Original Assignee: Coral Biotech KK
• Inventors: Oda, Toshiharu, Yoshizumi, Satoshi
• Primary Examiner(s): DUDASH, DIANA L
• Application Number:
  US09/077,890
• Time in Patent Office: 634 Days
• Field of Search: 427/4, 427/430.1, 427/443.1, 427/345, 427/350, 427/354, 427/308, 427/309, 427/377, 427/380, 427/383.3, 427/244, 427/352, 427/353, 427/215, 427/337, 427/369, 426/74, 424/439, 424/489, 424/520, 424/549, 210/500.1, 210/501, 210/506, 210/354, 210/355
• US Class Current: 427/244
• CPC Class Codes: A23L 33/16 Inorganic salts, minerals or trace elements
• CPC Class Codes: A23L 33/29 Mineral substances, e.g. mineral oils or clays
• CPC Class Codes: B01D 39/06 Inorganic material, e.g. asbestos fibres, glass beads or fibres
• CPC Class Codes: B01J 3/006 Processes utilising sub-atmospheric pressure; Apparatus therefor
• CPC Class Codes: C02F 1/286 using natural organic sorbents or derivatives thereof
• CPC Class Codes: C02F 1/50 by addition or application of a germicide or by oligodynamic treatment C02F1/4606, C02F1/467, C02F1/76 take precedence

Abstract

Weathered reef-building coral is immersed in an aqueous alkali solution under reduced pressure to carry out alkali washing to make the aqueous alkali solution penetrate into the weathered reef-building coral throughout its fine structure inside the porous tissue, which is subsequently washed with water until a washing from the inside of the porous tissue is neutralized.

As a result of this washing, various marine algae, various microorganisms including Vibrio bacteria inhabiting the ocean and other various organic substances held in the inner fine structure of weathered reef-building coral can be removed. Thus, a weathered reef-building coral material can be obtained whose safety has been ensured. This weathered reef-building coral material is suitable for food materials, filter mediums for water purifiers and so forth.

Claims

1. A process for manufacturing a weathered reef-building coral material, comprising the steps of;

immersing weathered reef-building coral in an aqueous 0.1N to 6N alkali solution under reduced pressure to carry out alkali washing to make the aqueous alkali solution penetrate into the weathered reef-building coral throughout its fine structure inside the porous tissue; and

washing it with water until a washing from the inside of the porous tissue is neutralized, wherein said alkali washing is carried out by forcibly passing the aqueous alkali solution through the weathered reef-building coral immersed in the aqueous alkali solution or is carried out by agitating the weathered reef-building coral in said aqueous alkali solution and wherein the aqueous alkali solution is heated.

2. The process for manufacturing a weathered reef-building coral material according to claim 1, wherein said aqueous alkali solution comprises an aqueous solution of NaOH, KOH, Na₂ CO₃ or K₂ CO₃.

3. The process for manufacturing a weathered reef-building coral material according to claim 1, wherein the water washing is carried out by immersing the weathered reef-building coral in water under reduced pressure and forcibly passing the water through the weathered reef-building coral.

4. The process for manufacturing a weathered reef-building coral material according to claim 1, wherein the water washing is carried out by immersing the weathered reef-building coral in water under reduced pressure and agitating the weathered reef-building coral in the water.

5. The process for manufacturing a weathered reef-building coral material according to claim 1, wherein, after the washing with water, the weathered reef-building coral is subjected to dry heat disinfection or dry sterilization, or roasting, and thereafter pulverized and sifted to make it into a powder having a particle diameter of 27.28 μ

m or smaller.

6. The process for manufacturing a weathered reef-building coral material according to claim 1, wherein, after the washing with water, the weathered reef-building coral is roasted at 100 to 750°

C.

7. A process for manufacturing a silver-added weathered reef-building coral material, comprising, after the washing with water in the process for manufacturing a weathered reef-building coral material according to claim 1;

subjecting the weathered reef-building coral to dry heat disinfection or dry sterilization, or roasting, followed by immersion in an aqueous silver solution under reduced pressure to make the aqueous silver solution penetrate into the weathered reef-building coral throughout its fine structure inside the porous tissue; and

reducing the silver with a reducing agent to coat the weathered reef-building coral with silver throughout its fine structure inside the porous tissue.

8. A weathered reef-building coral material obtained by the manufacturing process according to claim 1.

9. A food material comprising the weathered reef-building coral material obtained by the manufacturing process according to claim 5.

10. A filter medium comprising the weathered reef-building coral material obtained by the manufacturing process according to claim 6.

11. A silver-added material comprising the weathered reef-building coral material obtained by the manufacturing process according to claim 7.

12. The method according to claim 1, wherein the alkali washing and water washing is conducted for a period of 30 to 60 minutes.

13. A process according to claim 1, wherein the reduced pressure is 70 mmHg or less.