Method for chromium plating titanium alloy

• US 6,039,860 A
• Filed: 11/09/1998
• Issued: 03/21/2000
• Est. Priority Date: 11/09/1998
• Status: Expired due to Term

• Current Assignee: Mcdonnell Douglas Corporation (The Boeing Co.)
• Original Assignee: Mcdonnell Douglas Corporation (The Boeing Co.)
• Inventors: Hazencomb, Robert M., Cooper, Austin M., Wright, Robert William, Silva, Albert W.
• Primary Examiner(s): Wong, Edna
• Application Number:
  US09/188,731
• Time in Patent Office: 498 Days
• Field of Search: 205/206, 205/208, 205/222, 148/264
• US Class Current: 205/208
• CPC Class Codes: C25D 5/38 of refractory metals or nickel
• CPC Class Codes: C25D 5/48 After-treatment of electroplated surfaces

Abstract

A method for chromium plating a part made of titanium or titanium alloy eliminates the conventional chemical cleaning of the part prior to electroplating, and instead employs a mechanical cleaning of the part including degreasing the part and then grit-blasting the part with aluminum oxide particles. Immediately following the grit-blasting step, for example within one minute of its completion, the part is connected to the negative terminal of a DC power supply and is then immersed into a bath of chromium plating solution which contains an anode element connected to the positive terminal of the power supply. The part is left in the bath for a period of time so as to deposit a plating of chromium on the surface of the part. For final finishing of the part, a post-plating grinding operation is performed in which the surface speed of the grinding wheel is not greater than about 6500 surface feet per minute and the in-feed rate is less than about 0.00015 inch per pass of the grinding wheel, and preferably is about 0.0001 inch per pass.

Claims

1. A method for chromium plating a surface of a part made of titanium or an alloy thereof, comprising:

mechanically cleaning the surface of the part to remove impurities therefrom;

electrically connecting the part to a negative terminal of a direct current power supply; and

while the part is connected to the negative terminal of the power supply, immersing the part in a bath of a chromium plating solution which contains an anode element connected to a positive terminal of the direct current power supply, and maintaining the part immersed for a period of time such that a plating of chromium is deposited on the surface of the part.

2. The method of claim 1, wherein the cleaning step comprises grit blasting the surface of the part.

3. The method of claim 2, wherein the cleaning step further comprises the step of wiping the surface of the part with a degreasing agent prior to the grit blasting step.

4. The method of claim 2, further comprising the steps, performed after the chromium plating is deposited on the surface, of removing the part from the bath and grinding the chromium plating with a rotating grinding tool having a peripheral speed relative to the surface of the part which is less than about 6500 surface feet per minute.

5. The method of claim 4, wherein the grinding step comprises contacting the plating of chromium with the periphery of a rotating grinding wheel, and passing the grinding wheel over the surface so as to remove a predetermined thickness of chromium from the part.

6. The method of claim 5, wherein the grinding step comprises removing less than about 0.00015 inch of chromium per pass of the grinding wheel over the surface.

7. The method of claim 5, wherein the grinding step comprises removing less than about 0.0001 inch of chromium per pass.

8. The method of claim 1, wherein the step of immersing the part in the bath and maintaining the part in the bath comprises initially subjecting the part to a relatively higher current density beginning when the part is placed into the bath, and subjecting the part to a reduced current density after a predetermined period of time.

9. The method of claim 8, wherein the part is initially plated at a current density of about 2.5-5 amps per square inch of surface area of the part.

10. The method of claim 9, wherein the current density is reduced to about 1-2 amps per square inch of surface area after the predetermined period of time has elapsed.

11. The method of claim 1, wherein the step of immersing the part in the bath is performed within three minutes of completing the mechanical cleaning step.

12. The method of claim 1, wherein th e mechanical cleaning step comprises the steps of wiping the surface of the part with a solvent and then grit-blasting the surface.

13. A method for chromium plating a surface of a part made predominantly of titanium, comprising the steps of:

degreasing the surface of the part;

after the degreasing step, grit-blasting the surface of the part;

within three minutes of completion of the grit-blasting step, electrically connecting the part to a negative terminal of a direct current power supply and thereafter immersing the part in a bath of chromic acid solution which contains an anode element connected to a positive terminal of the direct current power supply; and

maintaining the part immersed for a period of time such that a plating of chromium is deposited on the surface of the part.

14. The method of claim 13, wherein the degreasing step includes a step of wiping the surface of the part with a solvent so as to develop a water break-free condition on the surface.

15. The method of claim 13, wherein the step of electrically connecting the part to the negative terminal of the power supply comprises applying an electrical potential of about 7 volts between the part and the positive terminal of the power supply.

16. The method of claim 13, further comprising the steps of removing the part from the bath after the plating has been deposited on the surface and grinding the chromium plating with a grinding wheel operating at a peripheral speed relative to the part of less than about 6500 surface feet per minute.