Calibration standard for infrared absorption gauge

• US 6,078,042 A
• Filed: 03/04/1998
• Issued: 06/20/2000
• Est. Priority Date: 09/05/1995
• Status: Expired due to Term

• Current Assignee: Infra-Red Engineering Limited
• Original Assignee: Infra-Red Engineering Limited
• Inventors: Fellows, Timothy Gordon
• Primary Examiner(s): Hannaher, Constantine
• Application Number:
  US09/029,242
• Time in Patent Office: 839 Days
• Field of Search: 250/252.1, 359/350, 359/359, 252/587, 73/1.01 T
• US Class Current: 250/252.1
• CPC Class Codes: G01N 21/278 Constitution of standards
• CPC Class Codes: G01N 21/3554 for determining moisture content
• CPC Class Codes: G01N 21/3559 in sheets, e.g. in paper

Abstract

A calibration standard for use with an infrared optical absorption measurement gauge having an assembly with an optical interference filter (22) and one or more optical elements. The interference filter has spectrally selective properties so that all but a selected spectral band is reflected by the filter towards the detectors of the gauge. The transmitted band is selectively absorbed by the optical element(s) which are spectrally unselective and also directed towards the detectors of the gauge. The position and strength of the selected band can thereby be adjusted to simulate an absorption spectrum, i.e., a corresponding spectral band which is characteristic of the absorption spectrum of a material under measurement. The standard is used to calibrate the absorption measurement gauge.

Claims

1. A calibration standard including an assembly comprising:

(i) an optical interference filter having spectrally selective infrared transmission and reflection characteristics, and

(ii) one or more optical elements, which respectively reflect, transmit, or absorb infrared radiation transmitted by the optical interference filter in a spectrally unselective manner;

the optical interference filter and the optical element or elements being selected so as to provide, in the assembly, an infrared reflection spectrum having at least one prominent predetermined wavelength absorption band with a predetermined strength.

2. A standard according to claim 1 in which at least one of the optical elements is a neutral density filter having a predetermined reflection and/or transmission characteristic.

3. A standard according to claim 1 including either a light absorbing, or light reflecting element for absorbing, or reflecting respectively light transmitted by said optical element or elements.

4. A standard according to claim 1 in which said optical element or elements is partly reflecting and partly absorbing.

5. A standard according to claim 4 in which said optical element comprises a substrate containing at least one reflective area and at least one radiation absorbing area.

6. A calibration standard for calibrating an infrared absorption gauge that includes a source of infrared electromagnetic radiation and a detector for detecting the intensity of infrared radiation incident upon it, the standard comprising:

means for locating the standard relative to an infrared gauge so that it can receive infrared radiation from the radiation source of the gauge and direct infrared radiation towards the detector of the gauge,

an optical interference filter being locatable to receive infrared radiation from the said radiation source of the gauge, said filter being such that it transmits radiation in at least one infrared wavelength band and reflects radiation having other wavelengths along an optical path on which the gauge detector can be located, and

optical element means for attenuating the intensity of radiation in at least one wavelength band transmitted by the interference filter and directing the attenuated radiation (if any) along an optical path on which the gauge detector can be located, wherein the interference filter and the optical element means are such that the said radiation directed along said optical path or paths on which the gauge detector can be located has a spectrum made up of said radiation reflected from the filter and said attenuated radiation and so includes at least one prominent predetermined absorption band with a predetermined strength having a wavelength band corresponding to the wavelength band transmitted by the said filter.

7. A standard as claimed in claim 6, wherein the optical element means comprises a neutral density filter having a predetermined reflection and transmission characteristic.

8. A standard as claimed in claim 6, wherein the optical element means comprises at least one optical element that transmits light incident upon it and further includes either a light absorbing, or a light reflecting, element for absorbing or reflecting (respectively) light transmitted by said at least one optical element.

9. A standard as claimed in claim 6, wherein the optical element means comprises at least one element that partly reflect incident radiation.

10. A standard as claimed in claim 9, wherein the said at least one element comprises a substrate containing at least one radiation reflective area and at least one radiation absorbing area.

11. A method of calibrating, or checking the calibration of, an infrared absorption gauge, which gauge is arranged to measure a given quantity or parameter of a sample having a characteristic infrared absorption spectrum, the method comprising the steps of:

providing a calibration standard or standards comprising (i) an optical interference filter having spectrally selective infrared transmission and reflection characteristics, and (ii) one or more optical elements which respectively reflect, transmit or absorb infrared radiation transmitted by the optical interference filter in a spectrally unselective manner,

selecting the interference filter and said optical elements so that the infrared reflection spectrum of the assembly corresponds substantially to the infrared absorption spectrum of the sample or samples under measurement; and

calibrating the absorption gauge with one or more of the said calibration standards.