Method and apparatus for recirculating a heavier solution from the separation part of two separable solutions into a mixing unit

• US 6,083,400 A
• Filed: 03/16/1999
• Issued: 07/04/2000
• Est. Priority Date: 04/30/1996
• Status: Expired due to Term

• Current Assignee: Outotec Oyj (Metso Outotec Oyj)
• Original Assignee: Outokumpu Technology OYJ (Metso Outotec Oyj)
• Inventors: Saarenpaa, Timo, Hultholm, Stig-Erik, Lilja, Launo, Nyman, Bror, Lyyra, Juhani, Kuusisto, Raimo, Taipale, Petri
• Primary Examiner(s): Popovics, Robert J.
• Application Number:
  US09/171,597
• Time in Patent Office: 476 Days
• Field of Search: 210/634, 210/511
• US Class Current: 210/634
• CPC Class Codes: B01D 11/0457 comprising rotating mechanisms, e.g. mixers, mixing pumps
• CPC Class Codes: B01D 17/0208 by sedimentation
• CPC Class Codes: B01D 17/0211 with baffles
• CPC Class Codes: B01D 17/0214 with removal of one of the phases
• CPC Class Codes: B01D 17/045 with coalescers
• CPC Class Codes: C22B 3/02 Apparatus therefor
• CPC Class Codes: C22B 3/26 by liquid-liquid extraction using organic compounds
• CPC Class Codes: Y02P 10/20 Recycling

Abstract

The invention relates to a method for recirculating the heavier solution from the separation part of liquid--liquid extraction to the mixing unit of the same extraction step, so that part of the recirculated solution is returned to the mixing unit from the overflow of the discharge end of the separation part. An essential feature of the invention is that the major part of the heavier solution recirculated into the mixing unit is obtained from the separation part proper, along the whole width thereof. The invention also relates to an apparatus based on said method, in which apparatus, in the bottom part of the settler (6) there is located a heavier solution collecting channel (13) extending over the whole width of the settler and being provided with suction pipes (15) which are oriented in an inclined fashion towards the solution to be collected from the channel.

Claims

1. A method of recirculating the heavier solution phase of two different solution phases, one being heavier and the other lighter, of a liquid--liquid extraction process from a separation zone of said extraction process to a mixing zone of said extraction process comprising:

(a) passing dispersed and settled solutions through at least one picket fence forming a restricted transversal surface in said separation zone;

(b) obtaining a part of said heavier solution phase for recirculation to the mixing zone from that portion of said separation zone between a last picket fence and a discharge point of said lighter solution phase and extending along an entire width of said separation zone; and

(c) returning from an upper discharge point of the separation zone a part of the lighter phase solution to the mixing zone.

2. A method according to claim 1, wherein the heavier solution is obtained from the bottom of the separation part.

3. A method according to claim 1, wherein the liquid--liquid extraction is copper extraction.

5. An apparatus according to claim 1, wherein the collecting channel is located in between the last picket fence of the settler and the overflow chute of the organic solution.

6. An apparatus according to claim 1, wherein the collecting channel is located in the settler, in the heavier solution layer underneath the organic solution layer, and that the suction pipes are directed downwards in an inclined fashion.

7. An apparatus according to claim 1, wherein the collecting channel is located in the bottom structure of the settler, so that the suction pipes are directed upwards in an inclined fashion.

8. An apparatus according to claim 1, wherein the transversal surface area of the collecting channel expands gradually in the flowing direction of the channel, according to the number of the suction pipes.

9. An apparatus according to claim 1, wherein the number of the suction pipes is 3-7.

10. An apparatus according to claim 1, wherein the suction pipes are attached in the collecting channel in the direction of the channel flow.

11. An apparatus according to claim 1, wherein the suction pipes enter the collecting channel for a length which is 0.1-0.4 times the channel height.

12. An apparatus according to claim 1, wherein the ends of the suction pipes are cut horizontally inside the collecting channel.

13. An apparatus according to claim 1, wherein the collecting channel is encased in a channel encasing.

14. An apparatus according to claim 13, wherein the sides of the channel casing that are parallel to the settler flow are designed to be curved.

4. An apparatus for effecting liquid--liquid extraction of two solution phases, one being heavier than the other, comprising a settler separator, a mixer, a pump unit, and recirculation system wherein said settler separator has:

(i) a picket fence at a front end of said settler;

(ii) a collecting channel at a bottom part of said settler and extending across said settler;

(iii) suction pipes inclined from said channel towards a liquid solution;

(iv) a discharge end having an overflow chute for said lighter solution phase;

(v) a discharge chute for said heavier solution phase; and

(vi) a circulation passage from said settler to said mixer.