Process and equipment for sanitizing and packaging food using ozone

• US 6,086,833 A
• Filed: 09/08/1997
• Issued: 07/11/2000
• Est. Priority Date: 09/08/1997
• Status: Expired due to Fees

• Current Assignee: American Air Liquide Incorporated (L'Air Liquide SA), L'Air Liquide Societe Anonyme Pour L'Etude et L'Exploitation Des Procedes Georges Claude (L'Air Liquide SA), Air Liquide America LP (Mitsubishi Chemical Group Corp.)
• Original Assignee: American Air Liquide Incorporated (L'Air Liquide SA), Air Liquide America LP (Mitsubishi Chemical Group Corp.)
• Inventors: Thaler, Michael, Schnepper, Carol A., Sauer, Richard, Boisrobert, Christine, Yuan, Tsz-Ching J., Bajcar, Miles, Hubert, John-Luc, Conners, Robert W.
• Primary Examiner(s): MCKANE, ELIZABETH L
• Application Number:
  US08/925,274
• Time in Patent Office: 1,037 Days
• Field of Search: 422/3, 422/32, 422/292, 426/320, 99/467, 99/468, 99/473, 99/478, 99/479, 99/534
• US Class Current: 422/292
• CPC Class Codes: A61L 2/202 Ozone

Abstract

Systems and processes are described for sanitizing a food product with ozone gas. The ozone gas is generated using a low pressure, low volume ozone gas generator and is delivered to a fluid injector. The fluid injector receives high pressure carrier fluid from a carrier fluid source and causes the ozone to be entrained in a stream of carrier fluid. The entrainment is created by passing the carrier fluid through a venturi diffuser inside the injector which creates a negative pressure in the sanitizing fluid line, thus drawing the sanitizing fluid into the carrier fluid and creating a highly homogenized fluid jet. The fluid jet is then injected into a container which contains a food product to be sanitized by the ozone. The container may also be provided with a mixing paddle to vigorously mix the food product while the ozone/carrier fluid jet is injected into the food product, which further ensures that the food product is contacted with sanitizing ozone gas. The container can be sealed to be pressurized by the ozone/carrier fluid jet by selective opening and closing of a vent. The ozone/carrier fluid jet may also be selectively humidified before injection into the container.

Claims

1. A device for mixing ozone with a carrier fluid for use in reducing the microbial content of food, comprising:

venturi nozzle including an outlet and two inlets;

a blender, said outlet of said venturi nozzle being connected to said blender; and

a source of liquid cryogenic carrier fluid and a source of ozone connected to the venturi nozzle via said inlets such that delivery of said liquid cryogenic carrier fluid to said venturi nozzle creates a vacuum which is sufficient to draw ozone at or near atmospheric pressure into said venturi nozzle.

2. The device according to claim 1, wherein the liquid cryogenic carrier fluid is selected from the group consisting of carbon dioxide, nitrogen, water, air, and mixtures thereof.

3. The device according to claim 1, wherein the liquid cryogenic carrier fluid is carbon dioxide.

4. A device for reducing the microbial content of a product comprising:

a container including an interior space for containing said product;

mixing means in said interior space, wherein when a product is contained in said interior space said mixing means is capable of mixing said product;

a first injector including a fluid lumen in fluid communication with said interior space, a first inlet for connection to a source of pressurized carrier fluid, and a second inlet;

means for generating a sanitizing gas at a first pressure in fluid communication with said second inlet;

wherein said injector is capable of delivering said sanitizing gas through said fluid lumen to said interior space when a source of pressurized carrier fluid is in fluid communication with said first inlet; and

whereby when a product is contained in said container, said injector is capable of delivering sanitizing gas to said interior space in an amount effective to sanitize said product;

a source of carrier fluid at a second pressure higher than said first pressure in fluid communication with said injector first inlet; and

wherein said high pressure carrier fluid is a liquid cryogenic fluid selected from the group consisting of CO₂, N₂, and mixtures thereof.

5. A device according to claim 4, wherein said injector is mounted exteriorly of said container.

6. A device according to claim 4, further comprising a second injector including a fluid lumen in fluid communication with said interior space.

7. A device according to claim 4, wherein said sanitizing gas is ozone gas.

8. A device according to claim 4, wherein said first pressure is within the range of about 100 kPa absolute to about 790 kPa absolute.

9. A device according to claim 4, wherein said generating means comprises a pressure regulator which regulates the pressure of the sanitizing gas in fluid communication with said second inlet, and a metering valve which meters the rate at which sanitizing gas can flow to said second inlet.

10. A device according to claim 4, further comprising a gas sampling line and a sanitizing gas analyzer, said gas sampling line in fluid communication between said interior space and said sanitizing gas analyzer, said sanitizing gas analyzer capable of analyzing the concentration of said sanitizing gas in a sample of gas from said interior space.

11. A device according to claim 10, further comprising a first valve for controlling the flow of sanitizing gas to said second inlet from said sanitizing gas generating means, said sanitizing gas analyzer generating a control signal which is a function of the concentration of ozone in said sample, said sanitizing gas analyzer in control signal communication with said first valve, said first valve controlling said flow of sanitizing gas in response to said control signal.

12. A device according to claim 11, wherein said control signal is an electronic control signal, and further comprising a current-to-pressure converter in control signal communication between said sanitizing gas analyzer and said first valve, said current-to-pressure converter converting said electronic control signal to a fluid pressure control signal.

13. A device according to claim 11, wherein said sanitizing gas analyzer is in direct control signal communication with said first valve.

14. A device according to claim 4, further comprising a diffuser in fluid communication with said injector which, when a fluid jet exits said injector, diffuses said fluid jet and lowers the force of said fluid jet on said product.

15. A device according to claim 14, further comprising a gas sampling line and a sanitizing gas analyzer, said gas sampling line in fluid communication between said injector fluid lumen and said sanitizing gas analyzer, said sanitizing gas analyzer capable of analyzing the amount of said sanitizing gas in a sample of gas from said injector fluid lumen.

16. A device according to claim 4, further comprising a sanitizing gas control valve for controlling the flow of sanitizing gas to said second inlet, a pressurized carrier fluid control valve for controlling the flow of pressurized carrier fluid to said first inlet, and a pressure switch in pressure sensing communication with said interior space, said pressure switch in control signal communication with said sanitizing gas control valve and said pressurized carrier fluid control valve to open and close said sanitizing gas control valve and said pressurized carrier fluid control valve, said pressure switch controlling both said sanitizing gas control valve and said pressurized carrier fluid control valve to close when said pressure switch senses a pressure in said interior space above a first threshold pressure level.

17. A device according to claim 16, said pressure switch further controlling both said sanitizing gas control valve and said pressurized carrier fluid control valve to open when said pressure switch senses a pressure in said interior space below a second threshold pressure level, said second threshold pressure level being less than said first threshold pressure level.

18. A device according to claim 4, further comprising a vent and a vent valve in fluid communication with said interior space, said vent valve operable to close off said vent to allow said first injector to pressurize said container.

19. A device according to claim 4, further comprising means for humidifying said sanitizing gas in fluid communication with said injector.

20. A device according to claim 19, wherein said means for humidifying comprises a third inlet in said first injector and a source of water vapor in fluid communication with said third inlet, said first injector capable of delivering said water vapor to said interior space.

21. A device according to claim 19, wherein said means for humidifying comprises a bubbler in fluid communication between said second inlet and said sanitizing gas generating means.