Chemical delivery systems and methods of delivery

• US 6,098,843 A
• Filed: 12/31/1998
• Issued: 08/08/2000
• Est. Priority Date: 12/31/1998
• Status: Expired due to Term

• Current Assignee: Air Liquide Electronics US LP (Air Liquide SA)
• Original Assignee: Silicon Valley Group, Inc. (ASML Holding NV), Semco LLC
• Inventors: Forshey, Randy, Soberanis, David
• Primary Examiner(s): Bomberg, Kenneth
• Application Number:
  US09/224,607
• Time in Patent Office: 586 Days
• Field of Search: 137/403, 137/408, 222/53, 222/56, 222/58
• US Class Current: 222/53
• CPC Class Codes: B67D 7/0238 utilising compressed air or other gas acting directly or indirectly on liquids in storage containers for dispensing beverages on draught B67D1/04
• CPC Class Codes: B67D 7/0272 specially adapted for transferring liquids of high purity
• CPC Class Codes: B67D 7/0283 specially adapted for transferring liquids of high purity
• CPC Class Codes: B67D 7/74 Devices for mixing two or more different liquids to be transferred coin-freed apparatus G07F13/06
• CPC Class Codes: C30B 25/14 Feed and outlet means for the gases; Modifying the flow of the reactive gases

Abstract

The present invention relates to chemical delivery systems and methods for delivery of liquid chemicals. In one embodiment, the present invention relates to systems having multi-reservoir load cell assemblies for delivering chemicals used in the semiconductor industry. In one embodiment, the present invention provides a multi-reservoir load cell assembly, including a controller, a buffer reservoir, a main reservoir, one or more load cells, coupled to the assembly and to the controller, operable to weigh the liquid in the reservoir(s), a plurality of supply lines, each supply line having a valve and connecting one of the supply containers to the main reservoir, and a gas and vacuum sources for withdrawing the liquid from the assembly when demanded by the controller and for refilling the assembly from the supply containers.

Claims

1. A liquid chemical delivery system for use with a plurality of supply containers, comprising:

a controller;

a multi-reservoir load cell assembly, including, a buffer reservoir with a chemical output, a main reservoir, a reservoir valve connecting the buffer reservoir to the main reservoir, and a load cell, coupled to the assembly and to the controller, operable to weigh the liquid in the reservoir assembly;

a plurality of supply lines, each having a valve coupled to the controller and to one of the supply containers to the main reservoir; and

means for withdrawing the liquid from the chemical output, opening and closing the reservoir valve, and refilling the main reservoir from the supply containers when demanded by the controller based on signals from the load cell.

2. The system of claim 1, wherein the means for withdrawing the liquid from the output and for refilling the main reservoir from the supply containers, includes a gas line connected to the main reservoir, a gas source connected to the gas line, a vacuum source, a vacuum line connecting the vacuum source to the gas line, a gas valve connecting the gas line, the gas source, and the vacuum source, wherein the controller opens the gas valve to permit gas to flow from the gas source to the main reservoir when liquid is withdrawn from the reservoir and to generate a vacuum in the main reservoir when the reservoir is refilled from the supply containers.

3. The system of claim 1, wherein the controller closes the buffer reservoir from the main reservoir when the reservoir is refilled and liquid is withdrawn such that the buffer reservoir undergoes no negative pressure from the vacuum in the main reservoir.

4. A chemical delivery system, comprising:

a multi-reservoir load cell assembly comprising a main reservoir capable of fluid communication with a buffer reservoir and a first load cell weighing the assembly and generating an output signal indicative of the weight; and

means, responsive to the output signal, for adjusting the pressure in the main reservoir and in the buffer reservoir, for calculating the amount of chemical in the assembly, and for controlling fluid communication between the main reservoir from the buffer reservoir.

5. The system of claim 4, wherein the first load cell generates an output signal proportional to the weight of the chemical in the main reservoir.

6. The system of claim 4, wherein the first load cell generates an output signal proportional to the weight of the chemical in the buffer reservoir.

7. The system of claim 4, 5, or 6, wherein the means responsive to the output signal includes means for refill of the assembly with the chemical when the weight of chemical drops to a predetermined amount by the following sequence:

a) isolating the main reservoir from the buffer reservoir,

b) reducing the gas pressure in the main reservoir to draw the chemical into the main reservoir until the chemical rises to a predetermined amount,

c) increasing the gas pressure in the main reservoir, and

d) opening communication between the main reservoir and the buffer reservoir to allow the chemical in the main reservoir to flow into the buffer reservoir.

8. The system of claim 5, further comprising a first supply container connected to the main reservoir, a second supply container connected to the main reservoir, a first valve associated with the first supply container, a second valve associated with a second supply container, and wherein the means responsive to the output signal monitors the first output signal and shuts and opens the first valve based on the value of the first output signal.

9. The system of claim 5, further comprising a first supply container connected by a first line to the main reservoir, a second supply container connected by a second line to the main reservoir, a first valve on the first line, a second valve on the second line, wherein the logic device monitors the first output signal and shuts and opens the first valve based on the value of the first output signal.

10. A liquid chemical delivery system, comprising:

a multi-reservoir load cell assembly, including a main reservoir with a gas inlet, a liquid inlet, and a liquid outlet, and a buffer reservoir with a gas inlet and a liquid inlet;

at least one load cell to weigh the chemical contained in the assembly and generate an output signal indicative of the weight;

a first valve and a second valve associated with the main reservoir liquid inlet;

a third valve connecting the main reservoir liquid outlet and the buffer reservoir liquid inlet;

a fourth valve connecting the main reservoir gas inlet and the buffer reservoir gas inlet;

means, responsive to the output signal, for refilling the buffer reservoir with chemical when the output signal indicates chemical in the buffer reservoir has dropped to a predetermined level, comprising;

closing the third valve to isolate the main reservoir from the buffer reservoir,

opening the fourth valve to evacuate the main reservoir to draw liquid chemical into the main reservoir until the liquid chemical rises to a predetermined level,

opening the valve between the main reservoir and the buffer reservoir to allow the liquid chemical in the main reservoir to flow into the buffer reservoir.

11. A liquid chemical delivery system coupled to one or more supply containers, comprising:

a multi-reservoir load cell assembly, including a main reservoir, a buffer reservoir, and at least one load cell;

a logic device coupled to the load cell(s) providing output signals to actuate;

means for sealing and unsealing the buffer reservoir from the main reservoir,

a vacuum generator for evacuating the main reservoir to draw liquid chemical from the supply container(s) to the main reservoir; and

a gas source supplying the main reservoir to blanket the liquid chemical in the main reservoir.

12. The system of claim 11, wherein the means for sealing and unsealing includes a shaft or valve disposed between the main reservoir from the buffer reservoir.

13. The system of claim 11, wherein the assembly includes a first load cell and a second load cell generating first and second signals indicating the weight of the main and buffer reservoirs to the logic device.

14. The system of claim 11, wherein the logic device monitors the weight of the buffer reservoir so that if the rate of liquid chemical consumption will empty the buffer reservoir before the refill is complete, the system can stop refill and/or transport liquid chemical from the main reservoir to the buffer reservoir to prevent emptying the buffer reservoir.

15. The system of claim 11, wherein the means for refill include means for flexibly connecting the buffer reservoir to a main valve at the main reservoir and suspending the buffer reservoir from the main reservoir.

16. The system of claim 13, further comprising means for starting refill when the second load cell detects the weight of the buffer reservoir is decreasing which indicates the main reservoir is empty.

17. A liquid chemical delivery system adapted for one or more supply containers, comprising:

a multi-reservoir load cell assembly, including a main reservoir, a buffer reservoir, and at least one load cell;

a logic device coupled to the load cell(s) providing output signals to actuate;

means for sealing and unsealing the buffer reservoir from the main reservoir,

a vacuum generator communicating with the main reservoir for evacuating the main reservoir to draw liquid chemical from the supply container(s) into the main reservoir; and

a gas source communicating with the main reservoir to blanket the liquid chemical in the main reservoir.