Method of molding powdered plant fiber into high density materials

• US 6,103,377 A
• Filed: 11/24/1998
• Issued: 08/15/2000
• Est. Priority Date: 06/27/1996
• Status: Expired due to Term

• Current Assignee: Robert N. Clausi
• Original Assignee: Robert N. Clausi
• Inventors: Clausi, Robert N.
• Primary Examiner(s): WEISBERGER, RICHARD C
• Application Number:
  US09/198,626
• Time in Patent Office: 630 Days
• Field of Search: 428/221, 428/323, 428/332, 428/340, 428/357, 428/292.4, 428/397
• US Class Current: 428/397
• CPC Class Codes: B27N 3/02 from particles
• CPC Class Codes: Y10T 428/249921 Web or sheet containing structurally defined element or component
• CPC Class Codes: Y10T 428/249925 Fiber-containing wood product [e.g., hardboard, lumber, or wood board, etc.]
• CPC Class Codes: Y10T 428/25 Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
• CPC Class Codes: Y10T 428/26 Web or sheet containing structurally defined element or component, the element or component having a specified physical dimension
• CPC Class Codes: Y10T 428/27 Web or sheet containing structurally defined element or component, the element or component having a specified weight per unit area [e.g., gms/sq cm, lbs/sq ft, etc.]
• CPC Class Codes: Y10T 428/29 Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
• CPC Class Codes: Y10T 428/2973 Particular cross section

Abstract

A high density fiber product is made from natural lignin containing plant fibers. Plant fibers ranging in size below about 3000 microns in diameter are used. Binding agents and other additives may be mixed with the fibers to enhance product or process performance. The plant fibers or mixture of fibers and additives are heated to between about 50 degrees C. to about 140 degrees C. The heated fibers are compressed in a mold to an average density of about 50 pounds per cubic foot to about 100 pounds per cubic foot. Compression pressures of about 500 psi to about 2500 psi are used to achieve product densities within this range. The compressed fibers are cured under these temperature and pressure conditions. After the curing time has elapsed, the compressed fiber product is released from the mold and the mold may be reused. A high density product made from small plant fibers is provided.

Claims

1. A high density plant fiber product made substantially from plant fibers containing protolicnin and being of less than about 3000 microns in diameter compressed to an average density of at least about 50 pounds per cubic foot.

2. The product of claim 1 wherein the said product has been compressed to an average density of at least 60 pounds per cubic foot.

3. The product of claim 1 wherein the plant fibers are between about 50 microns to about 1500 microns in diameter.

4. The product of claim 1 wherein the plant fibers are compressed to an average density of between about 50 pounds per cubic foot to about 100 pounds per cubic foot.

5. The product of claim 4 wherein the plant fibers comprise less than about 20 per cent water by weight.

6. The product of claim 5 wherein the plant fibers comprise between about 5 per cent and 12 per cent water by weight.

7. The product of claim 6 containing one or more of the group of additives comprising a binding agent, a releasing agent, a surface coating, a catalyst, a flame retardant, a flame resistant agent, a fire resistant agent, and a lubricating agent.

8. The product of claim 7 containing a binding agent and release agent, the binding agent comprising between about 0.25 per cent and about 50 per cent by weight of the plant fiber mixture.

9. The product of claim 8 containing a binding agent comprising between about 2 per cent and about 20 per cent by weight of the plant fiber mixture.

10. The product of claim 6 wherein the plant fibers are compressed to an average density of between about 60 pounds per cubic foot to about 90 pounds per cubic foot.

11. The product of claim 9 wherein the plant fibers are compressed to an average density of between about 60 pounds per cubic foot to about 90 pounds per cubic foot.

12. The product of claim 9 wherein the binding agent is a resin.

13. The product of claim 12 wherein the resin is one of the group of unsaturated polyester resin, polymeric diphenyl methane di-isocyanate.

24. The product of claim 1 compressed to an average density of at least 60 pounds per cubic foot.

25. The product of claim 24 made from the said plant fibers in a mixture comprising a thermoset binding agent and one or more of the group of additives comprising a releasing agent, a surface coating, a catalyst, a flame retardant, a flame resistant agent, pigment, and a lubricating agent.

26. The product of claim 25 wherein the binding agent is one of the group of unsaturated polyester resin, polymeric diphenyl methane di-isocyanate, methane di-isocyanate, melamine, urea, ester containing compounds, urea formaldehyde, and melamine-formaldehyde.

27. The product of claim 26 wherein the amount of the binding agent in the mixture is less than 25 per cent by weight of the mixture.

28. The product of claim 27 compressed to an average density of at least 70 pounds per cubic foot.

29. The product of claim 28 wherein the amount of binding agent in the mixture is less than 10 per cent by weight of the mixture.

30. The product of claim 27 comprising at least two zones, the first zone being compressed to a first density, the second zone being compressed to a second density, and the first density being greater than the second density.

31. The product of claim 30 wherein the density of the first zone is at least 60 pounds per cubic foot.

32. The product of claim 30 compressed to an average density of at least 75 pounds per cubic foot.

33. The product of claim 28 comprising an internal reinforcing member.

34. The product of claim 26 wherein the plant fibers are less than 1500 microns in diameter.

35. The product of claim 1 made from the said plant fibers in a mixture comprising a thermoset binding agent and one or more of the group of additives comprising a releasing agent, a surface coating, a catalyst, a flame retardant, a flame resistant agent, pigment, and a lubricating agent;

the binding agent being one of the group of unsaturated polyester resin, polymeric diphenyl methane di-isocyanate, methane di-isocyanate, melamine, urea, ester containing compounds, urea formaldehyde, and melamine-formaldehyde, in an amount of less than 25% by weight of the mixture; and

the mixture having been compressed into at least two zones, the first zone being compressed to a first density, the second zone being compressed into a second density, and the first density being greater than the second density.

36. The product of claim 35 wherein the plant fibers are less than 1500 microns in diameter.

37. The product of claim 36 wherein the amount of binding agent in the mixture is less than 10 per cent by weight of the mixture.

38. The product of claim 37 wherein the second density is at least 60 pounds per cubic foot and the first density is at least 75 pounds per cubic foot.

14. A plant fiber product mixture comprising plant fibers containnig protolignin and being of less than about 3000 microns in diameter and a binding agent equal to less than about 50 per cent by weight of the plant fiber mixture.

15. The product of claim 14 wherein the amount of binding agent represents less than about 20 per cent of the amount of plant fiber mixture.

16. The product of claim 14 wherein the binding agent is a resin.

17. The product of claim 16 wherein the resin is one of the group of unsaturated polyester resin, polymeric diphenyl methane di-isocyanate, methane di-isocyanate, melamine, urea, ester containing compounds, urea formaldehyde, and melamine-formaldehyde.

18. The product of claim 17 wherein the plant fibers are between about 50 microns to about 1500 microns in diameter.

19. The product of claim 18 wherein the plant fibers contain less than about 20 per cent water.

20. The product of claim 19 wherein the amount of binding agent is less than about 5 per cent of the plant fiber mixture.

21. A high density plant fiber product manufactured by a method comprising the steps of:

introducing powdered plant fiber particles containing protolignin and with a diameter less than 3000 microns into a mold;

heating the contents of the mold to a temperature between 50 degrees C. to 220 degrees C.;

compressing the powdered contents of the mold to an average density of at least 50 pounds per cubic foot;

curing the compressed contents within the mold; and

releasing the compressed contents from the mold.

22. A high density plant fiber product manufactured by a method comprising the steps of:

providing plant fibers containing protolignin and containing less than 20 per cent water by weight, the fibers being between 50 microns to 3000 microns in diameter;

blending a fluidized mixture of plant fibers and one or more of the group of additives consisting of a thermoset binding agent, a pigment, a releasing agent, a catalyst, a flame retardant, a flame resistant agent, a fire resistant agent, and a lubricating agent;

introducing the fluidized mixture of plant fibers and additives into the cavity of a mold;

compressing the mixture by applying a pressure of at least 500 psi to the surface of the mixture;

heating the contents of the mold cavity to between 50 degrees C. to 220 degrees C.;

curing the compressed contents; and

removing the compressed contents from the mold.

23. A high density plant fiber product manufactured by a method comprising the steps of:

preparing a particulate mixture comprising plant fibers less than 1500 microns in diameter and containing protolignin, a thermoset binding agent, and one or more of the group of additives consisting of a pigment, a releasing agent, a catalyst, a flame retardant, a flame resistant agent, and a lubricating agent;

introducing the particulate mixture into a mold;

heating the particulate mixture to a temperature between 60 degrees C. and 220 degrees C.;

compressing the mixture to an average density of at least 60 pounds per cubic foot within the mold; and

removing the compressed contents from the mold.