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Method for separation of liquid and solid phases for solid phase organic syntheses

  • US 6,121,054 A
  • Filed: 11/19/1997
  • Issued: 09/19/2000
  • Est. Priority Date: 11/19/1997
  • Status: Expired due to Fees
First Claim
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1. A method for separating a liquid phase from a solid phase, comprising:

  • (a) positioning an array of reaction vessels, said vessels containing a slurry of solid phase supports in a liquid, on the perimeter of a centrifuge rotor; and

    (b) spinning the rotor of the centrifuge at a speed so that the solid phase supports sediment in a pocket of the vessels from which material cannot be removed by centrifugal force and the liquid in excess of the volume of the pocket is expelled from the top of the vessels while spinning.

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