Method for processing mother liquors from the production of bisphenol
First Claim
1. In the working up the mother liquor obtained in the process for producing a dihydroxydiarylalkane by reacting phenols with ketone and isoalkenylphenol in the presence of acid catalyst the improvement comprising(a) removing phenol from said mother liquor by distillation, combining the bottoms thus obtained with a basic catalyst and continuously decomposing the combination in a reactive rectification stage into (i) phenol and isoalkenylphenol which pass overhead as the distillate, and (ii) bottoms, and (b) mixing said bottoms with an acid catalyst, continuously introducing the resulting mixture into a second reactive rectification stage to cause the decomposition of the mixture into (i) phenol and (ii) discarded bottoms, and (c) returning the phenol and isoalkenylphenol from stages (a) and (b) to said process.
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Abstract
The present invention relates to a process for working up the residual mother liquors from the production of dihydroxydiarylalkanes (bisphenols) discharged from the process once the bisphenol has been separated.
30 Citations
1 Claim
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1. In the working up the mother liquor obtained in the process for producing a dihydroxydiarylalkane by reacting phenols with ketone and isoalkenylphenol in the presence of acid catalyst the improvement comprising
(a) removing phenol from said mother liquor by distillation, combining the bottoms thus obtained with a basic catalyst and continuously decomposing the combination in a reactive rectification stage into (i) phenol and isoalkenylphenol which pass overhead as the distillate, and (ii) bottoms, and (b) mixing said bottoms with an acid catalyst, continuously introducing the resulting mixture into a second reactive rectification stage to cause the decomposition of the mixture into (i) phenol and (ii) discarded bottoms, and (c) returning the phenol and isoalkenylphenol from stages (a) and (b) to said process.
Specification
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- Resources
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Current AssigneeBayer AG
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Original AssigneeBayer AG
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InventorsFengler, Gerd, Fennhoff, Gerhard, Buysch, Hans-Josef
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Primary Examiner(s)Shippen, Michael L.
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Application NumberUS09/423,764Time in Patent Office466 DaysField of Search568/728, 568/727, 568/749US Class Current568/728CPC Class CodesC07C 39/04 PhenolY02P 20/10 Process efficiency
