System and method for contraband detection using nuclear quadrupole resonance

• US 6,194,898 B1
• Filed: 09/05/1997
• Issued: 02/27/2001
• Est. Priority Date: 03/08/1995
• Status: Expired due to Term

• Current Assignee: Quantum Magnetics, Inc. (GE Aerospace)
• Original Assignee: Quantum Magnetics, Inc. (GE Aerospace)
• Inventors: Magnuson, Erik E., Sheldon, Alan G., Moeller, Charles R., Shaw, Julian D.
• Primary Examiner(s): Oda, Christine K.
• Assistant Examiner(s): Shrivastav, Bry B.
• Application Number:
  US08/913,086
• Time in Patent Office: 1,271 Days
• Field of Search: 324/300, 324/309, 324/318, 324/322, 324/321
• US Class Current: 324/300
• CPC Class Codes: G01N 24/084 Detection of potentially hazardous samples, e.g. toxic samples, explosives, drugs, firearms, weapons
• CPC Class Codes: G01R 33/441 Nuclear Quadrupole Resonance [NQR] Spectroscopy and Imaging
• CPC Class Codes: G06V 10/255 Detecting or recognising potential candidate objects based on visual cues, e.g. shapes

Abstract

A system for detecting a target substance within a class of explosives and narcotics containing quadrupolar nuclei through the use of nuclear quadrupole resonance (NQR). The system applies an RF signal to a coil (34) to excite the substance under test. If the target material is present, an NQR signal will be picked up by the same coil, That signal is compared with known NQR signals in frequency and amplitude. A signal is displayed in an appropriate way if a threshold value of the NQR signal is equalled or exceeded. The empty coil is statically tuned by means of adjusting the location or capacitance values, or both, of static tuning capacitors (102) in the coil. The coil is tuned after the specimen is inserted into the coil by means of an auto-tune feature (36). Effective RFI shielding (37) is provided to prevent external contaminating signals from being detected by the coil and to prevent RF signals from escaping from the scanner. The invention also includes the method for performing tests with the system.

Claims

1. A system for detecting a target substance within a class of explosives and narcotics containing quadrupolar nuclei in a specimen employing the phenomenon of nuclear quadrupole resonance (NQR), said system comprising:

a sequence controller configured to provide timing and programming pulses to said system;

a radio frequency (RF) subsystem comprising a variable frequency RF source to provide pulsed RF excitation at a frequency generally corresponding to predetermined characteristic nuclear quadrupolar resonant frequency of the specimen, wherein nuclear quadrupolar resonant frequency is the frequency of nuclear precession due to quadrupolar interaction with molecular electric field gradients;

a detection subsystem comprising;

a distributed RF coil sheet shaped and configured to define a cavity of predetermined volume therein and to receive the specimen within the cavity defined by said RF coil, said cavity having a first end and a second end, the RF signal from said RF source being transmitted within said cavity and being applied to the specimen within said RF coil cavity, said RF coil also functioning as the pickup coil for the NQR signals from the specimen and providing an NQR output signal;

apparatus for adaptively tuning said RF coil to about the desired characteristic nuclear quadrupolar resonant frequency for the specimen under test; and

an electrically conductive RF shield surrounding and spaced from said RF coil, said RF shield being shaped and configured to provide electromagnetic interference and radio frequency interference (EMI/RFI) shielding from external noise and to prevent RF and magnetic flux from escaping from said RF coil cavity and RF shield combination, said RF shield being an electrically integral part of said RF coil and being shaped and configured to improve the Q and the efficiency of said RF coil and contributing to the effectiveness of the flux field applied to the specimen within said RF coil, said RF coil and RF shield together forming a scanner;

a signal capture and data processing subsystem comprising;

a receiver for the NQR output signal from said RF coil;

a memory which stores characteristics of NQR signals from at least one target substance in the class of explosives and narcotic compounds;

a processor for the NQR output signal from said RF coil; and

a comparator for comparing characteristics of the processed NQR output signal

with the characteristics in memory and emitting a final output signal; and

an indicating device receiving the final output signal from said signal capture and data processing subsystem and, in response thereto, said display device indicating the presence of the target substance.

2. The system recited in claim 1, wherein said RF coil cavity is configured to leave at least one end accessible, through which the specimen can be inserted.

3. The system recited in claim 2, wherein both ends of said cavity are open to enable specimens to enter at one end and leave at the other end in a continuous manner.

4. The system recited in claim 1, wherein said cavity is rectangular in shape, with its shorter sides having a first dimension, the spacing between said RF coil and said RF shield being in the range of about one-third of said first dimension to the full length of said first dimension.

5. The system recited in claim 4, wherein the spacing between said RF coil and said RF shield is about one-half of said first dimension.

6. The system recited in claim 4, wherein said RF shield extends past at least the open end of said RF coil by a distance that is substantially equal to one-half of said first dimension.

7. The system recited in claim 1, and further comprising at least one cavity extension element coupled to said scanner and comprising a wave guide below cut-off, said extension element having an opening therethrough which is about the same size as said cavity.

8. The system recited in claim 1, and further comprising a cavity extension element coupled to each end of said scanner and having an opening therethrough which is about the same size as said cavity, said extension elements comprising wave guides below cut-off.

9. The system recited in claim 2, wherein said cavity is rectangular in shape, with its shorter sides having a first dimension, the spacing between said RF coil and said RF shield being in the range of about one-third of said first dimension to the full length of said first dimension.

10. The system recited in claim 9, wherein said RF shield extends past at least the open end of said RF coil by a distance that is substantially equal to one-half of said first dimension.

11. The system recited in claim 1, wherein said adaptive tuning apparatus comprises means for automatically tuning said RF coil after the specimen is inserted therein for maximum power transfer efficiency.

12. The system recited in claim 11, wherein said automatic tuning means comprises:

a series of fixed value capacitors switched by controllable switch means; and

control means for controlling the switching sequence of said capacitors to establish maximum power transfer efficiency of said RF coil.

13. The system recited in claim 12, wherein each successive capacitor has a capacitive value which is a power of two greater than the previous one.

14. The system recited in claim 12, wherein said controllable switch means comprise a series of vacuum relays, one for each said capacitor, said vacuum relays being individually controlled by said control means.

15. The system recited in claim 1, and further comprising means to identify and differentiate acoustic ringing signals from NQR signals.

16. The system recited in claim 15, wherein said identifying and differentiating means comprises said sequence controller and said RF source, in combination with said detection subsystem to apply excitation RF pulses to said RF coil which are separate and distinct from the RF excitation pulses at the quadrupolar resonant frequency.

17. The system recited in claim 1, wherein said RF coil is formed on an insulator frame with a linear gap between confronting edges of said RF coil sheet, said detection subsystem further comprising:

a multiplicity of static tuning capacitors connected between said RF coil confronting edges, said static tuning capacitors being configured and spaced to provide an RF flux field of predetermined characteristics within said RF coil cavity when excited by RF pulses.

18. The system recited in claim 17, wherein said static tuning capacitors are so spaced that capacitance values are concentrated and spread farther apart based upon the NOR resonant frequency of the target substance.

19. A method for detecting a target substance within a class of explosives and narcotics containing quadrupolar nuclei in a specimen, said method employing the phenomenon of nuclear quadrupole resonance (NQR) in a detection system and comprising the steps of:

forming a scanner comprised of a distributed RF coil sheet shaped and configured to define a cavity of predetermined volume therein and to receive the specimen within the cavity defined by the RF coil, the RF coil being surrounded by an electrically conductive RF shield which is spaced from the RF coil, the shield being shaped and configured to provide electromagnetic interference and radio frequency interference (EMI/RFI) shielding from external noise and to prevent RF and magnetic flux from escaping from the scanner, the RF coil and RF shield being an integral combination portion of the scanner and being shaped and configured to improve the Q and the efficiency of the RF coil, the RF coil and RF shield contributing to the effectiveness of the flux field applied to the specimen when it is inserted within the RF coil cavity;

entering known characteristics of NQR signals of target substances in memory in a signal processor in the detection system;

providing programmed timing pulses to the detection system;

inserting the specimen within the cavity formed in the RF coil;

then

automatically adaptively tuning the RF coil to maximum power transfer efficiency for RF signals transmitted within the RF coil cavity;

providing excitation RF pulses of a predetermined frequency to the RF coil;

transmitting the RF pulses into the cavity formed by the RF coil and creating a flux field with the RF coil to which the specimen is subjected;

detecting by the RF coil the NQR signals emitted by target substances within the specimen;

processing the NQR signals and comparing them to known signal characteristics to determine whether the detected NQR signals indicate the presence of a target substance; and

indicating whether the target substance is present in the specimen.

20. The method of claim 19, and comprising the further step of identifying acoustic ringing signals and differentiating said ringing signals from NQR signals.

21. The method recited in claim 20, wherein said identifying and differentiating step comprises the steps of applying an RF signal to the RF coil which is separate and distinct from the NQR excitation signal, and determining if a ringing signal is present.

22. The method recited in claim 19, wherein said indicating step further provides indications whether conditions of the received signal indicate that further examination is necessary.

23. The method recited in claim 19, wherein said RF coil is formed around an insulative frame with a linear gap between confronting edges of the RF coil sheets, the confronting edges being coupled by means of static tuning distributed capacitance in the form of spaced fixed value capacitors, the spacing of the static tuning capacitors being determined by:

exciting the RF coil to about the target resonant frequency;

sensing the RF flux field intensities at locations throughout the RF coil cavity to map the relative field intensities;

linearly adjusting the capacitance in the gap;

re-mapping the field within the RF coil cavity and readjusting the gap capacitance to achieve a field within the RF coil cavity of predetermined characteristics when the RF coil is excited by RF pulses.

24. The method recited in claim 23, wherein the capacitance is adjusted by changing relative locations of the static tuning capacitors in the gap based upon the NOR resonant frequency of the target substance.