Process for recovery of corn coarse fiber (pericarp)

• US 6,254,914 B1
• Filed: 07/02/1999
• Issued: 07/03/2001
• Est. Priority Date: 07/02/1999
• Status: Expired due to Term

• Current Assignee: Board of Trustees of The University of Illinois
• Original Assignee: Board of Trustees of The University of Illinois
• Inventors: Eckhoff, Steven R., Singh, Vijay
• Primary Examiner(s): PADEN, CAROLYN A
• Application Number:
  US09/345,018
• Time in Patent Office: 732 Days
• Field of Search: 426/18, 426/31, 426/549, 426/618, 426/478, 426/479, 426/481, 426/482, 127/43, 536/128
• US Class Current: 426/482
• CPC Class Codes: B02B 3/00 Hulling; Husking; Decorticating decorticating textile fibres D01B1/14; Polishing; Removing the awns in threshing machines A01F12/42; Degerming
• CPC Class Codes: B02B 5/02 Combined processes
• CPC Class Codes: B03B 5/28 by sink-float separation
• CPC Class Codes: B03B 5/34 Applications of hydrocyclones
• CPC Class Codes: B03B 9/00 General arrangement of separating plant, e.g. flow sheets

Abstract

A method of recovering corn coarse fiber by flotation, which features the use of a hydrocyclone, or other separating machinery, in which the specific gravity of the slurry contained therein has been increased to approximately 12-14 Baumé so that the corn coarse fiber is of a lighter density than the remainder of the slurry. Therefore, the corn coarse fiber can be separated from the remainder of the slurry because it floats to the top of the slurry. If the present pericarp recovery process is added to a modified dry-grind ethanol production line, a high value co-product (the pericarp) is added to the other co-products and the end-product of ethanol, which can all be sold, and the economic efficiency of the plant is increased. More specifically, the present invention provides a process for recovering corn coarse fiber including the steps of: soaking corn in water to loosen the attachments of various grain components therein to each other, degerminating the soaked corn to strip the corn coarse fiber and the germ away from the endosperm, recovering the germ, and recovering the corn coarse fiber by flotation.

Claims

1. A process for recovering corn coarse fiber comprising the steps of:

soaking corn in water to loosen the attachments of various grain components therein to each other;

degerminating the soaked corn to strip the corn coarse fiber and germ away from the endosperm;

recovering the germ by increasing the specific gravity of a slurry including the germ and corn coarse fiber therein to approximately within the range of 7.5 to 11 Baumé

for removal of the germ; and

recovering the corn coarse fiber by increasing the specific gravity of a slurry including the corn coarse fiber therein to approximately within the range of 11-16 Baumé

so that the corn coarse fiber floats to the top of said slurry for removal of said corn coarse fiber.

2. The process of claim 1, wherein said step of soaking the corn comprises soaking the corn in distilled water.

3. The process of claim 1, wherein said step of soaking the corn comprises soaking the corn for approximately 12 hour s at a temperature of approximately 59°

C.

4. The process of claim 1, wherein said step of degerminating the soaked corn comprises grinding the soaked corn.

5. The process of claim 1, wherein said step of recovering the germ comprises using germ hydrocyclones.

6. The process of claim 1, wherein the specific gravity of said slurry is increased by adding at least one of the following to said slurry:

corn starch, a salt, and sugar syrup.

7. The process of claim 1, wherein the specific gravity of said slurry is approximately within the range of 12-14 Baumé

.

8. The process of claim 1, wherein said corn coarse fiber. is separated from said slurry using hydrocyclones.

9. The process of claim 1, wherein said step of recovering the germ and said step of recovering the corn coarse fiber are performed together by flotation.

10. The process of claim 9, further comprising the steps of:

drying the combination of germ and corn coarse fiber; and

separating the germ and the corn coarse fiber from each other using an aspirator.

11. The process of claim 1, wherein said step of recovering said germ is performed prior to said step of recovering said corn coarse fiber.

12. A corn product removal process comprising the steps of:

soaking corn in water to loosen the attachments of various grain components therein to each other;

degerminating the soaked corn to strip the corn coarse fiber and germ away from the endosperm;

recovering the germ by increasing the specific gravity of a slurry including the germ and corn coarse fiber therein to approximately within the range of 7.5 to 11 Baumé

for removal of the germ;

recovering the corn coarse fiber by increasing the specific gravity of a slurry including the corn coarse fiber therein to approximately within the range of 11-16 Baumé

so that the corn coarse fiber floats to the top of said slurry for removal of said corn coarse fiber;

fermenting remaining slurry; and

distilling fermented liquid to produce ethanol.

13. The process of claim 12, wherein the specific gravity of said slurry is approximately within the range of 12-14 Baumé

.

14. The process of claim 13, wherein the specific gravity of said slurry is increased by adding at least one of the following to said slurry:

corn starch, a salt, and sugar syrup.

15. The process of claim 13, wherein said corn coarse fiber is separated from said slurry using hydrocyclones.

16. The process of claim 12, wherein said step of recovering the germ and said step of recovering the corn coarse fiber are performed together by flotation.

17. The process of claim 16, further comprising the steps of:

drying the combination of germ and corn coarse fiber; and

separating the germ and the corn coarse fiber from each other using an aspirator.

18. The process of claim 12, wherein said step of recovering said germ is performed prior to said step of recovering said corn coarse fiber.

19. A process for recovering corn coarse fiber during a dry-grind ethanol production process, said recovery process comprising the steps of:

soaking corn in chemical-free water to loosen the attachments of various grain components therein to each other;

degerminating the soaked corn to strip the corn coarse fiber and germ away from the endosperm; and

recovering the corn coarse fiber by increasing the specific gravity of a slurry including the corn coarse fiber therein to approximately within the range of 11-16 Baumé

so that the corn coarse fiber with the germ floats to the top of said slurry for removal of said corn coarse fiber with the germ.