Methods and apparatus for obtaining transmission spectra of liquid and solid samples

• US 6,280,690 B1
• Filed: 12/30/1998
• Issued: 08/28/2001
• Est. Priority Date: 12/30/1997
• Status: Expired due to Fees

• Current Assignee: Jay Tadion
• Original Assignee: Jay Tadion
• Inventors: Tadion, Jay
• Primary Examiner(s): Soderquist, Arlen
• Application Number:
  US09/222,757
• Time in Patent Office: 972 Days
• Field of Search: 422/99, 422/100, 422/102, 422/104, 436/164, 245/7-8, 250/339.07, 356/244
• US Class Current: 422/560
• CPC Class Codes: G01N 21/3563 for analysing solids; Preparation of samples therefor

Abstract

A sample holder for spectroscopy is formed by pressing a wire mesh so that its thickness is reduced. Preferably the mesh is formed of stainless steel strands of 25 microns thickness, and is pressed to a thickness of 10-20 microns.

Claims

1. A spectroscopic sample holder comprising a mesh formed from strands of wire and supported in a frame having an open aperture, which mesh has been pressed to reduce its thickness to no more than 20 microns, the pressed mesh having a transmission of at least about 60%.

2. A sample holder as claimed in claim 1, wherein said wire is stainless steel.

3. A sample holder as claimed in claim 2, wherein the mesh has been thermally treated to improve the wettability in order to improve the uptake of liquid samples or solutions.

4. A sample holder as claimed in claim 2, wherein the mesh has been chemically treated to improve the wettability order to improve the uptake of liquid samples or solutions.

5. A sample holder as claimed in claim 1 wherein the thickness of the pressed mesh is in the range of 10-20 microns.

6. A sample holder as claimed in claim 1, wherein the mesh has been thermally treated to improve the wettability in order to improve the uptake of liquid samples or solutions.

7. A sample holder as claimed in claim 1, wherein the mesh has been chemically treated to improve the wettability order to improve the uptake of liquid samples or solutions.

8. A method of forming a spectroscopic sample holder comprising the steps of:

providing a mesh formed from wires,

pressing said mesh between hardened dies so as to Seduce its thickness to no more than 20 microns and such that its transmission is at least about 60% and mounting said mesh in a holder having an open aperture.

9. A method as claimed in claim 8, wherein the pressure applied to the mesh is in the region of 150-250 MPa.

10. A method as claimed in claim 8 wherein said wire is stainless steel.

11. A method as claimed in claim 10, wherein after the mesh has been pressed the total thickness thereof is in the region of 10-20 microns.

12. A method as claimed in claim 8, wherein after the mesh has been pressed the total thickness thereof is in the region of 10-20 microns.

13. A method as claimed in claim 8, further comprising thermally treating the mesh to improve the wettability in order to improve the uptake of liquid samples or solutions.

14. A method as claimed in claim 8, further comprising chemically treating the mesh to improve the wettability in order to improve the uptake of liquid samples or solutions by washing the mesh in acid.

15. A method of forming a sample holder for spectroscopy, comprising:

providing a mesh formed from stainless steel wires of thickness in the region of 25 microns, said mesh having a transmission of about 80%, pressing said mesh between hardened dies so as to reduce its thickness to the region of 10-20 microns with a transmission of at least about 60%, and mounting said mesh in a holder having an open aperture.