Non-invasive fluid flow sensing based on injected heat tracers and indirect temperature monitoring

• US 6,386,050 B1
• Filed: 12/21/1999
• Issued: 05/14/2002
• Est. Priority Date: 12/21/1999
• Status: Expired due to Term

• Current Assignee: Agilent Technologies Europe BV (Agilent Technologies, Inc.)
• Original Assignee: Agilent Technologies, Inc.
• Inventors: Templin, Catherine, Yin, Hongfeng
• Primary Examiner(s): PATEL, HARSHAD R
• Application Number:
  US09/468,695
• Time in Patent Office: 875 Days
• Field of Search: 738/619.5, 738/610.7, 732/041.4
• US Class Current: 73/861.95
• CPC Class Codes: A61M 2205/3306 Optical measuring means
• CPC Class Codes: A61M 5/16886 for measuring fluid flow rate, i.e. flowmeters
• CPC Class Codes: G01F 1/6847 where sensing or heating elements are not disturbing the fluid flow, e.g. elements mounted outside the flow duct
• CPC Class Codes: G01F 1/7084 using thermal detecting arrangements
• CPC Class Codes: G01F 1/7086 using optical detecting arrangements
• CPC Class Codes: G01F 1/7088 using electrically charged particles as tracers

Abstract

A system and method for measuring flow rate within a fluid-bearing passageway include introducing heat fluctuations into the flow and then non-invasively monitoring the effects of the heat fluctuations propagating to or from one or more interrogation regions. In one embodiment, the non-invasive monitoring detects fluctuations in the refractive index of the flowing fluid as a result of variations in the temperature of the fluid. In another embodiment, electrical conductivity of the fluid is monitored. The heat fluctuations may be introduced using an optical heat generator, such as an infrared laser, or may be introduced using an electrical member, such as a heater coil. Determining the refractive index along the interrogation region may be achieved by monitoring characteristics on an interference pattern, but other optical arrangements may be utilized.

Claims

1. A system for monitoring flow comprising:

a fluid-bearing passageway having an interrogation region;

a heat generator that is physically isolated from fluid flow through said fluid-bearing passageway while being in thermal transfer engagement with said fluid-bearing passageway, said heat generator being configured to selectively introduce temperature fluctuations into said fluid flow through said fluid-bearing passageway;

one of an optical and electrical source that is physically isolated from said fluid flow through said fluid-bearing passageway while being operationally associated with said interrogation region to form at least one of a capacitive cell and a light probing arrangement at said interrogation region;

a detector positioned relative to said interrogation region to monitor temperature changes within said interrogation region, said detector being configured to measure at least one of resistivity within said interrogation region and light redirected at said interrogation region as a result of interaction with said fluid flow and said fluid-bearing passageway; and

rate determination capability connected to said detector to monitor progress of said temperature fluctuations through said fluid-bearing passageway on a basis of measurements of at least one of resistivity and refractive index, said rate determination capability being configured to identify fluid flow rate within said fluid-bearing passageway based upon said monitoring of said progress.

2. The system of claim 1 wherein said source includes a laser and wherein said detector is positioned to detect an interference pattern generated by redirections of incident light from said fluid flow and said fluid-bearing passageway.

3. The system of claim 2 wherein said detector is an imaging detector having a field of view that is sufficiently large to detect a plurality of maxima of said interference pattern.

4. The system of claim 2 wherein said detector is a single-element light sensor having a field of view that is restricted to detecting less than two adjacent maxima or two adjacent minima of said interference pattern.

5. The system of claim 2 wherein said laser has a center wavelength of less than 1100 nm and wherein said heat generator is a heating laser having a center wavelength within the infrared range of the light spectrum.

6. The system of claim 2 wherein said laser and said detector are cooperative to propagate light energy through said fluid-bearing passageway and to detect said light energy, said rate determination capability being adapted to identify temperature fluctuations within said fluid-bearing passageway based upon angular fluctuations of the axis of said light energy following propagation through said fluid flow and said fluid-bearing passageway.

7. The system of claim 1 wherein said source is configured to form a capacitive cell by positioning electrode plates adjacent to said fluid-bearing passageway and wherein said detector measures resistivity of fluid within said interrogation region.

8. The system of claim 1 wherein said fluid-bearing passageway is a capillary tube micro.

9. The system of claim 1 further comprising:

a second source of optical or electrical energy physically isolated from but operationally associated with said fluid flow upstream of said heat generator, thereby defining a second interrogation region; and

a second detector positioned relative to said second interrogation region of said fluid-bearing passageway to monitor temperature changes within said interrogation region, said detector being configured to measure at least one of resistivity and light redirected at said second interrogation region, said second detector having an output that is indicative of measurements of said at least one of said resistivity and said redirected light;

wherein said rate determination capability is enabled to dynamically identify said flow rate based upon temperature-dependent differences in at least one of resistivities and refractive indices upstream and downstream of said heat generator.

10. A method of monitoring flow in a fluid-bearing passageway comprising steps of:

introducing propagating heat fluctuations into a flow of liquid through said passageway, said propagating heat fluctuations being introduced at a first position along said passageway;

measuring temperature-dependent changes in resistivity of said liquid along a first interrogation region of said passageway, including monitoring said resistivity over a period of time sufficiently great to enable at least one said propagating heat fluctuation to propagate into said first interrogation region; and

determining a flow rate of said liquid based upon said monitoring of said resistivity to determine times for said propagating heat fluctuations to travel from said first position to said interrogation region.

11. The method of claim 10 wherein said step of measuring resistivity includes applying an alternating current to electrodes positioned adjacent to said first interrogation region and includes calculating measurements of resistivity on a basis of parameters related to capacitive coupling across said electrodes.

12. The method of claim 10 further comprising steps of:

measuring temperature-dependent changes in resistivity of said liquid along a second interrogation region of said passageway, said first and second interrogation regions being on opposite sides of said first position, including monitoring said resistivity along said second interrogation region over said period of time simultaneously with monitoring said resistivity along said first interrogation region; and

utilizing said step of monitoring said resistivity along said second interrogation region to determine said flow rate.

13. The method of claim 12 wherein said steps of introducing said propagating heat fluctuations and measuring resistivity are implemented in an absence of physical contact between said liquid and equipment for performing said steps, said step of determining said flow rate including monitoring shifts between a phase of said heat fluctuations and a phase of fluctuations in resistivity.

14. The method of claim 10 further comprising providing a capillary having a cross sectional dimension of less than 500 μ

m and includes directing a liquid of interest through said capillary, thereby providing said fluid-bearing passageway.

15. A method of monitoring flow in a fluid-bearing passageway comprising steps of:

introducing heat fluctuations into a flow of liquid through said passageway, said heat fluctuations being introduced at a first position along said passageway;

directing a beam from a light source into said liquid at a first interrogation region of said passageway;

detecting light energy from said beam following interaction of said light energy with said liquid, including monitoring refractive index of said liquid over a period of time; and

determining a flow rate of said liquid based upon said monitoring of said refraction index and upon determining times required for said heat fluctuations to travel from said first position to said first interrogation region, including detecting entrances of said heat fluctuations into said first interrogation region by correlating changes in said refractive index with said entrances of said heat fluctuations.

16. The method of claim 15 wherein said step of monitoring said refraction index includes detecting an interference pattern created by said step of directing said beam, and wherein said step of determining said flow rate includes determining calculations of said flow rate on a basis of variations in said interference pattern as a function of said entrances of said heat fluctuations into said first interrogation region.

17. The method of claim 15 further comprising steps of:

directing a second beam into said liquid at a second interrogation region that is upstream of said first position and said first interrogation region;

detecting light energy from said second beam following refraction as a result of interaction with said liquid; and

utilizing said detected light from said second beam in said step of determining said flow rate.

18. The method of claim 15 wherein said step of detecting said light energy includes determining fluctuations in angles of said light energy that propagates through said liquid.

19. The method of claim 15 wherein said step of introducing said heat fluctuations includes directing modulated infrared light into a capillary and wherein said step of directing said beam includes utilizing a laser source having a center frequency that does not exceed 1100 nm.