Method and apparatus for delivery of fragrances and vapors to the nose

• US 6,390,453 B1
• Filed: 04/30/2001
• Issued: 05/21/2002
• Est. Priority Date: 10/22/1997
• Status: Expired due to Term

• Current Assignee: Microfab Technologies, Inc.
• Original Assignee: Microfab Technologies, Inc.
• Inventors: Frederickson, Christopher J., Taylor, David W., Wallace, David B., Hayes, Donald J., Hayes, Matthew D.
• Primary Examiner(s): Hopkins, Robert A.
• Application Number:
  US09/845,714
• Time in Patent Office: 386 Days
• Field of Search: 261/78.2, 261/26, 261/100, 261/142, 261/DIG.17, 261/DIG.65, 261/DIG.88, 422/123, 422/124
• US Class Current: 261/26
• CPC Class Codes: A61M 11/001 Particle size control
• CPC Class Codes: A61M 11/042 electrical
• CPC Class Codes: A61M 15/02 with activated or ionised fluids, e.g. electrohydrodynamic [EHD] or electrostatic devices; Ozone-inhalators with radioactive tagged particles
• CPC Class Codes: A61M 15/025 Bubble jet droplet ejection devices
• CPC Class Codes: A61M 2205/8206 battery-operated
• CPC Class Codes: B01F 23/12 with vaporisation of a liquid disinfection, sterilisation or deodorisation of air A61L9/00
• CPC Class Codes: B01F 23/2132 using nozzles
• CPC Class Codes: B01F 35/71791 using ink jet heads or cartridges, e.g. of the thermal bubble jet or piezoelectric type
• CPC Class Codes: F24F 8/50 by odorisation
• CPC Class Codes: Y10S 261/65 Vaporizers
• CPC Class Codes: Y10S 261/88 Aroma dispensers

Abstract

A method and apparatus is disclosed which employs a pulse-controlled microdroplet fluid delivery system for precisely dispensing fragrances and other odor producing vapors. The pulse-controlled fluid delivery device is capable of ejecting microdroplets of fluid with a diameter less than 350 micrometers at a controlled ejection rate based upon ink-jet printing technology. The pulse-controlled fluid delivery system includes mechanisms for vaporizing the fluids and delivery of the vapors to the nose, which is controlled by a programmable system controller capable of real time data-driven dispensing with a multi-fluid capability. Synthesis of custom fragrances is made possible by a multijet programmed control system which adjusts dispensing rates of components. Calibration of a prior art “electronic nose” is disclosed. A precise calibration gas is produced in real-time to counteract the effect of drifting.

Claims

1. Apparatus for controlled dispensing of volatile material, comprising:

a housing containing a target medium comprising a heater having a heating surface and an air-flow outlet;

an electronically operated fluid droplet ejection device mounted with the housing, said ejection device having a fluid supply reservoir and a droplet ejection orifice aimed to deposit fluid droplets onto the heating surface;

drive electronics operably connected to said ejection device;

a system controller operably connected to the drive electronics and a power source whereby operating signals are delivered to the drive electronics to cause sequential droplets of fluid to be deposited onto the heating surface where they can be completely_volatilized and pass from the housing through the air-flow outlet, to be perceived by the mammalian_nose.

2. The apparatus of claim 1 wherein the housing includes an air movement device positioned to move air from t he housing through the air-flow outlet.

3. The apparatus of claim 1 wherein the heater is under control of the system controller, having a quickly heatable heating_surface upon which said fluid droplets are deposited.

4. The apparatus of claim 3 wherein the heater is controlled to quickly raise the temperature of the quickly heatable heating surface to a temperature selected to vaporize fluid droplets deposited thereon when the ejection device is operated and return to an unheated state when the ejection device ceases operation in order to control vaporization of the deposited fluid.

5. The apparatus of claim 3 wherein said housing includes an air-flow passageway leading to the air-flow outlet wherein said heating surface is exposed and positioned to receive fluid droplets deposited thereon by the ejection device whereby vapor is released into the air-flow passageway by volatilization of said droplets.

6. The apparatus of claim 5 wherein the air movement device comprises a fan operated by the system controller positioned to force air over the heating surface in the air flow passageway and thereby carry vapor from the passageway to the air flow outlet.

7. The apparatus of claim 1 wherein the ejection device includes a heater operated by the system controller to maintain the ejection device at an elevated temperature above ambient temperature.

8. The apparatus of claim 1 further including an electronic sensor operated by the controller wherein the volatilized fluid which passes from the housing is sensed by the electronic sensor to generate a signal representative of the volatilized fluid.

9. The apparatus of any one of claims 1 to 8, wherein the heating surface is a wettable surface which is wettable by said sequential droplets of fluid deposited onto the heating surface.

10. Apparatus for controlled dispensing of volatile fluids, comprising:

a support structure having a target medium comprising a heater having a heating surface;

a printhead mounted with the support structure, the printhead having a plurality of electronically operated fluid droplet ejection channels, each channel having a fluid supply reservoir and at least one orifice oriented to eject fluid droplets which are deposited on the heating surface of the target medium;

drive electronics operably connected to each ejection channel; and

a system controller operably connected to said drive electronics and a power source for the apparatus whereby operating signals are selectively delivered to the ejection channels thereby depositing fluid droplets from a selected one or ones of the ejection channels onto the heating surface where they can be completely volatilized and pass from the support structure to be perceived by the human nose.

11. The apparatus of claim 10 wherein the support structure includes an air-flow channel having an air-flow outlet.

12. The apparatus of claim 11 wherein the air-flow channel is provided with an air movement device, positioned to move air across the heating surface to the air-flow outlet.

13. The apparatus of claim 12 wherein the printhead is a heated printhead controlled by the system controller to increase printhead temperature above ambient temperature thereby increasing the temperature of fluid in the printhead before it is ejected.

14. The apparatus of claim 11 wherein the heater having a heated surface which comprises the target medium is controlled by the system controller to increase the rate of volatilization of fluid droplets deposited thereon.

15. The apparatus of claim 10 further including an electronic sensor operated by the system controller whereby volatilized fluid is measured.

16. The apparatus of any one of claims 10 to 15, wherein the heating surface is a wettable surface which is wettable by said sequential droplets of fluid deposited onto the heating surface.

17. Apparatus for controlled dispensing of volatile fluids, comprising:

a support structure,

the support structure including an air-flow channel having an air-flow outlet containing a target medium;

a printhead mounted on the support structure, the printhead having a plurality of electronically operated fluid droplet ejection channels, each channel having a fluid supply reservoir and at least one orifice oriented to eject fluid droplets which are deposited on the target medium;

drive electronics operably connected to each ejection channel;

a system controller operably connected to said drive electronics and a power source for the apparatus whereby operating signals are selectively delivered to the ejection channels thereby depositing fluid droplets from a selected one or ones of the ejection channels onto the target medium where thy can volatilize and pass from the support structure and

wherein the target medium comprises a heater controlled by the system controller having a plurality of differentially heatable surfaces and whereby the plurality of ejection channels are oriented to deposit fluid droplets on selected ones of said heatable surfaces to thereby control the rate at which different fluid droplets vaporize.

18. The apparatus of claim 17 wherein the air-flow channel is provided with an air movement device positioned to move air across the target medium to the air-flow outlet.

19. The apparatus of claim 18 wherein said air movement device is a fan operated by the system controller.

25. The method of claim 18 further including the steps providing an electronic sensor operably connected to the system controller and the step of sensing the odors produced by the ejection channels with the electronic sensor.

20. Method for controlled dispensing, comprising the steps of:

providing a support structure having a target medium, wherein the target medium comprises a heated target surface;

providing a printhead mounted on the support structure, the printhead having a plurality of electronically operated fluid droplet ejection channels and a fluid supply reservoir for each channel, each channel having at least one orifice oriented to deposit droplets of fluid onto the target medium;

providing a system controller connected to drive electronics for the printhead whereby commands are supplied through the system controller to selectively operate the ejection channels thereby depositing fluid droplets from a selected one or ones of the ejection channels onto the target medium;

loading some of the fluid supply reservoirs with different volatile fluids having different odor characteristics;

ejecting and depositing droplets of first fluid from a selected one of the ejection channels onto the heated surface for a first period of time to produce a first odor; and

ejecting and depositing droplets of a different second fluid from a different selected one of the ejection channels onto the heated surface for a time period, to produce a different odor.

21. The method of claim 20 wherein the droplets of first fluid and droplets of second fluid are ejected in a time sequence selected to produce a combined odor.

22. The method of claim 20 wherein the step of ejecting droplets of first fluid and the step of ejecting droplets of different second fluid are conducted respectively at a first rate and a second rate different from said first rate, said first and second rates being selected to deposit greater amounts of one of the first or second fluids on the target medium to generate a sufficient vapor concentration to achieve a desired odor experience.

23. The method of claim 20 wherein the time periods during which the first and second fluid are ejected and volatilized are selected to partially or completely overlap whereby an odor characteristic of the first fluid is segued into an odor characteristic of the second fluid.

24. The method of claim 20 comprising the steps of:

selecting the first and second fluids to produce a desired combined odor effect;

selecting respective first and second ejection rates to balance the amount of first and second fluid deposited to create the desired combined odor effect;

contemporaneously ejecting droplets of said first and second fluids at the selected first and second ejection rates to produce a desired odor effect.

32. The method of any one of claim 20 or 26 or 27 or 30 comprising the steps of:

providing an air-flow channel containing the target medium, having an air-flow outlet;

providing an air movement device cooperating with the air-flow channel in response to signals from the system controller to move air across the target medium to the air-flow outlet;

operating the air movement device during one or more of the droplet ejecting steps to increase volatilization of droplets deposited onto the target medium.

26. Method for controlled dispensing, comprising the steps of:

providing a support structure having a target medium;

providing a printhead mounted on the support structure, the printhead having a plurality of electronically operated fluid droplet ejection channels and a fluid supply reservoir for each channel, each channel having at least one orifice oriented to deposit droplets of fluid onto the target medium;

providing a system controller connected to drive electronics for the printhead whereby commands are supplied through the system controller to selectively operate the ejection channels thereby depositing fluid droplets from a selected one or ones of the ejection channels onto the target medium;

wherein the target medium comprises a first and second heated surface for volatilizing said fluids;

loading some of the fluid supply reservoirs with different volatile fluids having different odor characteristics;

ejecting and depositing droplets of first fluid from a selected one of the ejection channels onto the first heated surface for a first period of time to produce a first odor; and

ejecting and depositing droplets of a different second fluid from a different selected one of the ejection channels onto the second heated surface for a time period, to produce a different odor.

27. Method for controlled dispensing, comprising the steps of:

providing a support structure having a target medium;

providing a printhead mounted on the support structure, the printhead having a plurality of electronically operated fluid droplet ejection channels and a fluid supply reservoir for each channel, each channel having at least one orifice oriented to deposit droplets of fluid onto the target medium;

providing a system controller connected to drive electronics for the printhead whereby commands are supplied through the system controller to selectively operate the ejection channels thereby depositing fluid droplets from a selected one or ones of the ejection channels onto the target medium wherein the target medium comprises a medium having a target surface temperature controlled by the system controller;

loading some of the fluid supply reservoirs with different volatile fluids having different odor characteristics;

ejecting and depositing droplets of first fluid from a selected one of the ejection channels onto the target medium and raising the temperature of the target surface above ambient temperature to quickly evaporate any remnants of the first fluid from the target surface for a first period of time to produce a first odor before ejecting droplets of the second fluid onto the target medium; and

ejecting and depositing droplets of a different second fluid from a different selected one of the ejection channels onto the target medium for a time period, to produce a different odor.

28. The method of claim 27 further including the steps of:

ejecting said droplets of second fluid onto the target surface; and

raising the temperature of the target surface to quickly evaporate any remnants of second fluid from the target surface.

29. The method of claim 27 wherein the step of providing a target medium includes the step of providing a medium having at least two target surfaces comprising first and second target surfaces temperature controlled by the system controller and the step of ejecting droplets comprises the step of ejecting droplets of first fluid into a first target surface and second fluid onto a second target surface.

30. Method for controlled dispensing, comprising the steps of:

providing a support structure having a target medium comprising a first and second heated surface;

providing a printhead mounted on the support structure, the printhead having a plurality of electronically operated fluid droplet ejection channels and a fluid supply reservoir for each channel, each channel having at least one orifice oriented to deposit droplets of fluid onto one of the first and second heated surfaces;

providing a system controller connected to drive electronics for the printhead whereby commands are supplied through the system controller to selectively operate the ejection channels thereby depositing fluid droplets from a selected one or ones of the ejection channels onto the target medium;

loading some of the fluid supply reservoirs with different volatile fluids having different odor characteristics;

raising the temperature of the first and second target surfaces above ambient temperature; and

ejecting and depositing droplets of a first fluid onto said first heated surface and depositing droplets of said second fluid onto said second heated surface.

31. The method of claim 30 wherein the step of raising the temperature of the target surfaces above ambient temperature is the step of raising the first and second target surfaces to a predetermined temperature dependent respectively upon said first and second fluids.

33. A method of synthesizing an aroma, comprising the steps of:

providing a multiple fluid printhead having a plurality of electronically operated fluid droplet ejection channels and a fluid supply reservoir for each channel, each channel comprising a fluid ejection device having an orifice aimed to deposit ejected droplets into a testing space;

providing a programmed computer and drive electronics operably connected to the printhead wherein the programmed computer is programmed to selectively operate the ejection channels at a selected rate to eject droplets into the testing space;

providing multiple and different volatile testing fluids for the fluid supply reservoirs;

selecting a group of the fluid ejection devices to operate and selecting an operating rate;

operating the selected group of fluid ejection devices at the selected operating rate to produce a custom aroma which can be sensed in the vicinity of the testing space;

sensing the aroma produced by the selected fluid ejection devices at the testing space;

adjusting the selected rates at which some of the selected fluid ejection devices operate;

sensing the aroma produced at the selected rates by the selected fluid sensing devices; and

repeating the previous steps until a desired custom aroma is produced.

34. The method of claim 33 wherein the step of sensing the aroma is the step of sensing the aroma with a mammalian nose.

35. The method of claim 33 wherein the step of sensing the aroma is the step of sensing the aroma with an electronic sensor.

36. A method of synthesizing an aroma, comprising the steps of:

providing a multiple fluid printhead having a plurality of electronically operated fluid droplet ejection channels and a fluid supply reservoir for each channel, each channel comprising a fluid ejection device having an orifice aimed to deposit ejected droplets into a testing space;

providing a programmed computer and drive electronics operably connected to the printhead wherein the programmed computer is programmed to selectively operate the ejection channels at a selected rate to eject droplets into the testing space;

providing multiple and different volatile testing fluids for the fluid supply reservoirs;

selecting a group of the fluid ejection devices to operate and selecting an operating rate;

operating the selected group of fluid ejection devices at the selected operating rate to produce a custom aroma which can be sensed in the vicinity of the testing space;

providing a target medium at the testing space, the target medium comprising a heater having a heatable target surface which intercepts ejected droplets from some ejection devices;

providing a temperature control for the heater which is responsive to signals from the computer to generate an operating temperature above ambient temperature for the heatable target surface;

whereby volatilization of ejected droplets from said some ejection devices is enhanced during the operation step.

37. A method of synthesizing an aroma, comprising the steps of:

providing a multiple fluid printhead having a plurality of electronically operated fluid droplet ejection channels and a fluid supply reservoir for each channel, each channel comprising a fluid ejection device having an orifice aimed to deposit ejected droplets into a testing space;

providing a programmed computer and drive electronics operably connected to the printhead wherein the computer is programmed to selectively operate the ejection channels at a selected rate to eject droplets into the testing space;

providing multiple and different volatile testing fluids for the fluid supply reservoirs;

selecting a group of the fluid ejection devices to operate and selecting an operating rate;

providing a target medium at the testing space, the target medium comprising an array of heaters each having a heatable target surface which intercepts ejected droplets from some ejection devices;

providing a temperature control for the heaters which is responsive to signals from the computer to generate an operating temperature above ambient temperature for the heatable target surfaces at least some of which are being held at different surface temperatures above ambient temperature;

operating the selected group of fluid ejection devices at the selected operating rate to produce a custom aroma which can be sensed in the vicinity of the testing space; and

whereby volatilization of ejected droplets from said some ejection devices is enhanced during the operation step.

38. Method for controlled dispensing of volatile materials, comprising:

providing a support structure having a target medium comprising a heater having a heating surface;

providing a printhead having a plurality of electronically digitally operated fluid droplet ejection devices and a fluid supply reservoir for each device, each device having at least one ejection orifice oriented to deposit sequential droplets of fluid onto the heating surface;

providing a system controller having drive electronics connected to the printhead whereby commands are supplied to the printhead through the system controller to selectively operate one or more of the ejection devices thereby depositing fluid droplets produced by at least one of the ejection devices onto the heating surface;

providing different volatile fluids having different odor characteristics in at least some of the fluid supply reservoirs;

selecting at least one of the ejection devices containing a volatile fluid for operation to produce a desired odor;

operating the heater to raise the heating surface to an elevated temperature calculated to promptly volatilize the volatile fluid from the selected ejection device;

operating the selected at least one ejection device to deposit its volatile fluid onto the heating surface where it is quickly volatilized to produce an odor; and

delivering the volatilized fluid to an outlet where the odor can be experienced by the human nose.

39. The method of claim 38 wherein the step of selecting at least one of the ejection devices comprises the step of selecting two of the ejection devices to produce different odors and the step of operating the selected at least one ejection device comprises the step of operating the selected ejection devices sequentially to deposit droplets of different volatile fluids onto the elevated temperature surface so as to produce two different odor sensations.

40. The method of claim 38 or 39 wherein the step of providing a target medium comprising a heater having a heating surface is the step of producing a heating surface which is wettable by the volatile fluids and the step of operating the selected at least one ejection device to volatilize the selected volatile fluid is accompanied by wetting of the heating surface by said volatile fluid.