Method and apparatus for lysing sludge and dividing solids in liquid suspension

• US 6,402,065 B1
• Filed: 12/22/1999
• Issued: 06/11/2002
• Est. Priority Date: 06/24/1997
• Status: Expired due to Fees

• Current Assignee: Kady International
• Original Assignee: Kady International
• Inventors: Higgins, John A.
• Primary Examiner(s): Ostrager, Allen
• Assistant Examiner(s): Hong, William
• Application Number:
  US09/446,567
• Time in Patent Office: 902 Days
• Field of Search: 241/20, 241/21, 241/46.06, 241/46.17, 241/185.6, 241/258
• US Class Current: 241/21
• CPC Class Codes: B02C 18/0092 for waste water or for garbage
• CPC Class Codes: B02C 18/062 with rotor elements extending axially in close radial proximity of a concentrically arranged slotted or perforated ring
• CPC Class Codes: C02F 11/121 by mechanical de-watering
• CPC Class Codes: C02F 3/1221 comprising treatment of the recirculated sludge
• CPC Class Codes: Y02W 10/10 Biological treatment of water, waste water, or sewage

Abstract

Apparatus and system to mechanically lyse microbial cells and disintegrate particulate in liquid and recycling the lysed cells, cytoplasm and particulates to the aeration system of a wastewater treatment plant. The method of lysis is cavitation and impingement in a mill, which preferably has a plurality of stages, each with a rotor/stator set. A corresponding plurality of dividers within the mill channel the fluid sequentially through each of the plurality of stages. Orifice plates may be utilized to maximize cavitation by controlling flow into the rotors, which preferably have tapering slots to maximize cavitation.

Claims

1. A dispersion mill, comprising an annular rotor with a first series of slots therein, each slot of said first series of slots having a first slot wall and a second slot wall, said first slot wall and said second slot wall of a plurality of said first series of slots converging toward one another in a radially outward direction;

and an annular stator with a second series of slots therein, each slot of said second series of slots intermittently aligning with each slot of said first series of slots as said rotor is rotated relative to said stator to thereby discharge flowable matter from said rotor into said stator when said rotor is rotated.

2. The dispersion mill of claim 1, wherein said first slot wall of each of said plurality of said first series of slots diverges from a radial orientation by about 23 degrees and wherein said second slot wall of each of said plurality of said first series of slots diverges from a radial orientation by about 34 degrees.

3. The dispersion mill of claim 1, wherein said second series of slots includes a plurality of chamfered slots, each of which is chamfered at a leading edge thereof.

4. The dispersion mill of claim 1, wherein said rotor has a central axially-extending opening, an inner circumferential surface delimiting said opening, and an outer circumferential surface delimiting a periphery of said rotor, said first series of slots extending generally radially through said rotor from said inner circumferential surface thereof to said outer circumferential surface thereof.

5. The dispersion mill of claim 4, wherein each slot of said first series of slots is sized and shaped so as to discharge a corresponding stream of flowable matter in a generally radial direction relative to a longitudinal axis of said rotor upon the rotation of said rotor about said longitudinal axis.

6. Apparatus for producing liquid suspensions of finely divided matter, comprising a housing accommodating flowable matter, said housing having an input opening for admitting flowable matter to be processed and an output opening for discharging processed flowable matter;

a two-stage mill disposed within said housing, said mill including a rotable drive shaft extending through said housing, a first stage with a first annular rotor, which is mounted on said drive shaft and which has a first series of slots therein, and a first annular stator, which has a second series of slots therein and which cooperates with said first rotor to process flowable matter, and a second stage having a second annular rotor, which is mounted on said drive shaft and which has a third series of slots therein, and a second annular stator, which has a fourth series of slots therein and which cooperates with said second rotor to process flowable matter, each slot of said first series of slots intermittently aligning with each slot of said second series of slots to discharge flowable matter from said first rotor into said first stator, and each slot of said third series of slots intermittently aligning with each slot of said fourth series of slots to discharge flowable matter from said second rotor into said second stator; and

controlling means disposed within said housing for controlling the flow of flowable matter such that it passes through said first stage and then through said second stage.

7. The apparatus of claim 6, wherein said first rotor and said second rotor each have a central axially-extending opening, an inner circumferential surface delimiting said opening, and an outer circumferential surface delimiting a periphery thereof, said first series of slots extending generally radially through said first rotor from said inner circumferential surface thereof to said outer circumferential surface thereof, said third series of slots extending generally radially through said second rotor from said inner circumferential surface thereof to said outer circumferential surface thereof.

8. The apparatus of claim 7, wherein each slot of said first series of slots and said third series of slots is sized and shaped so as to discharge a corresponding stream of flowable matter in a generally radial direction relative to a longitudinal axis of said first and second rotors, respectively, upon the rotation of said first and second rotors about their respective longitudinal axis.

9. The apparatus of claim 6, wherein said controlling means includes at least one divider member.

10. The apparatus of claim 9, wherein said at least one divider member includes a first divider member disposed between said inlet opening and said first stage, said first divider member having a first orifice therein through which flowable matter passes to enter said first series of slots provided in said first rotor of said first stage.

11. The apparatus of claim 10, wherein said at least one divider member includes a second divider member disposed between said first stage and said second stage, said second divider member having a second orifice therein through which said flowable matter passes to enter said third series of slots provided in said second rotor of said second stage.

12. The apparatus of claim 11, wherein said controlling means includes a flow cage interposed between said first stator of said first stage and said second divider member, said flow cage permitting flowable matter exiting said first stator of said first stage to flow through said flow cage and enter said second orifice provided in said second divider member.

13. The apparatus of claim 12, wherein said drive shaft passes through said first and second orifices of said first and second divider members, respectively.

14. The apparatus of claim 13, wherein said housing is substantially cylindrical, said first and second divider members being substantially disc-shaped and sealingly received within said housing.

15. The apparatus of claim 14, wherein said housing has an interior surface, each of said first and second divider members forming a seal with said interior surface of said housing.

16. The apparatus of claim 15, further comprising a support spider mounted in said housing, said support spider having a plurality of spaced arms through which flowable matter may pass, said spaced arms supporting at one end thereof said first divider member, said first stator of said first stage being supported upon said first divider member, said flow cage being supported upon said stator of said first stage, said second divider member being supported upon said flow cage, and said second stator of said second stage being supported upon said second divider member.

17. The apparatus of claim 14, wherein said first divider member includes a first inner member in which said first orifice is formed and a first outer member in which said first inner member is inserted to define said first divider member.

18. The apparatus of claim 17, wherein said first inner member is disc-shaped and said first orifice is substantially circular and proximate a center of said first inner member.

19. The apparatus of claim 18, wherein said first outer member is disc-shaped with a central aperture therein accommodating said first inner member, whereby said first inner member is separately replaceable relative to said first outer member.

20. The apparatus of claim 19, wherein said second divider member includes a second inner member in which said second orifice is formed and a second outer member in which said second inner member is inserted to define said second divider member.

21. The apparatus of claim 20, wherein said first inner member is proximate and substantially parallel to a lower surface of said first rotor.

22. The apparatus of claim 10, wherein the size of said first orifice in said first divider member is selected to provide maximum cavitation effects within said first stage of said mill.

23. The apparatus of claim 11, wherein the size of said second orifice in said second divider member is selected to provide maximum cavitation effects within said second stage of said mill.

24. A dispersion mill, comprising an annular rotor having a first series of slots therein, each slot of said first series of slots having an inner slot opening with an associated area and an outer slot opening with an associated area, the cumulative area of said inner slot openings exceeding the cumulative area of said outer slot openings;

and an annular stator with a second series of slots therein, each slot of said second series of slots intermittently aligning with each slot of said first series of slots as said rotor rotates relative to said stator to thereby discharge flowable matter from said rotor into said stator when said rotor is rotated.

25. The dispersion mill of claim 24, wherein said rotor has a central axially-extending opening, an inner circumferential surface delimiting said opening, and an outer circumferential surface delimiting a periphery of said rotor, said first series of slots extending generally radially through said rotor from said inner circumferential surface thereof to said outer circumferential surface thereof.

26. The dispersion mill of claim 25, wherein each slot of said first series of slots is sized and shaped so as to discharge a corresponding stream of flowable matter in a generally radial direction relative to a longitudinal axis of said rotor upon the rotation of said rotor about said longitudinal axis.

27. The dispersion mill of claim 24, wherein the ratio of the cumulative area of said inner slot openings to the cumulative area of said outer slot openings Is selected to maximize the cavitation effect in said mill based upon the solids concentration of flowable matter.

28. The dispersion mill of claim 27, wherein said ratio is about 2.1 for flowable matter with solids concentrations of about 1%.

29. The dispersion mill of claim 27, wherein said ratio is about 1:

1 for flowable matter with solids concentrations greater than about 4%.

30. The dispersion mill of claim 27, wherein said ratio is about 8:

1 for flowable matter with solids concentrations from about 0.01% to about 0.5%.

31. A method for dewatering a sludge stream, comprising the steps of:

continuously directing at least a portion of said stream to a dispersion mill of the type having an annular rotor with a first series of slots therein, each slot of said first series of slots having a first slot wall and a second slot wall, said first slot wall and said second slot wall of a plurality of said first series of slots converging toward one another in a radially outward direction, and an annular stator with a second series of slots therein, each slot of said second series of slots intermittently aligning with each slot of said first series of slots as said rotor is rotated relative to said stator to thereby discharge said slurry from said rotor into said stator when said rotor is rotated;

lysing solids in said portion in said dispersion mill to thereby generate nutrients for cellular respiration; and

reintroducing said portion passing through said mill to said stream, whereby nutrients generated by said lysing step support cellular respiration in said stream after reintroduction.

32. The method of claim 31, wherein said steps of lysing and reintroducing cause a reduction in cell population present in said stream greater than the increase in cell population attributable to the generation of nutrients attributable to said lysing.

33. The method of claim 31, wherein said step of lysing is a two step process including introducing said portion into a first stage of said mill, processing said portion in said first stage, said portion exiting said first stage after being processed therein and entering a second stage of said mill, and processing said portion in said second stage prior to said step of reintroducing said portion to said stream.

34. The method of claim 31, wherein said steps of lysing and reintroducing favor the reproduction of selected microorganisms present in said stream, whereby the percentage of said favored microorganisms relative to other microorganisms present in said stream exceeds that percentage prevalent in an unprocessed stream.

35. The method of claim 31, wherein said step of lysing creates an elevation in temperature and pressure of said portion in said mill leading to an increased rate of oxidation of said portion and oxidation of cytoplasm of lysed cells present within said portion.

36. The method of claim 35, wherein said elevation in temperature and pressure results in the conversion of odorous hydrogen sulfide to less odorous sulfates.

37. The method of claim 31, further including the step of varying the duty cycle of said mill to meet the varying quantity of said solids in said stream, with larger amounts of solids giving rise to increased duty cycles and smaller amounts of solids giving rise to decreased duty cycles.

38. The method of claim 31, wherein said portion of said stream is subjected to clarification in a primary clarifier, aeration in an aeration basin and clarification in a secondary clarifier prior to being processed in said mill and wherein said portion is returned to said aeration basin after being processed in said mill.

39. The method of claim 31, wherein said steps of lysing and reintroducing establish an endogenous phase of respiration of microorganisms present in said portion.

40. A method for the production of extracts, comprising the steps of:

preparing a fluid slurry of a raw material containing a material to be extracted therefrom;

directing at least a portion of said slurry to a dispersion mill of the type having an annular rotor with a first series of slots therein, each slot of said first series of slots having a first slot wall and a second slot wall, said first slot wall and said second slot wall of a plurality of said first series of slots converging toward one another in a radially outward direction, and an annular stator with a second series of slots therein, each slot of said second series of slots intermittently aligning with each slot of said first series of slots as said rotor is rotated relative to said stator to thereby discharge said slurry from said rotor into said stator when said rotor is rotated;

lysing solids in said portion in said dispersion mill to thereby yield finely comminuted solids within said slurry; and

extracting said material to be extracted from said slurry of finely comminuted solids.

41. A method for the production of extracts, comprising the steps of:

preparing a fluid slurry of a raw material containing a material to be extracted therefrom;

directing at least a portion of said slurry to an apparatus having a housing accommodating said portion said housing having an input opening for admitting said portion to be processed and an output opening for discharging processed slurry, a two-stage mill disposed within said housing, said mill including a rotable drive shaft extending through said housing, a first stage with a first annular rotor, which is mounted on said drive shaft and which has a first series of slots therein, and a first annular stator, which has a second series of slots therein and which cooperates with said first rotor to process said slurry, and a second stage having a second annular rotor, which is mounted on said drive shaft and which has a third series of slots therein, and a second annular stator, which has a fourth series of slots therein and which cooperates with said second rotor to process said slurry, each slot of said first series of slot intermittently aligning with each slot of said second series of slots to discharge said slurry from said first rotor into said first stator, and each slot of said third series of slots intermittently aligning with each slot of said fourth series of slots to discharge said slurry from said second rotor into said second stator; and

controlling means disposed within said housing for controlling the flow of said slurry such that it passes through said first stage and then through said second stage.

lysing solids in said portion in said apparatus to thereby yield finely comminuted solids within said slurry; and

extracting said material to be extracted from said slurry of finely comminuted solids.

42. The method of claim 41, wherein said solids include cells and said material to be extracted is cellular matter.

43. A method for the production of extracts, comprising the steps of:

preparing a fluid slurry of a raw material containing a material to be extracted therefrom;

directing at least a portion of said slurry to a dispersion mill of the type having an annular rotor having a first series of slots therein, each slot of said first series of slots having an inner slot opening with an associated area and an outer slot opening with an associated area, the cumulative area of said inner slot openings exceeding the cumulative area of said outer slot openings, and an annular stator with a second series of slots therein, each slot of said second series of slots intermittently aligning with each slot of said first series of slots as said rotor rotates relative to said stator to thereby discharge said slurry from said rotor into said stator when said rotor is rotated;

lysing solids in said portion in said dispersion mill to thereby yield finely comminuted solids within said slurry; and

extracting said material to be extracted from said slurry of finely comminuted solids.