Acoustic viscometer and method of determining kinematic viscosity and intrinsic viscosity by propagation of shear waves

• US 6,439,034 B1
• Filed: 10/30/2000
• Issued: 08/27/2002
• Est. Priority Date: 10/30/2000
• Status: Expired due to Fees

• Current Assignee: Conagra Grocery Products Company LLC (Conagra Brands, Inc.)
• Original Assignee: Conagra Grocery Products Company LLC (Conagra Brands, Inc.)
• Inventors: Sacher, Robert F., Fleck, Charles, Farone, William A.
• Primary Examiner(s): Williams, Hezron
• Assistant Examiner(s): WIGGINS, JOHN DAVID
• Application Number:
  US09/699,949
• Time in Patent Office: 666 Days
• Field of Search: 73/542.4, 73/542.7, 736/48, 735/92, 73/544.1
• US Class Current: 73/54.24
• CPC Class Codes: G01F 1/667 Arrangements of transducers for ultrasonic flowmeters; Circuits for operating ultrasonic flowmeters
• CPC Class Codes: G01N 11/16 by measuring damping effect upon oscillatory body
• CPC Class Codes: G01N 2291/02836 Flow rate, liquid level
• CPC Class Codes: G01N 9/002 using variation of the resonant frequency of an element vibrating in contact with the material submitted to analysis G01N9/34 takes precedence
• CPC Class Codes: G01N 9/32 by using flow properties of fluids, e.g. flow through tubes or apertures

Abstract

An acoustic viscometer and method for determining both the kinematic viscosity and the intrinsic viscosity of a liquid which includes an acoustic wave generator, a transmitting piezoelectric transducer, a receiving piezoelectric transducer, and a phase-shift detector. The transmitting piezoelectric transducer is positioned so as to be in contact with the liquid and is operably connected to the acoustic wave generator. The transmitting piezoelectric transducer propagates a longitudinal wave of known frequency through the liquid. The receiving piezoelectric transducer is spaced apart from the transmitting piezoelectric transducer and detects the longitudinal wave and a corresponding shear wave propagated through the liquid. The phase-shift detector is operably connected to both the transmitting and receiving piezoelectric transducers and measures the difference in phase between the longitudinal wave propagated by the transmitting piezoelectric transducer and the longitudinal and shear wave detected by the receiving piezoelectric transducer. The difference in phase is used to determine the velocity of the shear wave, and the kinematic and intrinsic viscosities of the liquid in terms of liquid density.

Claims

1. An acoustic viscometer for determining both the kinematic viscosity and the intrinsic viscosity of a liquid comprising:

an acoustic wave generator;

a transmitting piezoelectric transducer operably connected to the acoustic wave generator and positioned so as to be in contact with the liquid so as to propagate a longitudinal wave of known frequency through the liquid;

a receiving piezoelectric transducer, spaced apart from the transmitting piezoelectric transducer and in contact with liquid, so as to detect the longitudinal, wave and a corresponding shear wave propagated through the liquid in terms of liquid density; and

a phase-shift detector operably connected to the transmitting piezoelectric transducer and the receiving piezoelectric transducer to measure a difference in phase between the longitudinal wave propagated by the transmitting piezoelectric transducer and the longitudinal and shear wave detected by the receiving piezoelectric transducer, the difference in phase used to determine the velocity of the shear wave, and the kinematic viscosity and the intrinsic viscosity of the liquid in terms of liquid density.

2. The acoustic viscometer of claim 1 wherein the transmitting piezoelectric transducer is capable of propagating the shear wave in the liquid over a distance of at least about one inch.

3. The acoustic viscometer of claim 1 wherein the transmitting piezoelectric transducer is driven by a voltage of at least about ninety volts.

4. The acoustic viscometer of claim 1 wherein the transmitting piezoelectric transducer is driven by a voltage of between about ninety and about three hundred volts.

5. The acoustic viscometer of claim 1 wherein the difference in phase between the longitudinal wave propagated by the transmitting piezoelectric transducer and the longitudinal and shear wave detected by the receiving piezoelectric transducer is determined without regard to the amplitudes of the longitudinal wave and the shear wave.

6. The acoustic viscometer of claim 1 wherein at least one of the transmitting piezoelectric transducer and the receiving piezoelectric transducer have a coating.

7. The acoustic viscometer of claim 6 wherein the coating has a thickness of less than 0.1 millimeter.

8. The acoustic viscometer of claim 1 wherein the transmitting piezoelectric transducer propagates the shear wave with a frequency between about 20 kHz and about 100 kHz.

9. The acoustic viscometer of claim 1 wherein the transmitting piezoelectric transducer propagates the shear wave with a frequency between about 36 kHz and about 44 kHz.

10. The acoustic viscometer of claim 1 further comprising a temperature sensor for measuring the temperature of the liquid.

11. The acoustic viscometer of claim 1 wherein the acoustic wave generator is a pulse generator.

12. The acoustic viscometer of claim 1 wherein the acoustic wave generator is a crystal oscillator.

13. The acoustic viscometer of claim 1 wherein the acoustic viscometer is battery powered.

14. The acoustic viscometer of claim 1 further comprising:

a phase-to-voltage convector operably connected to the phase-shift detector to convert the difference in phase between the longitudinal wave propagated by the transmitting piezoelectric transducer and the longitudinal and shear wave detected by the receiving piezoelectric transducer to a voltage; and

an output device operably connected to the phase-to-voltage convector for displaying a value corresponding to the voltage.

15. A method for determining both the kinematic viscosity and the intrinsic viscosity of a liquid comprising:

placing a transmitting piezoelectric transducer and a receiving piezoelectric transducer in contact with the liquid;

propagating a longitudinal wave and a corresponding shear wave in the liquid by vibrating the transmitting piezoelectric transducer;

detecting the longitudinal and shear wave With the receiving piezoelectric transducer;

determining a difference in phase between the longitudinal wave propagated by the transmitting piezoelectric transducer and the longitudinal and shear wave detected by the receiving piezoelectric transducer; and

determining a velocity of the shear wave, and the kinematic viscosity and the intrinsic viscosity of the liquid in terms of liquid density.

16. The method of claim 15 wherein the transmitting piezoelectric transmitter and the receiving piezoelectric transducer are at least about one inch apart.

17. The method of claim 15 wherein the difference in phase between the longitudinal wave propagated by the transmitting piezoelectric transducer and the longitudinal and shear wave detected by the receiving piezoelectric transducer is determined without regard to the amplitudes of the longitudinal wave and shear wave.

18. The method of claim 15 wherein the transmitting piezoelectric transducer propagates the shear wave with a frequency between about 20 kHz and about 100 kHz.

19. The method of claim 15 wherein the transmitting piezoelectric transducer propagates the shear wave with a frequency between about 36 kHz and about 44 kHz.

20. The method of claim 15 further comprising determining the temperature of the liquid.

21. The method of claim 15 wherein the liquid flows past the transmitting piezoelectric transducer and the receiving piezoelectric transducer.

22. The method of claim 15 wherein the liquid is present within a piece of fruit.

23. The method of claim 15 further comprising:

converting the difference in phase between the longitudinal wave propagated by the transmitting piezoelectric transducer and the longitudinal and shear wave detected by the receiving piezoelectric transducer to a voltage; and

transmitting the voltage to an output device for displaying a value corresponding to the voltage.