Apparatus and method for generating droplets

• US 6,446,878 B1
• Filed: 03/01/2000
• Issued: 09/10/2002
• Est. Priority Date: 03/01/1999
• Status: Expired due to Fees

• Current Assignee: Rahim Jivraj, Sanjeev Chandra
• Original Assignee: Rahim Jivraj, Sanjeev Chandra
• Inventors: Jivraj, Rahim, Chandra, Sanjeev
• Primary Examiner(s): Ganey, Steven J.
• Application Number:
  US09/516,183
• Time in Patent Office: 923 Days
• Field of Search: 239/13, 239/83, 239/70, 239/75, 239/1, 239/119, 239/135, 239/548, 239/347, 239/373, 239/566, 239/690, 239/348, 239/533.15, 239/533.1, 239/99, 239/101, 239/128, 239/104, 239/120, 239/126, 738/648.1, 738/648.3, 738/648.4, 738/630.1, 222/325, 222/394, 222/397, 222/399, 222/401, 222/420
• US Class Current: 239/1
• CPC Class Codes: B05B 12/02 for controlling time, or sequence, of delivery
• CPC Class Codes: B05B 12/06 for effecting pulsating flow nozzles, spray head or outlet with means for generating a discharge of pulsating nature B05B1/08
• CPC Class Codes: B05B 9/002 incorporating means for heating or cooling, e.g. the material to be sprayed
• CPC Class Codes: B05B 9/04 with pressurised or compressible container aerosol containers B65D83/14; with pump
• CPC Class Codes: B05C 11/1034 specially designed for conducting intermittent application of small quantities, e.g. drops, of coating material B05C5/0225, B05C11/1026 take precedence
• CPC Class Codes: B22F 2009/0804 Dispersion in or on liquid, other than with sieves
• CPC Class Codes: B22F 2009/0816 by casting with pressure or pulsating pressure on the metal bath
• CPC Class Codes: B22F 2009/0864 by oil, other non-aqueous fluid or fluid-bed cooling
• CPC Class Codes: B22F 2998/00 Supplementary information concerning processes or compositions relating to powder metallurgy
• CPC Class Codes: B22F 3/115 by spraying molten metal, i.e. spray sintering, spray casting
• CPC Class Codes: B22F 9/08 by casting, e.g. through sieves or in water, by atomising or spraying using electric discharge B22F9/14

Abstract

An apparatus and method for the production of small, uniform sized droplets. The apparatus is a droplet generator including a housing defining a chamber for holding a material to be ejected therefrom, an inlet and a droplet outlet communicating with the chamber. The housing is coupled to a pressurizing system connected to the inlet for applying pressure pulses to the chamber. The housing includes a vent in communication with the chamber for relieving pressure in the chamber. The vent has an effective size so that during application of the pressure pulse the chamber is pressurized to a pressure effective to eject a droplet of the material therefrom and thereafter the chamber is vented through the vent at a rate sufficient to prevent further discharge of droplets. The droplet generator produces molten metal or alloy droplets and is particularly suitable for generating single droplets on demand in manufacturing techniques using droplet deposition. It is also useful for production of spherical microspheres and uniform sized powders, and dispensing of precise quantities of materials such as adhesives and pharmaceuticals.

Claims

1. An apparatus for generating and ejecting droplets therefrom, comprising:

a) a housing enclosing a chamber for holding a material to be ejected therefrom, a gas inlet and an outlet passageway communicating with said chamber;

b) pressurizing means connected to said gas inlet for pressure pulsing said chamber with a gas for forcefully ejecting at least one droplet through said outlet passageway; and

c) pressure relief means for relieving pressure in said chamber sufficiently rapidly to avoid ejection of further droplets from said chamber to provide control of a number of droplets ejected from said chamber through said outlet passageway.

2. The apparatus according to claim 1 wherein said pressure relief means includes a vent in communication with said chamber for relieving pressure in the chamber, the vent having an effective size so that during application of a gas pulse the chamber is pressurized to a pressure sufficient to eject a droplet of said material therefrom and thereafter the chamber is vented through the vent at a rate sufficient to prevent further discharge of droplets.

3. The apparatus according to claim 2 wherein said pressurizing means includes a timing circuit for controlling the length of time said gas pulses are applied to said chamber.

4. The apparatus according to claim 3 wherein said pressurizing means includes a gas handling system for applying gas pulses to said chamber.

5. The apparatus according to claim 2 wherein said housing includes a heater for heating a material in said chamber.

6. The apparatus according to claim 5 including a fluid bath for receiving droplets discharged from said outlet passageway for rapidly cooling said droplets.

7. The apparatus according to claim 6 wherein said fluid bath includes a container for holding said fluid, said housing being partially immersed in said container so droplets ejected from said outlet passageway contact said fluid, said fluid having an effective viscosity and density to solidify molten droplets ejected from said outlet passageway as said droplets fall a preselected distance in said fluid.

8. The apparatus according to claim 7 wherein said fluid is oil.

9. The apparatus according to claim 2 wherein said outlet passageway includes a sapphire nozzle, said sapphire nozzle having a passageway diameter in a preselected range.

10. The apparatus according to claim 2 wherein said outlet passageway is a first outlet passageway, said housing including a plurality of outlet passageways each in communication with said chamber.

11. The apparatus according to claim 2 wherein said outlet passageway has a diameter to produce droplets having a preselected diameter.

12. The apparatus according to claim 1 wherein said pressure relief means includes a vent in flow communication with said chamber and a solenoid valve for opening and closing said vent.

13. The apparatus according to claim 1 wherein said pressure relief means includes a pressure relief valve in flow communication with said chamber.

14. A method of producing droplets, comprising:

pressure pulsing a chamber using a gas, the chamber holding a material to be ejected as droplets, the chamber being pressurized for a length of time sufficient to build up a pressure sufficient to forcefully eject at least one droplet of said material through an outlet and thereafter relieving the pressure sufficiently rapidly to avoid ejection of further droplets from the chamber.

15. The method according to claim 14 wherein said pressure is relieved using a vent in communication with said chamber, and the vent being selected to have a size small enough such that when the chamber is pressurized by applying a pressure pulse using said gas for an effective period of time at least one droplet of said material is ejected through said outlet and large enough that after ejection of the droplet the pressure drops sufficiently rapid to avoid ejection of further droplets from the chamber.

16. The method according to claim 15 wherein said pressure pulse is applied using an inert gas supplied from a compressed gas source using a timing circuit for controlling the length of time said pressure pulse is applied.

17. The method according to claim 15 wherein the material being ejected is a molten metal.

18. The method according to claim 17 wherein said droplet is ejected into a fluid that is inert towards the material being ejected for rapidly cooling and solidifying said droplet.

19. The method according to claim 18 wherein said fluid has an effective viscosity and density to solidify molten droplets ejected from said outlet passageway as said droplets fall through a preselected distance in said fluid.

20. The method according to claim 15 wherein said outlet passageway has a diameter selected to produce droplets with a preselected diameter.

21. The method according to claim 14 including heating said material contained within said chamber.

22. The method according to claim 14 wherein said material to be ejected is a powder.

23. The method according to claim 14 wherein said outlet passageway has a diameter selected to produce droplets with a preselected diameter.