Translucent alumina sintered body and a process for producing the same

• US 6,482,761 B1
• Filed: 08/28/2000
• Issued: 11/19/2002
• Est. Priority Date: 08/30/1999
• Status: Expired due to Fees

• Current Assignee: Sumitomo Chemical Company Limited
• Original Assignee: Sumitomo Chemical Company Limited
• Inventors: Watanabe, Hisashi, Uchida, Yoshio
• Primary Examiner(s): Koslow, C. Melissa
• Application Number:
  US09/648,812
• Time in Patent Office: 813 Days
• Field of Search: 501/153, 501/127
• US Class Current: 501/153
• CPC Class Codes: C04B 35/115 Translucent or transparent products
• CPC Class Codes: H01J 61/302 characterised by the material of the vessel

Abstract

A translucent alumina sintered body wherein the total content of an alkali metal element and an alkaline earth metal element is 50 ppm or less, and the linear transmittance of a light having a wavelength of 600 nm is 40% or more at a thickness of the sintered body of 0.85 mm.

Claims

1. A translucent alumina sintered body wherein the total content of an alkali metal element and an alkaline earth metal element is 50 ppm or less, and the in line transmittance of a light having a wavelength of 600 nm is 40% or more at a thickness of the sintered body of 0.85 mm.

2. The translucent alumina sintered body according to claim 1 wherein the average grain size the alumina sintered body is 5 to 50 μ

m, and the maximum grain size (particle diameter of the maximum structure in the crystal structure) is 1.5-fold or more of the average grain size.

3. A method for producing a translucent alumina sintered body according to claim 1, wherein the sintered body is obtained by

forming a mixed powder prepared by adding a sintering agent to an α

alumina powder which comprises a polyhedral primary particle having substantially no fractured surface, has a BET specific surface area of 1 to 10 m²/g and has a purity of 99.99% or more, and

sintering the green body at a temperature of from 1700 to 1900°

C. under reducing atmosphere from atmospheric pressure to vacuum.

4. The method for producing a translucent alumina sintered body according to claim 3, wherein the sintering agent is a magnesium compound and the addition amount thereof is 10-100 ppm in terms of the oxide based on the total amount of alumina.

5. A method for producing a translucent alumina sintered body according to claim 1, wherein the sintered body is obtained by

forming a mixed powder prepared by adding a magnesium compound in an amount of 10 to 100 ppm in terms of the oxide based on the total amount of alumina, or a magnesium compound in an amount of 10 to 100 ppm in terms of the oxide based on the total amount of alumina and one or more compounds selected from the group consisting of compounds of group IIIA elements and group IVA elements of the periodic table in an amount of 1 to 100 wt % in terms of the oxide based on the total amount of the magnesium compound, to an α

alumina powder which comprises a polyhedral primary particle having substantially no fractured surface, has a BET specific surface area of 1 to 10 m²/g and has a purity of 99.99% or more, and

sintering the green body at a temperature of from 1700 to 1900°

C. under reducing atmosphere from atmospheric pressure to vacuum.

6. The method for producing a translucent alumina sintered body according to claim 3 comprising the steps of (1) mixing a mixed powder according to claim 3 with organic binder, plasticizer, dispersing agent, lubricant, and water or an organic solvent to prepare a slurry, (2) forming said slurry, and (3) prefiring said green body in atmosphere at a temperature of from 500 to 1500°

C., and then sintering the prefired green body under reducing atmosphere of from atmospheric pressure to vacuum at a temperature of from 1700 to 1900°

C.

7. The method for producing a translucent alumina sintered body according to claim 6, wherein the slurry is a slurry obtained by dispersing an alumina powder only by mechanical stirring, or a slurry obtained by dispersing an alumina powder by mechanical stirring and ultrasonic dispersing.

8. A lamp constitution member comprising a translucent alumina sintered body according to claim 1.

9. A semiconductor producing apparatus member comprising a translucent alumina sintered body according to claim 1.

10. A bioceramics member comprising a translucent alumina sintered body according to claim 1.