Method and device for detecting and differentiating between contaminations and accepts as well as between different colors in solid particles

• US 6,509,537 B1
• Filed: 01/11/2001
• Issued: 01/21/2003
• Est. Priority Date: 05/14/1999
• Status: Active Grant

• Current Assignee: Gunther Krieg
• Original Assignee: Gunther Krieg
• Inventors: Fey, Dirk, Krieg, Gunther, Dausch, Manfred, Bohleber, Jürgen
• Primary Examiner(s): Walsh, Donald P.
• Assistant Examiner(s): Beauchaine, Mark J.
• Application Number:
  US09/743,517
• Time in Patent Office: 740 Days
• Field of Search: 209/579, 209/585, 209/587, 356/73, 356/337, 356/340, 356/342, 356/343
• US Class Current: 209/579
• CPC Class Codes: B07C 5/3425 of granular material, e.g. ore particles, grain investigation moving fluids or granular solids using optical means G01N21/85
• CPC Class Codes: G01N 21/274 Calibration, base line adjustment, drift correction
• CPC Class Codes: G01N 21/85 Investigating moving fluids or granular solids

Abstract

The invention concerns a method and a device for detection of and differentiation between base materials, colors and contamination in granulate-like or tablet-shaped substances, characterized in that the substances are illuminated in a linear manner with a laser beam, the optical radiation re-emitted by the substances is spectroscopically analyzed, and the substances are classified and sorted into different groups.

Claims

1. A method of detecting and differentiating between base materials, colors and contamination in granulate-like or tablet-shaped substances, the method comprising the steps of:

a) linearly irradiating and exciting the substances with a laser;

b) detecting re-emitted secondary radiation from the substances;

c) spectroscopically analyzing said secondary radiation; and

d) classifying and sorting the substances following step c),

wherein step b) comprises detecting said re-emitted secondary radiation as a spectrum using a multi-anode photomultiplier tube, and step c) comprises effecting substance analysis, color determination and contaminant detection via signal preparation, programmed logic and mathematical algorithms including calibration vectors.

2. The method of claim 1, wherein said irradiating of the substances in step a) and said detecting of said re-emitted radiation in step b) are carried out via an optical arrangement comprising a reflecting polygonal wheel and a concave toroidal mirror.

3. The method of claim 2, wherein said concave toroidal mirror comprises several individual segments.

4. A method of detecting and differentiating between base materials, colors and contamination in granulate-like or tablet-shaped substances, the method comprising the steps of:

a) linearly irradiating and exciting the substances with a laser;

b) detecting re-emitted secondary radiation from the substances;

c) spectroscopically analyzing said secondary radiation; and

d) classifying and sorting the substances following step c),

wherein step b) comprises detecting said re-emitted secondary radiation as a spectrum using a multi-anode photomultiplier tube, and step c) comprises effecting substance analysis, color determination and contaminant detection by preparing signals with analog multi-channel signal processing according to mathematical models, summing up of the contents of all signal channels, and classifying a summed signal.

5. The method of claim 4, wherein said irradiating of the substances in step a) and said detecting of said re-emitted radiation in step b) are carried out via an optical arrangement comprising a reflecting polygonal wheel and a concave toroidal mirror.

6. The method of claim 5, wherein said concave toroidal mirror comprises several individual segments.

7. A method of detecting and differentiating between base materials, colors and contamination in granulate-like or tablet-shaped substances, the method comprising the steps of:

a) linearly irradiating and exciting the substances with a laser,

b) detecting re-emitted secondary radiation from the substances;

c) spectroscopically analyzing said secondary radiation; and

d) classifying and sorting the substances following step c),

wherein step b) comprises detecting said re-emitted secondary radiation as a spectrum using a multi-anode photomultiplier tube, and step c) comprises effecting substance analysis, color determination and contaminant detection via a processor having access to reference spectra contained in a data memory.

8. The method of claim 7, wherein said irradiating of the substances in step a) and said detecting of said re-emitted radiation in step b) are carried out via an optical arrangement comprising a reflecting polygonal wheel and a concave toroidal mirror.

9. The method of claim 8, wherein said concave toroidal mirror comprises several individual segments.

10. A method of detecting and differentiating between base materials, colors and contamination in granulate-like or tablet-shaped substances, the method comprising the steps of:

a) linearly irradiating and exciting the substances with a laser,

b) detecting re-emitted secondary radiation from the substances;

c) spectroscopically analyzing said secondary radiation; and

d) classifying and sorting the substances following step c),

wherein step b) comprises detecting said re-emitted secondary radiation as a spectrum using a multi-anode photomultiplier tube, and step c) comprises effecting substance analysis, color determination and contaminant detection via a processor and mathematical classification models.

11. The method of claim 10, wherein said irradiating of the substances in step a) and said detecting of said re-emitted radiation in step b) are carried out via an optical arrangement comprising a reflecting polygonal wheel and a concave toroidal mirror.

12. The method of claim 11, wherein said concave toroidal mirror comprises several individual segments.

13. A device for the examination of substance properties of a measuring material, a granulate, and tablet-like substances, the device comprising:

a laser beam;

an optical adjustment means for deflecting said beam and for simultaneously guiding said beam over the measuring material;

a device for spectral decomposition of secondary radiation re-emitted by the measuring material;

a sensor system for recording said secondary radiation, including a multi-anode photomultiplier for detecting said re-emitted secondary radiation;

means for evaluation of received secondary radiation, including signal preparation means, programmed logic and mathematical algorithms including calibration vectors for effecting substance analysis, color determination and contaminant detection.

14. The device of claim 13, wherein said optical adjustment means comprise a reflecting polygonal wheel and a concave toroidal mirror for irradiating the measuring material and for detecting said re-emitted secondary radiation.

15. The device of claim 14, wherein said concave toroidal mirror comprises several individual segments.

16. A device for the examination of substance properties of a measuring material, a granulate, and tablet-like substances, the device comprising:

a laser beam;

an optical adjustment means for deflecting said beam and for simultaneously guiding said beam over the measuring material;

a device for spectral decomposition of secondary radiation re-emitted by the measuring material;

a sensor system for recording said secondary radiation, including a multi-anode photomultiplier for detecting said re-emitted secondary radiation;

means for evaluation of received secondary radiation, including signal preparation means with analog multi-channel signal processing according to mathematical models with summing up of a contents of all signal channels and classification of a summed signal to effect substance analysis, color determination and contaminant detection.

17. The device of claim 16, wherein said optical adjustment means comprise a reflecting polygonal wheel and a concave toroidal mirror for irradiating tile substance and for detecting said re-emitted secondary radiation.

18. The device of claim 17, wherein said concave toroidal mirror comprises several individual segments.

19. A device for the examination of substance properties of a measuring material, a granulate, and tablet-like substances, the device comprising:

a laser beam;

an optical adjustment means for deflecting said beam and for simultaneously guiding said beam over the measuring material;

a device for spectral decomposition of secondary radiation re-emitted by the measuring material;

a sensor system for recording said secondary radiation, including a multi-anode photomultiplier for detecting said re-emitted secondary radiation;

means for evaluation of received secondary radiation, including a processor having access to reference spectra contained in a data memory for effecting substance analysis, color determination and contaminant detection.

20. The device of claim 19, wherein said optical adjustment means comprises a reflecting polygonal wheel and a concave toroidal mirror for irradiating the substance and for detecting said re-emitted secondary radiation.

21. The device of claim 20, wherein said concave toroidal mirror comprises several individual segments.

22. A device for the examination of substance properties of a measuring material, a granulate, and tablet-like substances, the device comprising:

a laser beam;

an optical adjustment means for deflecting said beam and for simultaneously guiding said beam over the measuring material;

a device for spectral decomposition of secondary radiation re-emitted by the measuring material;

a sensor system for recording said secondary radiation, including a multi-anode photomultiplier for detecting said re-emitted secondary radiation;

means for evaluation of received secondary radiation, including a processor and mathematical classification models for effecting substance analysis, color detection and contaminant detection.

23. The device of claim 22, wherein said optical adjustment means comprise a reflecting polygonal wheel and a concave toroidal mirror for irradiating the measuring material and for detecting said re-emitted secondary radiation.

24. The device of claim 23, wherein said concave toroidal mirror comprises several individual segments.