Cationically charged coating on hydrophobic polymer fibers with poly (vinyl alcohol) assist
First Claim
1. A method of preparing a fibrous filter, the method comprising:
- providing a fibrous filter comprised of hydrophobic polymer fibers;
treating the fibrous filter with an aqueous solution of a functionalized cationic polymer crosslinkable by heat under conditions sufficient to substantially coat the fibers with the functionalized cationic polymer, wherein the solution comprises the functionalized cationic polymer, a poly(vinyl alcohol), a polar solvent for the poly(vinyl alcohol), and water; and
treating the resulting coated fibrous filter with heat at a temperature and for a time sufficient to crosslink the functionalized cationic polymer present on the hydrophobic polymer fibers.
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Abstract
A hydrophobic polymer fiber having a cationically charged coating thereon, in which the coating includes a functionalized cationic polymer, such as an epichlorohydrin-functionalized polyamine or an epichlorohydrin-functionalized polyamido-amine, which has been crosslinked by heat. The present invention also provides a fibrous filter which includes hydrophobic polymer fibers having the foregoing cationically charged coating thereon. The present invention further provides a method of preparing a fibrous filter. The method involves providing a fibrous filter comprised of hydrophobic polymer fibers; treating the fibrous filter with an aqueous solution of a functionalized cationic polymer crosslinkable by heat under conditions sufficient to substantially coat the fibers with the functionalized cationic polymer, wherein the solution includes the functionalized cationic polymer, a poly(vinyl alcohol), a polar solvent for the poly(vinyl alcohol), and water; and treating the resulting coated fibrous filter with heat at a temperature and for a time sufficient to crosslink the functionalized cationic polymer present on the hydrophobic polymer fibers. The present invention additionally provides a method of preparing a fibrous filter. The method includes providing a fibrous filter comprised of hydrophobic polymer fibers; passing a solution of a functionalized cationic polymer crosslinkable by heat through the fibrous filter under conditions sufficient to substantially coat the fibers with the functionalized cationic polymer, wherein the solution includes the functionalized cationic polymer, a poly(vinyl alcohol), and water; and treating the resulting coated fibrous filter with heat at a temperature and for a time sufficient to crosslink the functionalized cationic polymer present on the hydrophobic polymer fibers.
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Citations
12 Claims
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1. A method of preparing a fibrous filter, the method comprising:
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providing a fibrous filter comprised of hydrophobic polymer fibers;
treating the fibrous filter with an aqueous solution of a functionalized cationic polymer crosslinkable by heat under conditions sufficient to substantially coat the fibers with the functionalized cationic polymer, wherein the solution comprises the functionalized cationic polymer, a poly(vinyl alcohol), a polar solvent for the poly(vinyl alcohol), and water; and
treating the resulting coated fibrous filter with heat at a temperature and for a time sufficient to crosslink the functionalized cationic polymer present on the hydrophobic polymer fibers. - View Dependent Claims (2, 3, 4, 5, 6)
from about 0.1 to about 2 percent by weight of the functionalized cationic polymer;
from about 0.1 to about 4 percent by weight of the poly(vinyl alcohol); and
from about 10 to about 50 percent by weight of the polar solvent;
with the remainder of the solution being water.
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5. The method of claim 4, in which the polar solvent is isopropyl alcohol.
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6. The method of claim 5, in which the aqueous solution of a functionalized cationic polymer comprises:
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from about 0.2 to about 1 percent by weight of the functionalized cationic polymer;
from about 0.1 to about 2 percent by weight of the poly(vinyl alcohol); and
from about 15 to about 45 percent by weight of the isopropyl alcohol;
with the remainder of the solution being water.
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7. A method of preparing a fibrous filter, the method comprising:
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providing a fibrous filter comprised of hydrophobic polymer fibers;
passing a solution of a functionalized cationic polymer crosslinkable by heat through the fibrous filter under conditions sufficient to substantially coat the fibers with the functionalized cationic polymer, wherein the solution comprises the functionalized cationic polymer, a poly(vinyl alcohol), and water; and
treating the resulting coated fibrous filter with heat at a temperature and for a time sufficient to crosslink the functionalized cationic polymer present on the hydrophobic polymer fibers. - View Dependent Claims (8, 9, 10, 11, 12)
from about 0.1 to about 4 percent by weight of the functionalized cationic polymer; and
from about 0.1 to about 2 percent by weight of the poly(vinyl alcohol);
with the remainder of the solution being water.
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11. The method of claim 10, in which the polar solvent is isopropyl alcohol.
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12. The method of claim 11, in which the aqueous solution of a functionalized cationic polymer comprises:
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from about 0.2 to about 2 percent by weight of the functionalized cationic polymer; and
from about 0.1 to about 1 percent by weight of the poly(vinyl alcohol);
with the remainder of the solution being water.
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Specification