Vapor plug for cryogenic storage vessels

• US 6,539,726 B2
• Filed: 05/08/2001
• Issued: 04/01/2003
• Est. Priority Date: 05/08/2001
• Status: Expired due to Term

• Current Assignee: CryoPort Systems, Inc. (Cryoport, Inc.)
• Original Assignee: CryoPort Systems, Inc. (Cryoport, Inc.)
• Inventors: Ventura, Mark, Roberts, Funn, Giesy, R. Kevin
• Primary Examiner(s): CAPOSSELA, RONALD C
• Application Number:
  US09/851,407
• Publication Number:
  US 20020166326A1
• Time in Patent Office: 693 Days
• Field of Search: 62/481, 62/511, 206/0.6, 206/0.7, 220/560.1, 220/592.2, 220/367.1, 220/373
• US Class Current: 62/48.1
• CPC Class Codes: F17C 13/06 Closures, e.g. cap, breakable member for autoclaves B01J3/03; closures for large containers in general B65D B65D90/54; for pressure vessels in general F16J13/00
• CPC Class Codes: F17C 3/02 with provision for thermal insulation thermal insulation in general F16L59/00 ; refrigerators F25D; insulation specially adapted for cryogenic vessels F17C13/001; tank vehicles B60P3/22; railway tank wagons B61D5/00

Abstract

A thermal barrier for a Dewar vessel combines an insulative vapor plug and a vapor barrier. The plug is sized so as to define an open space between it and the neck portion of the Dewar vessel to allow venting of vaporous cryogen from the inner vessel of the Dewar vessel through a Dewar opening. The vapor barrier provides an interference between the plug and the neck portion that disrupts venting of vaporous cryogen but does not form an airtight seal that would block venting and cause unacceptable build-up of pressure within the inner vessel. Multiple vapor barriers, especially four or more, provide multiple interferences that create multiple chambers between the plug and the neck portion. Each interference disrupts migration of vaporous cryogen as an incremental increase (e.g., 2 psig or less) in vapor pressure of each chamber causes the chamber to breach and then another incremental increase in vapor pressure of the liquid cryogen in the vaporous state is required to breach each successive chamber. The thermal barrier can be inserted into the neck portion of a conventional Dewar vessel to increase its holding time.

Claims

1. A Dewar vessel having an outer casing and an inner vessel with each having openings at their tops connected together by a neck portion forming an evacuable space between the outer casing and the inner vessel and a Dewar opening into the inner vessel, the improvement comprising:

an insulative vapor plug held within the neck portion; and

a vapor barrier that provides an interference between the plug and the neck portion;

wherein the plug and the neck portion are sized so as to define an open space between them that allows a liquid cryogen in a vaporous state to vent from the inner vessel through the Dewar opening; and

wherein the interference disrupts migration of the liquid cryogen in the vaporous state out of the Dewar opening through the open space but does not form an air tight seal between the plug and the neck portion.

2. A Dewar vessel as recited in claim 1, wherein the vapor barrier is comprised of a plurality of vapor barriers that provide a plurality of interferences between the plug and the neck portion and each of the plurality of interferences disrupts migration of the liquid cryogen in the vaporous state out of the Dewar opening through the open space and the plurality of interferences does not form the air tight seal.

3. A Dewar vessel as recited in claim 2, wherein the plurality of interferences define a plurality of chambers each of which disrupts migration of the liquid cryogen in the vaporous state out of the Dewar opening through the open space.

4. A Dewar vessel as recited in claim 3, wherein the plurality of chambers are sequentially breached as an incremental increase in vapor pressure of the liquid cryogen in the vaporous state in each given chamber causes the given chamber to breach and then another incremental increase in vapor pressure of the liquid cryogen in the vaporous state is required to breach another given chamber.

5. A Dewar vessel as recited in claim 1, wherein the vapor barrier is comprised of a cryogenically compatible material.

6. A Dewar vessel as recited in claim 5, wherein the cryogenically compatible material is a polymer film.

7. A Dewar vessel as recited in claim 5, further comprising:

a handle attached to the plug.

8. A Dewar vessel as recited in claim 7, wherein the handle extends through the plug and is affixed to a canister assembly.

9. A Dewar vessel as recited in claim 1, wherein the vapor barrier retains the liquid cryogen in the vaporous state within the vessel despite its orientation.

10. A Dewar vessel as recited in claim 1, wherein the vapor barrier provides a surface protrusion for the plug to inhibit the mean free path of dense, boiling vapors through the Dewar opening.

11. A Dewar vessel as recited in claim 10, wherein the plug occupies a majority of the open space within the neck portion.

12. A thermal barrier for a Dewar vessel having an outer casing and an inner vessel with each having openings at their tops connected together by a neck portion forming an evacuable space between the outer casing and the inner vessel and a Dewar opening into the inner vessel, comprising:

an insulative vapor plug sized so as to define an open space between it and the neck portion that allows a liquid cryogen in a vaporous state to vent from the inner vessel through the Dewar opening; and

a vapor barrier that provides an interference between the plug and the neck portion to disrupt migration of a liquid cryogen in a vaporous state out of the Dewar opening through the open space;

wherein the vapor barrier does not form an airtight seal between the plug and the neck portion.

13. A thermal barrier as recited in claim 12, wherein the vapor barrier is comprised of a plurality of vapor barriers that provide a plurality of interferences between the plug and the neck portion and each of the plurality of interferences disrupts migration of the liquid cryogen in the vaporous state out of the Dewar opening through the open space and the plurality of interferences does not form the air tight seal.

14. A thermal barrier as recited in claim 13, wherein the plurality of interferences define a plurality of chambers each of which disrupts migration of the liquid cryogen in the vaporous state out of the Dewar opening through the open space.

15. A thermal barrier as recited in claim 14, wherein the plurality of chambers are sequentially breached as an incremental increase in vapor pressure of the liquid cryogen in the vaporous state in each given chamber causes the given chamber to breach and then another incremental increase in vapor pressure of the liquid cryogen in the vaporous state is required to breach another given chamber.

16. A thermal barrier as recited in claim 15, wherein the plurality of vapor barriers is comprised of four or more vapor barriers.

17. A thermal barrier as recited in claim 15, wherein the plurality of vapor barriers is comprised of a cryogenically compatible material.

18. A thermal barrier as recited in claim 17, wherein the cryogenically compatible material is a polymer film.

19. A thermal barrier as recited in claim 17, wherein the plurality of vapor barriers are comprised of a plurality of protrusions extending outwardly from an outer surface of the plug.

20. A thermal barrier as recited in claim 19, wherein the plurality of protrusions is affixed to the plug by a plurality of laminations.

21. A thermal barrier as recited in claim 20, further comprising:

a handle attached to the plug that extends through the plug to a bottom point of the plug located beneath the plurality of laminations so that the plug can be removed from the vessel by an upward pulling force exerted on the bottom point.

22. A thermal barrier as recited in claim 21, wherein the handle is comprised of a webbing material.

23. A thermal barrier as recited in claim 21, wherein the handle extends through the plug and is affixed to a canister assembly.

24. A thermal barrier as recited in claim 23, wherein the handle is comprised of a webbing material.

25. A thermal barrier as recited in claim 19, wherein the vapor barrier retains the liquid cryogen in the vaporous state within the vessel despite its orientation.

26. A thermal barrier as recited in claim 25, wherein the vapor barrier inhibits the mean free path of dense, boiling vapors through the Dewar opening.

27. A thermal barrier as recited in claim 15, wherein the incremental increase in vapor pressure is less than 2 psig.

28. A method for extending the holding time of a Dewar vessel having an outer casing and an inner vessel with each having openings at their tops connected together by a neck portion forming an evacuable space between the outer casing and the inner vessel and a Dewar opening into the inner vessel, comprising the step of:

inserting an insulative vapor plug and a vapor barrier into the neck portion,

wherein the insulative vapor plug is sized so as to define an open space between it and the neck portion that allows a liquid cryogen in a vaporous state to vent from the inner vessel through the Dewar opening, and

wherein the vapor barrier provides an interference between the plug and the neck portion to disrupt migration of the liquid cryogen in the vaporous state out of the Dewar opening through the open space but the vapor barrier does not form an airtight seal between the plug and the neck portion.