Synthesis of 2H- and 13C-substituted dithanes
First Claim
Patent Images
1. A labeled compound, [2-13C]1,3dithiane wherein said 13C is directly bonded to exactly one or two deuterium atoms.
3 Assignments
0 Petitions
Accused Products
Abstract
The present invention is directed to labeled compounds, [2-13C]dithiane wherein the 13C atom is directly bonded to one or two deuterium atoms. The present invention is also directed to processes of preparing [2-13C]dithiane wherein the 13C atom is directly bonded to one or two deuterium atoms. The present invention is also directed to labeled compounds, e.g., [2H1−2, 13C]methanol (arylthio)-, acetates wherein the 13C atom is directly bonded to exactly one or two deuterium atoms.
-
Citations
4 Claims
- 1. A labeled compound, [2-13C]1,3dithiane wherein said 13C is directly bonded to exactly one or two deuterium atoms.
-
4. A process of preparing a labeled compound, [2-13C]1,3dithiane wherein said 13C atom is directly bonded to exactly one or two deuterium atoms comprising:
-
reacting [13C]methyl phenyl sulfoxide with sodium acylate to form an intermediate product; and
,reacting said intermediate product with HS—
(CH2)3—
SH to form said labeled compound, [2-13C]1,3dithiane wherein said 13C atom is directly bonded to exactly one or two deuterium atoms.
-
Specification