Pretreatment of chips before cooking

• US 6,544,384 B2
• Filed: 10/15/2001
• Issued: 04/08/2003
• Est. Priority Date: 06/02/1995
• Status: Expired due to Term

• Current Assignee: Andritz Incorporated
• Original Assignee: Andritz Incorporated
• Inventors: Stromberg, C. Bertil, Henricson, Kaj O., Vilpponen, Aki Hannu, Kettunen, Auvo Kimmo, Ramark, Hannu Olavi
• Primary Examiner(s): Nguyen, Dean T.
• Application Number:
  US09/975,984
• Publication Number:
  US 20020017370A1
• Time in Patent Office: 540 Days
• Field of Search: 162/17, 162/19, 162/37, 162/38, 162/39, 162/41, 162/42, 162/43
• US Class Current: 162/17
• CPC Class Codes: D21C 1/06 with alkaline reacting compounds

Abstract

The strength properties of chemical cellulose pulp (particularly kraft pulp) are improved by substituting a cold impregnation soak for conventional impregnation procedures. After steaming, wood chips are soaked in an alkaline liquid at a temperature of about 80-110° C. (preferably 80-100° C., or 90-105° C.) for between one-half-72 hours (typically about 2-4 hours) at a pressure of about 0-15 bar (preferably about 1-5 bar), to dissolve at least about 8% of the wood (preferably about 10-20%) and at least about 15% of the lignin. The alkaline liquid used preferably contains sulfide (e.g. black liquor, green liquor, white liquor, or mixtures thereof), but almost any alkaline liquid having an alkali concentration of about 1.0 mole of NaOH/liter or less (typically about 0.75 m/l or less) is suitable. The wood chips are then raised to a cooking temperature of about 145-180° C. and cooked to produce the cellulose chemical pulp. There may be an intermediate step, between soaking and raising the cooking temperature, of heating the wood chips to a temperature of about 110-150° C. (preferably about 120-140° C.) for about 10-90 minutes (preferably about 10-30 minutes). Alternatively or additionally the majority of the dissolved lignin (and/or other solids) may be removed before raising the wood chips to cooking temperature. The system for treating the wood chips need only include a low pressure soaking vessel (with an associated pump or other transfer device) in addition to conventional equipment.

Claims

1. A method of treating wood chips to produce chemical pulp, comprising the steps of sequentially continuously:

(a) steaming the chips to remove air from them and to heat them to a temperature of about 80-100°

C.;

(b) soaking the chips in an alkaline liquid having an alkaline concentration of about 0.75 moles per liter or less, at a temperature between about 80-100°

C., for a time of 30 minutes to 72 hours to produce dissolved organics;

(c) displacing out at least part of the dissolved organics after step (b) using white liquor, diluted white liquor, bleach plant effluent, or pulp washing effluent; and

(d) cooking the material from step (c) to a kappa number below 25.

2. A method as recited in claim 1, wherein the alkaline liquid in step (b) is black liquor, or a mixture of black liquor and white liquor.

3. A method as recited in claim 1, wherein step (c) is practiced so that the amount of dissolved organic solids during cooking in step (d) is 30-50% less as compared to chemical cooking processes in which step (c) is not practiced.