Apparatus and method for fluid analysis

• US 6,561,010 B2
• Filed: 02/01/2001
• Issued: 05/13/2003
• Est. Priority Date: 11/19/1999
• Status: Expired due to Term

• Current Assignee: Battelle Memorial Institute
• Original Assignee: Battelle Memorial Institute
• Inventors: Peters, Timothy J., Wilson, Bary W., Shepard, Chester L., Reeves, James H.
• Primary Examiner(s): Larkin, Daniel S.
• Assistant Examiner(s): Politzer, Jay L
• Application Number:
  US09/776,109
• Publication Number:
  US 20010013247A1
• Time in Patent Office: 831 Days
• Field of Search: 73/36, 73/540.1, 73/540.4, 73/540.7, 73/540.9, 73/542.3, 738/615.2, 250/343, 250/573, 356/414, 378/47, 702/108
• US Class Current: 73/54.04
• CPC Class Codes: G01N 11/08 by measuring pressure required to produce a known flow
• CPC Class Codes: G01N 23/223 by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence
• CPC Class Codes: G01N 33/2858 Metal particles
• CPC Class Codes: G01N 33/2888 Lubricating oil characteristics, e.g. deterioration lubricating properties G01N33/30

Abstract

The present invention is an apparatus and method for analyzing a fluid used in a machine or in an industrial process line. The apparatus has at least one meter placed proximate the machine or process line and in contact with the machine or process fluid for measuring at least one parameter related to the fluid. The at least one parameter is a standard laboratory analysis parameter. The at least one meter includes but is not limited to viscometer, element meter, optical meter, particulate meter, and combinations thereof.

Claims

1. A machine fluid analysis system comprising:

at least first and second sensors contacting a machine fluid under pressure of the machine;

a controller operable to collect data from the sensors for transmission to a remote location; and

a two-way wireless communicator coupled to the controller for receiving interrogation signals and for transmitting the collected data to the remote location;

wherein the first sensor includes an X-ray fluorescence meter including an X-ray source providing X-rays in the energy range of 5 KeV to 30 KeV and a thin walled tube of low element weight composition substantially transparent to source X-rays, the tube defining a fluid flow path past the X-ray source, and

wherein the second sensor includes at least one sensor selected from the group consisting of viscometer, optical meter, and particle counter.

2. The system of claim 1 wherein the second sensor includes a viscometer and wherein machine fluid contacting the X-ray fluorescence meter is at a substantially lower temperature than machine fluid contacting the viscometer.

3. The system of claim 2 wherein the X-ray fluorescence meter and the viscometer are coupled to a machine fluid line in parallel and a machine fluid cooler is upstream and in series with the X-ray fluorescence meter.

4. The system of claim 2 wherein the viscometer is an electromagnetic viscometer.

5. The system of claim 2 wherein the viscometer is a viscometer tube, a differential pressure transducer mounted on opposite ends of the viscometer tube, and a flowmeter in line with the viscometer tube.

6. The system of claim 1 wherein the controller includes at least one microprocessor, and

wherein the X-ray fluorescence meter includes an X-ray detector for receiving a produced X-ray fluorescence signal, a multi-channel analyzer for counting the number of X-ray photons in specific energy ranges, and a software for quantitative determination of the relative and absolute concentration of elements in the fluid.

7. The system of claim 6 wherein the flow fluid into the fluid flow path of the X-ray fluorescence meter is intermittent.

8. The system of claim 6 wherein the flow of fluid into the fluid flow path of the X-ray fluorescence meter is substantially continuous.

9. The system of claim 1 further comprising a two way communications bus between the controller and each of the plurality sensors.

10. The system of claim 1 wherein the second sensor includes an optical meter including an optical source operable to pass optical energy through the machine fluid and an optical detector operable to receive the optical energy passed through the machine fluid, and wherein there is no optical dispersive element between the optical energy source and the machine fluid or between the machine fluid and the detector.

11. The system of claim 10 wherein machine fluid is passed through a tubular cell in the optical meter.

12. The system of claim 10 wherein machine fluid is passed over a planar cell in the optical meter.

13. The system of claim 10 wherein optical energy source includes a non-coherent radiator and the optical meter includes a bandpass filter for filtering optical energy passed through the machine fluid.

14. The system of claim 10 wherein the optical energy source includes a coherent radiator.

15. The system of claim 3 further comprising an optical meter connected in series with the X-ray fluorescence meter.

16. The system of claim 15 wherein the optical meter and the X-ray fluorescence meter are contained in a thermally controlled compartment and the viscometer is outside the thermally controlled compartment.

17. The system of claim 16 further comprising a particle counter.

18. The system of claim 1 wherein the second sensor includes an optical particle counter operable to detect the presence of metallic or non-metallic particles.

38. The system of claim 2 wherein the viscometer has a dynamic range from about 10 cST to about 60 cST with an absolute certainty of no greater than ±

1%.

41. The system of claim 14 wherein the coherent radiator includes a quantum cascade laser.

19. A machine fluid analysis system comprising:

a plurality of different sensors contacting a fluid under pressure of a machine, wherein at least two of the plurality of sensors are selected from the group consisting of optical meter, viscometer, element meter, and particle counter;

a controller operable to collect data from the plurality of sensors for transmission to a remote location; and

a two-way wireless communicator coupled to the controller for receiving interrogation signals and for transmitting the collected data to the remote location; and

a fluid cooler operably coupled to at least one of the sensors;

wherein fluid is provided to different ones of the plurality of sensors at substantially different temperatures.

20. The system of claim 19 wherein the plurality of sensors include an element meter operable to determine the concentration of at least one specific element in the fluid.

21. The system of claim 20 wherein the specific element is selected from the group consisting of iron, lead, copper, silicon, chromium, aluminum, silver, and zinc.

22. The system of claim 20 wherein the element meter is an X-ray fluorescence meter including an X-ray source, a thin walled polymeric tube substantially transparent to source X-rays and providing a flow path past the X-ray source, and an X-ray detector for receiving an X-ray fluorescence signal from the fluid in the tube.

23. The system of claim 22 wherein the X-ray fluorescence meter includes an X-ray detector for receiving a produced X-ray fluorescence signal, a multi-channel analyzer for counting the number of X-ray photons in specific energy ranges, and software for quantitative determination of the relative and absolute concentration of elements in the fluid.

24. The system of claim 23 wherein each of the plurality of sensors are operable to determine a different machine fluid parameter selected from the group consisting of viscosity, pentane insolubles, soot, additive package, oxidation, or oil polymer breakdown products, nitration, sulfation, fuel dilution, water concentration, and concentration of a specific element.

25. The system of claim 22 wherein the X-ray fluorescence meter is provided in a thermally controlled compartment and the fluid cooler is provided in series with the X-ray fluorescence meter outside the thermally controlled compartment.

26. The system of claim 25 wherein a viscometer is outside the thermally controlled compartment and fluidly coupled in parallel with the X-ray fluorescence meter.

27. The system of claim 25 wherein the plurality of sensors includes an optical meter including an optical source operable to pass optical energy through the fluid and an optical detector operable to receive the optical energy passed through the fluid, and wherein there is no optical dispersive element between the optical energy source and the fluid or between the fluid and the detector.

28. The system of claim 27 wherein fluid is passed through a tubular cell in the optical meter.

29. The system of claim 27 wherein fluid is passed over a planar cell in the optical meter.

30. The system of claim 27 wherein optical energy source includes a non-coherent radiator and the optical meter includes a bandpass filter for filtering optical energy passed through the fluid.

31. The system of claim 27 wherein the optical energy source includes a coherent radiator.

39. The system of claim 26 wherein the viscometer has a dynamic range from about 10 cST to about 60 cST with an absolute certainty of no greater than ±

1%.

40. The system of claim 31 wherein the coherent radiator includes a quantum cascade laser.

32. A fluid analysis system comprising:

a plurality of different sensors contacting a fluid under pressure of a machine, wherein each of the plurality of sensors are operable to determine a different machine fluid parameter selected from the group consisting of viscosity, pentane insolubles, soot, additive package, oxidation or oil polymer breakdown products, nitration, sulfation, fuel dilution, water concentration, and concentration of a specific element;

a controller operable to collect data from the plurality of sensors for transmission to a remote location; and

p1 a two-way wireless communicator coupled to the controller for receiving interrogation signals and for transmitting the collected data to the remote location; and

p1 a thermally controlled compartment wherein at least one of the sensors is inside of and another is outside of the thermally controlled compartment whereby fluid is provided to different ones of the plurality of sensors at substantially different temperatures.

33. The system of claim 32 wherein a viscometer is outside the thermally controlled compartment.

34. The system of claim 32 wherein a non-dispersive optical meter is inside the thermally controlled compartment.

35. The system of claim 32 wherein an X-ray fluorescence meter is inside the thermally controlled compartment.

36. The system of claim 35 wherein the X-ray fluorescence meter includes an X-ray source, a thin walled polymeric tube substantially transparent to source X-rays and providing a flow path past the X-ray source, and an X-ray detector for receiving an X-ray fluorescence signal from the fluid inside the tube.

37. The system of claim 32 wherein the plurality of sensors are selected from the group consisting of viscometer, non-dispersive optical meter, element meter, and particle counter.