Method and apparatus for determining bulk material properties of elastomeric materials

• US 6,578,431 B2
• Filed: 04/03/2001
• Issued: 06/17/2003
• Est. Priority Date: 04/04/2000
• Status: Expired due to Fees

• Current Assignee: Virginia Polytechnic Institute and State University
• Original Assignee: Virginia Tech Intellectual Properties, Inc. (Virginia Polytechnic Institute and State University)
• Inventors: Lefebvre, Didier, Yu, Jang-Horng, Dillard, David A.
• Primary Examiner(s): NOORI, MAX H
• Application Number:
  US09/824,581
• Publication Number:
  US 20010049967A1
• Time in Patent Office: 805 Days
• Field of Search: 737/88, 737/90, 738/04, 738/07, 738/18, 738/19
• US Class Current: 73/819
• CPC Class Codes: G01N 11/16 by measuring damping effect upon oscillatory body
• CPC Class Codes: G01N 2203/0005 Repeated or cyclic
• CPC Class Codes: G01N 2203/0016 Tensile or compressive
• CPC Class Codes: G01N 2203/0051 Piezoelectric means
• CPC Class Codes: G01N 2203/0256 Triaxial, i.e. the forces being applied along three normal axes of the specimen

Abstract

A method and apparatus for determining bulk material constants such as Poisson'"'"'s ratio and the ratio of shear modulus to bulk modulus for elastomeric materials, including, but not limited to elastomers, rubbers, gels and sealants is disclosed. The bulk material properties are determined by measuring the pressure change of the elastomeric material when the elastomeric material is subjected to an applied pressure. The changes in the bulk material property due to temperature or a the addition of a diluent may also be determined. The apparatus includes a container that holds the elastomeric material. A pressure sensor is located in the container and is positioned to measure the pressure of the elastomeric material. The signal from the pressure sensor along with the applied pressure is used to determine a bulk material property such as Poisson'"'"'s ratio or the ratio of shear modulus to bulk modulus for the elastomeric material.

Claims

1. A method for measuring bulk material properties of an elastomeric material comprising the steps of:

applying pressure to an elastomeric material in a container which prevents radial expansion of said elastomeric material;

measuring the pressure of the elastomeric material from a signal generated by a pressure sensor in the container; and

determining a bulk material property selected from the group consisting of Poisson'"'"'s ratio and a ratio of shear modulus to bulk modulus for the elastomeric material using (A) the signal from the pressure sensor and (B) the magnitude of the applied pressure.

2. The method of claim 1 further comprising the steps of:

applying a temperature field to the elastomeric material; and

determining the coefficient of thermal expansion for the elastomeric material from the change in the bulk material property as a function of temperature.

4. The method of claim 1 further comprising the step of comparing the determined bulk material property of the elastomeric material with a known bulk material property.

3. A method for measuring bulk material properties of an elastomeric material comprising the steps of:

applying pressure to an elastomeric material in a container;

measuring the pressure of the elastomeric material from a signal generated by a pressure sensor in the container;

determining a bulk material property for the elastomeric material using the signal from the pressure sensor and the magnitude of the applied pressure;

adding a diluent to the elastomeric material; and

determining the coefficient of diluent expansion for the elastomeric material from the change in the bulk material property as a function of diluent addition.

5. An apparatus for determining a bulk material property of an elastomeric material comprising:

a container having a cavity adapted to hold an elastomeric material and which prevents radial expansion of said elastomeric material;

means for applying pressure to an elastomeric material contained in the cavity;

a pressure sensor in the cavity adapted to measure the pressure of the elastomeric material; and

means for determining a bulk material property of the elastomeric material (wherein the bulk material property is selected from the group consisting of Poisson'"'"'s ratio and a ratio of shear modulus to bulk modulus) in communication with the pressure sensor wherein the means for determining a bulk material property of the elastomeric material uses (A) the measured pressure from the pressure sensor and (B) the applied pressure to determine the bulk material property.

6. The apparatus of claim 5 further comprising an applied pressure sensor in the cavity adapted to measure the applied pressure.

7. The apparatus of claim 5 further comprising an environmental chamber surrounding the container wherein the environmental chamber controls the temperature of the container.

12. The apparatus of claim 5 wherein the means for applying pressure to the elastomeric material is a pressure chamber above the cavity.

13. The apparatus of claim 5 wherein the means for applying pressure to the elastomeric material is a piston adapted to be slidably received in the cavity of the container.

14. The apparatus of claim 5 wherein the means for determining a bulk material property of the elastomeric material is an electronic device.

15. The apparatus of claim 5 further comprising a means for determining the coefficient of thermal expansion for the elastomeric material from a change in the bulk material property as a function of temperature.

16. The apparatus of claim 15 wherein the means for determining the coefficient of thermal expansion is an electronic device.

17. The apparatus of claim 5 wherein the container is made of aluminum.

18. The apparatus of claim 5 wherein the container is selected from the group consisting of steel, stainless steel, alloys of steel, and combinations thereof.

19. The apparatus of claim 5 further comprising:

a plurality of cavities in the container; and

a pressure sensor for each of the plurality of cavities.

20. The apparatus of claim 19 wherein the geometric configuration for each cavity is different.

21. The apparatus of claim 5 wherein the cavities are cylindrical and have a height greater than the radius of the cavity.

8. An apparatus for determining a bulk material property of an elastomeric material comprising:

a container having a cavity adapted to hold an elastomeric material;

means for applying pressure to an elastomeric material contained in the cavity;

a pressure sensor in the cavity adapted to measure the pressure of the elastomeric material;

means for determining a bulk material property of the elastomeric material in communication with the pressure sensor wherein the means for determining a bulk material property of the elastomeric material uses the measured pressure from the pressure sensor and the applied pressure to determine the bulk material property; and

a diluent addition source in communication with the cavity of the container and adapted to add a diluent to the elastomeric material.

9. The apparatus of claim 8 wherein the diluent is selected from the group consisting of air, gas, hydrocarbon gases, organic gases, liquids, hydrocarbon liquids, organic liquids, or combinations thereof.

10. The apparatus of claim 8 further comprising a means for determining the coefficient of thermal expansion for the elastomeric material from a change in the bulk material property as a function of temperature.

11. The apparatus of claim 10 wherein the means for determining the coefficient of thermal expansion is an electronic device.

22. An apparatus for determining a bulk material property of a polymer with temperature compensation comprising:

a first container having a cavity adapted to hold an elastomeric material and which prevents radial expansion of said elastomeric material;

means for applying pressure to an elastomeric material contained in the first container adapted to measure the pressure of the elastomeric material;

a second container having a cavity adapted to hold the elastomeric material and which prevents radial expansion of said elastomeric material;

a second pressure sensor in the second container adapted to measure the pressure of the elastomeric material; and

means for determining a bulk material property of the elastomeric material (wherein the bulk material property is selected from the group consisting of Poisson'"'"'s ratio and a ratio of shear modulus to bulk modulus) in communication with the first and second pressure sensors wherein the means for determining a bulk material property uses (A) the measured pressures from the first and second pressure sensors and (B) the applied pressure to determine the bulk material property.