Dental composition containing discrete nanoparticles
First Claim
1. A dental composite, comprising:
- a polymerizable resin base; and
about 10% by volume to about 80% by volume filler consisting essentially of a ground structural filler and a non-ground nanofiller, wherein the ground structural filler comprises between about 10% by volume and about 70% by volume of the composite and consists of ground particles of mean particle size between about 0.05 μ
m and about 0.50 μ
m, and wherein the ground structural filler contains less than 50% by volume of particles above 0.5 μ
m in diameter, and wherein the non-ground nanofiller comprises between about 1.0% by volume and about 15% by volume of the composite and consists essentially of discrete, non-aggregated gamma alumina particles having a mean particle size of about 40 nm or less.
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Abstract
The present invention provides a dental composite which has the high strength required for load-bearing restorations, yet maintains a glossy appearance, even after substantial wear. Through the use of particles having a mean particle size between about 0.05 μm and about 0.50 μm, the composite is useful in stress bearing restorations and in cosmetic restorations. The structural filler used is typically ground to a mean particle size of less than 0.5 μm and also includes a nanofiller having discrete particles of a mean particle size less than 100 nm to improve handling and mechanical characteristics. The preferred dental composites maintain their surface finish even after substantial use and also have the strength properties of hybrid composite resins.
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Citations
15 Claims
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1. A dental composite, comprising:
-
a polymerizable resin base; and
about 10% by volume to about 80% by volume filler consisting essentially of a ground structural filler and a non-ground nanofiller, wherein the ground structural filler comprises between about 10% by volume and about 70% by volume of the composite and consists of ground particles of mean particle size between about 0.05 μ
m and about 0.50 μ
m, and wherein the ground structural filler contains less than 50% by volume of particles above 0.5 μ
m in diameter, andwherein the non-ground nanofiller comprises between about 1.0% by volume and about 15% by volume of the composite and consists essentially of discrete, non-aggregated gamma alumina particles having a mean particle size of about 40 nm or less. - View Dependent Claims (2, 3, 4, 5, 6, 7)
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8. A dental composite comprising:
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a polymerizable resin base; and
about 11% by volume to about 80% by volume filler in the resin base, the filler consisting essentially of a ground structural filler and a non-ground nanofiller, wherein the ground structural filler comprises between about 10% by volume and about 70% by volume of the composite and consists of ground particles having a mean particle size of between about 0.05 μ
m and about 0.50 μ
m, andwherein the non-ground nanofiller comprises between about 1.0% by volume and about 15% by volume of the composite and consists essentially of discrete, non-aggregated aluminosilicate particles having a mean particle size of less than about 100 nm, and a 1;
4 molar ratio of alumina to silica.- View Dependent Claims (9, 10, 11, 12, 13, 14, 15)
wherein the non-ground nanofiller comprises between about 5% by volume to about 12% by volume of the composite. -
12. The dental composite of claim 8, wherein the aluminosilicate particles have a mean particle size of about 80 nm.
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13. The dental composite of claim 8, wherein the resin composite, in the cured form, has a flexural strength of at least 100 MPa.
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14. The dental composite of claim 8, wherein the ground structural filler contains less than 10% by volume of particles above 0.8 μ
- m in diameter.
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15. The dental composite of claim 8, wherein the non-ground nanofiller has a refractive index in the range of about 1.48 to about 1.6.
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Specification