Liquid atomization methods and devices

• US 6,601,776 B1
• Filed: 06/06/2002
• Issued: 08/05/2003
• Est. Priority Date: 09/22/1999
• Status: Expired due to Term

• Current Assignee: Microcoating Technologies
• Original Assignee: Microcoating Technologies
• Inventors: Oljaca, Miodrag, Reese, Brian T., Hunt, Andrew Tije, Neuman, George
• Primary Examiner(s): EVANS, ROBIN OCTAVIA
• Application Number:
  US10/070,958
• Time in Patent Office: 425 Days
• Field of Search: 239/135, 239/128, 239/5, 239/132, 239/130, 239/133, 239/136
• US Class Current: 239/5
• CPC Class Codes: B05B 1/24 incorporating means for heating the liquid or other fluent material, e.g. electrically
• CPC Class Codes: B05B 17/04 operating with special methods
• CPC Class Codes: B05B 9/005 the liquid or other fluent material being a fluid close to a change of phase
• CPC Class Codes: Y10S 977/869 Optical microscope
• CPC Class Codes: Y10S 977/888 Shaping or removal of materials, e.g. etching
• CPC Class Codes: Y10S 977/89 Deposition of materials, e.g. coating, cvd, or ald
• CPC Class Codes: Y10S 977/896 Chemical synthesis, e.g. chemical bonding or breaking

Abstract

The present invention involves controlled atomization of liquids for various applications such as part/droplet seeding for laser-based measurements of flow velocity, temperature, and concentration; flame and a plasma based elemental analysis; nano-powder production; spray drying for generation of small-sized particles; nebulizers in the production of sub-micron size droplets and for atomizing fuel for use in combustion chambers. In these and other atomizer applications the control of droplet and/or particle size is very critical In some applications extremely small droplets are preferred (less than a micron), while in others, droplet diameters on the scale of several microns are required. The present invention has the flexibility of forming droplets within a particular range of diameters, wherein not only the size of the average droplet can be adjusted, but the range of sizes may be adjusted as well. The atomizer (4) itself is in the form of a heated tube (44) having an inlet end (48) and an outlet end (50). As liquid travels through the tube it is heated and upon exiting the tube and entering a reduced pressure area the liquid atomizes to form very fine droplets. By electrically heating the tube by passing a current therethrough, the heating adjustment can be performed on-the-fly allowing size adjustment during operation of the atomizer. Several different embodiments of the atomization device are disclosed.

Claims

1. A method for atomizing liquid, said method comprising the steps of:

(a) providing a chamber having a first end, a second end and an exit port, the exit port being unobstructed;

(b) routing pressurized liquid into the first end of the chamber;

(c) heating the liquid within the chamber; and

(d) controlling the temperature of the liquid from a first point between the first end and the second end, to the exit port of the chamber resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range and partial boiling occurs within the chamber.

2. The method of claim 1 wherein the liquid includes solid particles suspended therein, said solid particles being dispersed by the atomization of the liquid.

3. The method of claim 1 wherein the liquid is heated by passing heated fluid over or through a thermally conductive material that is thermally connected to the chamber.

4. The method of claim 3 wherein the heated fluid is an oil.

5. The method of claim 3 wherein the heated fluid is water.

6. The method of claim 3 wherein the heated fluid is glycol.

7. The method of claim 3 wherein the heated fluid is a flame.

8. The method of claim 3 wherein the heated fluid is a heated gas.

9. The method of claim 1 wherein the mean droplet size is less than 20 microns.

10. The method of claim 1, further comprising providing a sleeve surrounding said chamber.

11. A method for atomizing liquid, said method comprising the steps of:

(a) providing a chamber having a first end, a second end and an exit port, the exit port being unobstructed;

(b) routing pressurized liquid into the first end of the chamber;

(c) heating the liquid within the chamber; and

(d) controlling the temperature of the liquid from a first point between the first end and the second end, to the exit port of the chamber resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range;

wherein

the liquid is heated by passing an electrical current through material comprising the chamber, thereby heating the liquid in the chamber.

12. The method of claim 11 wherein the electrical current passed through the material surrounding the chamber is varied to adjust the heating of the liquid to:

(a) control the mean droplet size and the droplet size distribution of the atomized liquid;

(b) adjust for varying liquid flow rates; and

/or

(c) adjust for different liquids having different atomization properties.

13. A method for atomizing liquid, said method comprising the steps of:

(a) providing a chamber having a first end, a second end and an exit port, the exit port being unobstructed;

(b) routing pressurized liquid into the first end of the chamber;

(c) heating the liquid within the chamber; and

(d) controlling the temperature of the liquid from a first point between the first end and the second end, to the exit port of the chamber resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range, wherein said mean droplet size is between 1 and 20 microns.

14. The method of claim 13 wherein said mean droplet size is between 1 and 5 microns.

15. The method of claim 13 wherein said mean droplet size is between 5 and 20 microns.

16. A method for atomizing liquid, said method comprising the steps of;

(a) providing a chamber having a first end, a second end and an exit port, the exit port being unobstructed;

(b) routing pressurized liquid into the first end of the chamber;

(c) heating the liquid within the chamber, and

(d) controlling the temperature of the liquid from a first point between the first end and the second end, to the exit port of the chamber resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range;

wherein

the liquid at the exit of the chamber is in the form of droplets of the liquid as well as vapors and gases formed from the liquid and the stable gases and vapors at the exit of the chamber are composed of at least 1 wt % of the atomizing liquid.

17. The method of claim 16 wherein the stable gases and vapors are at the exit of the chamber are composed of at least 5 wt % of the atomizing liquid.

18. The method of claim 17 wherein the stable gases and vapors are at the exit of the chamber are composed of at least 10 wt % of the atomizing liquid.

19. The method of claim 18 wherein the stable gases and vapors are at the exit of the chamber are composed of at least 20 wt % of the atomizing liquid.

20. The method of claim 19 wherein the stable gases and vapors are at the exit of the chamber are composed of at least 40 wt % of the atomizing liquid.

21. A method for atomizing liquid, said method comprising the steps of:

(a) providing a chamber having a first end, a second end and an exit port, the exit port being unobstructed;

(b) routing pressurized liquid into the first end of the chamber,

(c) heating the liquid within the chamber; and

(d) controlling the temperature of the liquid from a first point between the first end and the second end, to the exit port of the chamber resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range;

wherein

the liquid is at a least pressure at the first end of the chamber and is at a second pressure at the exit of the chamber, the first pressure being at least 10 psi above the second pressure.

22. The method of claim 21, wherein said step of providing a chamber comprises providing a chamber that is circular in cross-section.

23. The method of claim 21 wherein the liquid at the exit of the chamber is in the form of droplets of the liquid as well as vapors and gases formed from the liquid.

24. The method of claim 21 wherein the first pressure is at least 50 psi above the second pressure.

25. The method of claim 24 wherein the first pressure is at least 100 psi above the second pressure.

26. The method of claim 25 wherein the first pressure is at least 300 psi above the second pressure.

27. The method of claim 21 wherein the liquid includes solid particles suspended therein, said solid particles being dispersed by the atomization of the liquid.

28. A device for atomizing liquid, said device comprising:

(a) a chamber having a first end, a second end and an exit port, the exit port being unobstructed; and

(b) means to control the temperature of the liquid within said chamber from a first point between said first and said second end, to said exit port;

wherein the liquid is supplied under pressure to said first end and the liquid atomizes as it exits said exit port of said chamber, resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range;

wherein

said means to control the temperature of the liquid includes a first electrical connection along said chamber, a second electrical connection along said chamber and spaced axially from said first electrical connection and a source of electrical power for providing a voltage across said electrical connections, the voltage across said connections induces an electrical current through material comprising said chamber, thereby directly heating the liquid within said chamber.

29. The device of claim 28 including means to vary the voltage across said connections, to adjust the heating of the liquid to:

(a) control the mean droplet size and the droplet size distribution of the atomized liquid;

(b) adjust for varying liquid flow rates; and

/or

(c) adjust for different liquids having different atomization properties.

30. The device of claim 28, wherein the means to control the temperature of the liquid includes a third electrical connection at said first end of said chamber.

31. A method for atomizing liquid, said method comprising the steps of:

(a) providing a chamber having a first end, a second end and an exit port, the exit port being unobstructed;

(b) routing pressurized liquid into the first end of the chamber;

(c) heating the liquid within the chamber, and

(d) controlling the temperature of the liquid from a first point between the first end and the second end, to the exit port of the chamber resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range;

wherein

the liquid is at a particular temperature at the exit of the chamber, the liquid in the chamber being at or above this temperature for less than one second.

32. The method of claim 31 wherein the mean droplet size is less than 20 microns.

33. The method of claim 31 wherein the liquid is at a particular temperature at the exit of the chamber, the liquid in the chamber being at or above this temperature for less than 0.01 second.

34. The method of claim 31 wherein the liquid is at a particular temperature at the exit of the chamber, the liquid in the chamber being at or above this temperature for less than 0.1 second.

35. A device for atomizing liquid, said device comprising:

(a) a chamber having a first end, a second end and an exit port, the exit port being unobstructed; and

(b) means to control the temperature of the liquid within said chamber from a first point between said first and said second end, to said exit port;

wherein the liquid is supplied under pressure to said first end and the liquid atomizes as it exits said exit port of said chamber, resulting in an atomized liquid spray exiting the chamber at the exit port such that the mean droplet size and the droplet size distribution of the atomized liquid are maintained within a desired range;

wherein

the liquid is at a first pressure at the first end of the chamber and is at a second pressure at the second end of the chamber, the first pressure being at least 10 psi above the second pressure.

36. The device of claim 35, wherein said chamber is circular in cross-section.

37. The device of claim 35, further comprising a sleeve surrounding said chamber.

38. The device of claim 35, wherein said exit port includes a plurality of exit ports to allow the liquid to exit said second end of said chamber.

39. The device of claim 38 wherein the liquid includes suspended particles the particles having a particular diameter, said plurality of exit ports each having a diameter at least twice the diameter of the suspended particles.

40. The device of claim 35, wherein said second end of said chamber is open.

41. A method for atomizing fuel, said method comprising the steps of:

(a) providing a chamber having a first end, a second end, an unobstructed exit port and a length to characteristic internal width CIW ratio of at least 10;

(b) routing pressurized fuel into the first end of the chamber; and

(c) directly heating the fuel within the chamber from a first point between the first and the second end, to the exit port;

wherein the fuel atomizes as it exits the exit port of the chamber.

42. A device for atomizing fuel, said device comprising:

(a) a chamber having a first end, a second end, an unobstructed exit port and a length to characteristic internal width CIW ratio of greater than 10; and

(b) means to directly heat the fuel within said chamber from a first point between the first and the second end, to the exit port;

wherein the fuel is supplied under pressure to said first end and the fuel atomizes as it exits said exit port of said chamber.

43. The device of claim 42 wherein said chamber has a length to CIW ratio of greater than 20.

44. The device of claim 43 wherein the chamber has a length to CIW ratio of greater than 50.

45. The device of claim 42, wherein said second end of said chamber is open.

46. The device of claim 42, wherein said exit port includes a plurality of ports.

47. The device of claim 42, further comprising a sleeve surrounding said chamber.

48. The device of claim 42, wherein said chamber is circular in cross-section.