On-line measuring system and method

• US 6,630,672 B1
• Filed: 06/21/2000
• Issued: 10/07/2003
• Est. Priority Date: 12/23/1997
• Status: Expired due to Term

• Current Assignee: Sugar Research Australia Limited
• Original Assignee: Bureau of Sugar Experiment Stations, Sugar North Limited
• Inventors: Berding, Nils, Mackintosh, Donald Lachlan, Atherton, Philip Gwyther, Lethbridge, Phillip John, Brotherton, George Alexander, Staunton, Stephen Paul, Grimley, Scott Clifford
• Primary Examiner(s): GAGLIARDI, ALBERT J
• Application Number:
  US09/581,211
• Time in Patent Office: 1,203 Days
• Field of Search: 250/339.07, 250/338.5, 250/339.01, 250/339.08, 250/339.09, 250/339.11, 250/339.12, 250/341.8, 250/339.03
• US Class Current: 250/339.07
• CPC Class Codes: G01N 21/3563 for analysing solids; Preparation of samples therefor
• CPC Class Codes: G01N 21/359 using near infrared light

Abstract

The invention relates to a system for the on-line measurement of a parameter in a processing stream. The system comprises a scanning head mounted adjacent a continuous stream of processed material, the scanning head comprising a remote light source and reflected light gathering and transmission apparatus; a near infrared spectrophotometer which includes a monochromator for resolving the reflected light into light of a discrete wavelength; a database containing a reference calibration equation linking absorption characteristics by wavelength and the quantified presence of the parameter of interest; and a computer for measuring the parameter by application of the calibration equation to the obtained spectrum for a sample and managing said system. The invention also comprises a method of on-line measurement of a parameter in a processing stream by NIR spectroscopy and networks comprising systems according to the invention. The system and method of the invention are particularly suited to measuring a parameter of interest in processed sugar cane.

Claims

1. A system for the on-line measurement of a parameter in processed sugar cane, the system comprising:

(a) a scanning head mounted adjacent a continuous stream of processed cane, the scanning head comprising a remote light source and reflected light gathering and transmission apparatus;

(b) a near infrared spectrophotometer which includes a monochromator for resolving the reflected light into light of a discrete wavelength;

(c) a database containing a reference calibration equation linking absorption characteristics by wavelength and the quantified presence of the parameter of interest; and

(d) a computer for measuring the parameter by application of the calibration equation to the obtained spectrum for a sample and managing said system.

2. The system according to claim 1, wherein said scanning head mounting includes vibration dampening.

3. The system according to claim 1, wherein said spectrophotometer is vibration insulated.

4. The system according to claim 1, wherein said spectrophotometer is temperature insulated.

5. The system according to claim 1, wherein said spectrophotometer is contained within an insulated and air-conditioned chamber.

6. The system according to claim 1, wherein said sensing head is remote from said spectrophotometer and is linked thereto by a fiber optic cable.

7. The system according to claim 1, wherein said database comprises a plurality of reference calibration equations.

8. The system according to claim 1, wherein said scanning head is mounted adjacent a feed chute for crushing rollers.

9. A network comprising a plurality of systems according to claim 1, said spectrophotometers of said network being standardised to one spectrophotometer within said network which serves as a master spectrophotometer.

10. A method of on-line measurement of a parameter in processed sugar cane, the method comprising the steps of:

(i) obtaining an infrared reflectance spectrum from a stream of said processed cane;

(ii) applying an appropriate calibration equation to the spectrum to quantify the presence of the parameter of interest; and

(iii) statistically validating the spectrum obtained as being represented by the calibration equation.

11. The method according to claim 10, wherein said parameter is selected from fiber content, juice brix, juice polarisation, commercial cane sugar, quality parameters, inorganic elements, or process parameters.

12. The method according to claim 10, wherein said processed sugar cane is selected from prepared cane, intermediate and final crushing roller bagasse, boiler feed materials, raw sugar, or crystalline sugar.

13. The method according to claim 10, wherein said spectrum is a single spectrum or the average of a plurality of obtained spectra.

14. The method according to claim 10, wherein said spectrum is measured over the range of 400 to 2,500 nm.

15. The method according to claim 10, wherein said infrared reflectance spectrum is obtained from a portion of the processed sugar cane passing through a by-pass line.

16. The method according to claim 10, wherein said infrared reflectance spectrum is obtained from a stream set up for analytical purposes.