Sputtering target, method of making same, and high-melting metal powder material

• US 6,676,728 B2
• Filed: 08/21/2002
• Issued: 01/13/2004
• Est. Priority Date: 07/07/1999
• Status: Expired due to Term

• Current Assignee: Hitachi Metals (Thailand) Ltd.
• Original Assignee: Hitachi Metals (Thailand) Ltd.
• Inventors: Han, Gang, Murata, Hideo, Nakamura, Hideki
• Primary Examiner(s): MAI, NGOCLAN THI
• Application Number:
  US10/224,402
• Publication Number:
  US 20030019326A1
• Time in Patent Office: 510 Days
• Field of Search: 753/42, 753/46, 75/101.9, 419/30, 419/48, 419/49
• US Class Current: 75/346
• CPC Class Codes: B22F 1/065 Spherical particles
• CPC Class Codes: B22F 1/14 Treatment of metallic powder mixing with lubricating or binding agents or with organic material B22F1/10
• CPC Class Codes: B22F 2201/013 Hydrogen
• CPC Class Codes: B22F 2202/13 Use of plasma
• CPC Class Codes: B22F 2998/00 Supplementary information concerning processes or compositions relating to powder metallurgy
• CPC Class Codes: B22F 2999/00 Aspects linked to processes or compositions used in powder metallurgy
• CPC Class Codes: B22F 3/15 Hot isostatic pressing
• CPC Class Codes: C22C 1/045 Alloys based on refractory metals
• CPC Class Codes: C23C 14/3414 Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy

Abstract

There is provided a method of making a high-melting metal powder which has high purity and excellent formability and, particularly, of a metal powder of spherical particles made of Ta, Ru, etc. having a higher melting point than iron. There is also provided a target of high-melting metal or its alloy, which is made by the sintering under pressure of these powders and which has high purity and a low oxygen concentration and shows high density and a fine and uniform structure. A powder metal material mainly composed of a high-melting metal material is introduced into a thermal plasma into which hydrogen gas has been introduced, thereby to accomplish refining and spheroidizing. Further, an obtained powder is pressed under pressure by hot isostatic pressing, etc.

Claims

1. A method of refining a metal powder comprising the steps of:

passing a metal into a thermal plasma into which a-hydrogen gas is introduced; and

refining the metal powder to have a purity of not less than 99.999% and an oxygen concentration of not more than 100 ppm.

2. A method of refining a metal powder according to claim 1, comprising passing the metal powder into a thermal plasma into which hydrogen gas is introduced, wherein the metal powder has a purity of not less than 99.9%.

3. A method of making a target comprising the steps of introducing a metal powder mainly composed of refractory metal into a thermal plasma into which hydrogen gas has been introduced, thereby to perform simultaneous refining of the metal powder and spheroidizing of the metal powder;

and sintering the obtained metal powder under pressure.

4. A method of making a target according to claim 3 comprising the steps of introducing the metal powder mainly composed of refractory metal into the thermal plasma into which hydrogen gas has been introduced, thereby to perform simultaneous refining of the metal powder and spheroidizing of the metal powder;

and sintering the obtained metal powder under hot isostatic pressing.

5. A method of making a target according to claim 3, comprising the steps of introducing the metal powder mainly composed of refractory metal into the thermal plasma into which hydrogen gas has been introduced, thereby to perform refining of the metal powder to a purity of not less than 99.99% and an oxygen concentration of not more than 100 ppm.

6. A method of making a target according to claim 3, comprising the steps of introducing the metal powder mainly composed of refractory metal into the thermal plasma into which hydrogen gas has been introduced, thereby to perform refining of the metal powder to a purity of not less than 99.999% and an oxygen concentration of not more than 100 ppm.

7. A method of making a target according to claim 3, comprising the steps of introducing the metal powder having a purity of not less than 99.9% mainly composed of the refractory metal into the thermal plasma into which the hydrogen gas has been introduced.