Method of hermetically sealing a fiber optic light guide in a metallic feedthrough sleeve with glass solder and hermetically sealed feedthrough device made thereby

• US 6,788,873 B2
• Filed: 11/26/2002
• Issued: 09/07/2004
• Est. Priority Date: 12/01/2001
• Status: Expired due to Term

• Current Assignee: Schott AG (Carl-Zeiss-Stiftung)
• Original Assignee: SCHOTT Glass
• Inventors: Fritz, Oliver, Steinberg, Andreas
• Primary Examiner(s): Nasri, Javaid H.
• Application Number:
  US10/305,293
• Publication Number:
  US 20030152356A1
• Time in Patent Office: 651 Days
• Field of Search: 385/138
• US Class Current: 385/138
• CPC Class Codes: G02B 6/3855 characterised by the method of anchoring or fixing the fibre within the ferrule G02B6/3854 takes precedence
• CPC Class Codes: G02B 6/4248 Feed-through connections for the hermetical passage of fibres through a package wall see provisionally also G02B6/4428
• CPC Class Codes: G02B 6/4428 Penetrator systems in pressure-resistant devices
• CPC Class Codes: G02B 6/4471 Terminating devices demountable connectors G02B6/3807; Cable clamps
• CPC Class Codes: G02B 6/44775 Cable seals e.g. feed-through cable seals integrated to the box seals G02B6/4444; pulling eyes G02B6/44465

Abstract

To hermetically seal a fiber optic light guide (1) in a stripped or de-coated state, I.e. the bare optical fiber (2), in a feedthrough sleeve (5) the bare optical fiber (2) is sealed together with the feedthrough sleeve (5) by composite-glass solder with local heating. To make a permanent hermetic glass seal, the feedthrough sleeve (5) is made from an Invar alloy with very low thermal expansion and the composite-glass solder is low-melting with thermal expansion properties adapted to the alloy. The composite-glass solder is molded into prefabricated half-cylinder-shaped pressed parts (7) in a press/sinter technology process, The stripped optical fiber (2) is inserted between the pressed parts (7) arranged in the feedthrough sleeve (5) and sealed by melting the pressed parts together with each other and with the stripped optical fiber and feedthrough sleeve.

Claims

1. A method for hermetically sealing a fiber optic light guide in a metallic feedthrough sleeve by means of glass solder, said fiber optic light guide comprising a longitudinally extending glass fiber (2) provided with at least one protective layer or coating (3,4), said method comprising the steps of:

a) preparing a feedthrough sleeve (5) consisting of a metallic material, said metallic material comprising an Invar alloy;

b) removing said at least one protective layer or coating (3,4) from an arbitrary position on the fiber optic light guide (1) to expose said glass fiber (2);

c) preparing two half-cylinder-shaped pressed parts (7) by a process according to press/sinter technology from a low-melting composite-glass solder, said low-melting composite-glass solder having thermal expansion properties adapted to said metallic material of the feedthrough sleeve (5), the half-cylinder-shaped pressed parts (7) each having a respective axial groove (7a) with a corresponding cross-section adapted to a diameter of the exposed glass fiber (2);

d) assembling half-cylinder-shaped pressed parts (7) together with the exposed glass fiber (2) inserted in the grooves (7a) of the half-cylinder-shaped pressed parts in said arbitrary position on the fiber optic light guide; and

e) melting the half-cylinder-shaped pressed parts (7) together with each other and with the glass fiber (2) and the feedthrough sleeve (5) by local heating.

2. The method as defined in claim 1, wherein said feedthrough sleeve (5) has a first axial section (5a) having a first interior diameter, said first axial section (5a) of said feedthrough sleeve (5) is filled with adhesive around said fiber optic light guide (1), said at least one protective layer or coating (3,4) is removed from only a portion of said fiber optic light guide (1) in said first axial section (5a), said feedthrough sleeve (5) has a second axial section (5b) having a second interior diameter for receiving the half-cylinder-shaped pressed parts (7) and said first interior diameter is less than said second interior diameter.

3. The method as defined in claim 1, wherein said Invar alloy consists of a NI—

Co—

Fe alloy.

4. The method as defined in claim 1, wherein said Invar alloy consists of a Fe—

Ni—

Cr alloy or a Fe—

NI alloy.

5. The method as defined in claim 1, further comprising gold coating the feedthrough sleeve (5).

6. The method as defined in claim 1, wherein said local heating is for local thermal sealing and takes place by means of an electrically heated incandescent filament, inductively, by means of focused infrared radiation or in an oven.

7. The method as defined in claim 1, wherein the half-cylinder-shaped pressed parts (7) of the composite-glass solder are made from a lead-borate glass powder and an inert expansion-lowering filling material by said process according to said press/sinter technology.

8. The method as defined in claim 7, wherein said filling material is β

-Eucryptite.

9. The method as defined in claim 1, wherein said half-cylinder-shaped pressed parts (7) of said composite-glass solder consist of a phosphate glass and an inert expansion-lowering filling material.

10. A hermetically sealed feedthrough device for hermetically sealing a fiber optic light guide (1) in a feedthrough sleeve by means of glass solder, said fiber optic light guide (1) comprising a longitudinally extending glass fiber (2) provided with at least one protective layer or coating (3,4), said hermetically sealed feedthrough device comprising

a metallic feedthrough sleeve (5) consisting of a metallic material, said metallic material comprising an Invar alloy;

and

prefabricated half-cylinder-shaped pressed parts (7) consisting of low-melting composite-glass solder, said low-melting composite-glass solder having thermal expansion properties adapted to said metallic material of the metallic feedthrough sleeve (5);

wherein a portion of the fiber optic light guide (1) in an arbitrary position on the fiber optic light guide (1) is sealed between said prefabricated half-cylinder-shaped pressed parts (7) after removal of the at least one protective layer or coating (3,4) provided on said portion at the fiber optic light guide by fusion or melting of said prefabricated half-cylinder-shaped pressed parts (7) together with said glass fiber (2) and with the metallic feedthrough sleeve (5).

11. The hermetically sealed feedthrough device as defined in claim 10, wherein said low-melting composite-glass solder has a thermal expansion coefficient of from 4.3 to 5 ppm/K and a processing temperature below Curie temperature of the Invar alloy during sealing.

12. The hermetically sealed feedthrough device as defined in claim 10, wherein said feedthrough sleeve (5) has a first axial section (5a) having a first interior diameter, said first axial section (5a) of said feedthrough sleeve (5) is filled with adhesive (6) around said fiber optic light guide (1), said at least one protective layer or coating (3,4) is removed from only a part of said fiber optic light guide (1) in said first axial section (5a), said feedthrough sleeve (5) has a second axial section (5b) having a second interior diameter for receiving the half-cylinder-shaped pressed parts (7) and said first interior diameter is less than said second interior diameter.

13. The hermetically sealed feedthrough device as defined in claim 10, wherein the Invar allay is a Ni—

Co—

Fe alloy, a Fe-Ni—

Cr alloy or a Fe—

Ni alloy.

14. A method for hermetically sealing a fiber optic light guide in a metallic feedthrough sleeve by means of glass solder, said fiber optic light guide (1) comprising a longitudinally extending glass fiber (2) provided with at least one protective layer or coating (3,4), said method comprising the steps of:

a) preparing a feedthrough sleeve (5) consisting of a metallic material, said metallic material comprising an Invar alloy;

b) removing said at least one protective layer or coating (3, 4) from the fiber optic light guide (1) to expose said glass fiber (2);

c) making two half-cylinder-shaped pressed parts (7) by a process according to press/sinter technology from a low-melting composite-glass solder, said low-melting composite-glass solder having thermal expansion properties corresponding to those of said metallic material of the feedthrough sleeve (5), the half-cylinder-shaped pressed parts (7) each having a respective axial groove (7a) with a corresponding cross-section adapted to a diameter of the exposed glass fiber (2);

d) assembling said two half-cylinder-shaped pressed parts (7) together with the exposed glass fiber (2) inserted in the grooves (7a) of the half-cylinder-shaped pressed parts; and

e) melting the half-cylinder-shaped pressed parts (7) together with each other and with the glass fiber (2) and with the feedthrough sleeve (5) by local heating;

wherein said composite-glass solder comprises a phosphate glass and an inert expansion-lowering filling material.

15. The method as defined in claim 14, wherein said low-melting composite-glass solder has a thermal expansion coefficient of from 4.3 to 5 ppm/K and said local heating is performed at temperatures below a Curie temperature of the metallic material of the feedthrough sleeve (5).

16. The method as defined in claim 14, wherein said feedthrough sleeve (5) has a first axial section (5a) with a first interior diameter and a second axial section (5b) with a second interior diameter, said second axial section receiving the half-cylinder-shaped pressed parts (7), said first axial section (5a) of said feedthrough sleeve (5) is filled with adhesive around said fiber optic light guide (1), said at least one protective layer or coating (3,4) is removed from only a part of said fiber optic light guide (1) in said first axial section (5a) but from all of said fiber optic light guide within said second axial section (5b) and said first interior diameter is less than said second interior diameter.

17. The method as defined in claim 14, wherein said process according to press/sinter technology comprises spray-drying an aqueous emulsion comprising a fine grained phosphate glass powder and an inert expansion-lowering filling material to form a glass press granulate, pressing the glass press granulate in a mold to form a green pressed part and sintering said green pressed part in an oven to form one of the half-cylinder-shaped pressed parts (7).

18. A method for hermetically sealing a fiber optic light guide in a metallic feedthrough sleeve by means of glass solder, said fiber optic light guide (1) comprising a longitudinally extending glass fiber (2) provided with at least one protective layer or coating (3,4), said method comprising the steps of:

a) preparing a feedthrough sleeve (5) consisting of a metallic material, said metallic material comprising an Invar alloy;

b) removing said at least one protective layer or coating (3,4) from the fiber optic light guide (1) to expose said glass fiber (2);

c) making two half-cylinder-shaped pressed parts (7) by a process according to press/sinter technology from a low-melting composite-glass solder, said low-melting composition glass solder having thermal expansion properties corresponding to those of said metallic material of the feedthrough sleeve (5), the half-cylinder-shaped pressed parts (7) each having a respective axial groove (7a) with a corresponding cross-section adapted to a diameter of the exposed glass fiber (2);

d) assembling said two half-cylinder-shaped pressed parts (7) together with the exposed glass fiber (2) inserted in the grooves (7a) of the half-cylinder-shaped pressed parts; and

e) melting the half-cylinder-shaped pressed parts (7) together with each other and with the glass fiber (2) and with the feedthrough sleeve (5) by local heating;

wherein said composite-glass solder comprises a lead-borate glass and an inert expansion-lowering filling material.

19. The method as defined in claim 18, wherein said low-melting composite-glass solder has a thermal expansion coefficient of from 4.3 to 5 ppm/K and said local heating is performed at temperatures below a Curie temperature of the metallic material of the feedthrough sleeve (5).

20. The method as defined in claim 18, wherein said feedthrough sleeve (5) has a first axial section (5a) with a first interior diameter and a second axial section (5b) with a second interior diameter for receiving the half-cylinder-shaped pressed parts (7), said first axial section (5a) of said feedthrough sleeve (5) is filled with adhesive around said fiber optic light guide (1), said at least one protective layer or coating (3,4) is removed from only a part of said fiber optic light guide (1) in said first axial section (5a) but from all of said fiber optic light guide within said second axial section (5b) and said first interior diameter is less than said second interior diameter.

21. The method as defined in claim 18, wherein said process according to press/sinter technology comprises spray-drying an aqueous emulsion comprising a fine grained lead-borate glass powder and an inert expansion-lowering filling material to form a glass press granulate, pressing the glass press granulate in a mold to form a green pressed part and sintering said green pressed part in an oven to form one of the half-cylinder-shaped pressed parts (7).