Device for forming, transporting and diffusing small calibrated amounts of liquid

• US 6,790,011 B1
• Filed: 05/24/2002
• Issued: 09/14/2004
• Est. Priority Date: 05/27/1999
• Status: Expired due to Term

• Current Assignee: Osmooze S.A.
• Original Assignee: Osmooze S.A.
• Inventors: Millet, Jean-Claude, Le Pesant, Jean-Pierre
• Primary Examiner(s): FREAY, CHARLES GRANT
• Application Number:
  US09/926,619
• Time in Patent Office: 844 Days
• Field of Search: 417/48, 417/50, 222/251
• US Class Current: 417/48
• CPC Class Codes: B01L 3/0241 Drop counters; Drop formers making arrays for combinatorial libraries B01J19/0046; automation of dispensing for analysis G01N35/10
• CPC Class Codes: B05B 5/16 Arrangements for supplying liquids or other fluent material
• CPC Class Codes: F04B 17/00 Pumps characterised by combination with, or adaptation to, specific driving engines or motors
• CPC Class Codes: F04B 19/006 Micropumps F04B43/043 and F04B43/095 take precedence

Abstract

The invention relates to a device for diffusing drops of at least one liquid, the device being of the type comprising at least one liquid displacement path defined by a series of pairs of close-together surfaces (4a, 6a, . . . , 14a) enabling liquid to be retained and to be displaced from one pair of surfaces to another. The device comprises:

both a series of pairs of close-together surfaces (4a, 6a, . . . , 14a) defining at least one displacement path, and co-operating to store the liquid, to form drops of liquid, and to move liquid drops to an outlet from said path leading towards a drop destination site; and

electric field application means applying a determined sequence of electric fields between the pairs of close-together surfaces so as to form drops of liquid from the liquid storage, and to move and mix the drops of liquid to the drop outlet of said path.

Claims

1. A device for diffusing calibrated small volumes or drops of at least one liquid, comprising:

at least one displacement path for the liquid defined by a series of pairs of close-together surfaces constructed and arranged to enable the liquid to be retained and to be moved from one pair of surfaces to another; and

means for applying an electric field between the pairs of surfaces in order to move the liquid from one pair of surfaces to another;

wherein;

the series of pairs of close-together surfaces defining at least one displacement path co-operate to store the liquid, to form drops of liquid, and to move liquid drops to an outlet from said path leading towards a drop destination site; and

the means for applying an electric field applies a predetermined sequence of electric fields between the pairs of close-together surfaces so as to form drops of liquid from the liquid storage and so as to move the drops to the drop outlet of said path.

2. A device according to claim 1, wherein said liquid is a liquid containing an active principle intended for applications in generating odors, in cosmetics, in medical treatments, in hygiene, in chemistry, or in medical analysis.

3. A device according to claim 2, wherein said liquid contains at least one essential oil and/or a pheromone.

4. A device according to claim 1, wherein the outlet for drops from the displacement path leads to the outside of the device.

5. A device according to claim 1, wherein the outlet for drops from the displacement path loads to a destination site situated within the device.

6. A device according to claim 4, wherein the outlet for drops is formed by at least one orifice putting the device into communication with the outside, said orifice having at least one electro-osmosis electrode or at least one heating resistance to accelerate the evaporation of liquids at the orifice.

7. A device according to claim 1, wherein said electric field application means comprises an electrode associated with at least one surface in each pair of close-together surfaces.

8. A device according to claim 1, said surfaces present wettability that is controlled by surface treatment.

9. A device according to claim 1, wherein at least one of two surfaces of a pair of surfaces is carried by a structure in the form of a mesa formed on a respective substrate, said mesa-forming structure causing said surfaces to be closer together than the respective substrates, so that capillarity maintains the liquid selectively in the zones where the surfaces are closer together.

10. A device according to claim 1, wherein the surfaces of a pair of surfaces are substantially parallel.

11. A device according to claim 1, wherein the surfaces of a pair of surfaces form between them a small angle, thus creating a zone towards one edge of said surfaces that is closer together than an opposite zone, thus enabling liquid to be entrained by capillarity towards said closer-together zone.

12. A device according to claim 11, wherein for a pair of surfaces, said closer-together zone is situated at the edge which is closer to a destination site for the displaced liquid.

13. A device according to claim 1, wherein at least one of the pairs of close together surfaces presents a plurality of planes so as to create a plurality of different spacings between said close-together surfaces.

14. A device according to claim 13, wherein the at least one pair of electrodes presenting a plurality of planes is arranged so that the close-together spacing is situated downstream relative to the liquid displacement direction.

15. A device according to claim 1, wherein pairs of close-together surfaces form at least one reservoir, a throttle pad, and a pad for forming a small drop of liquid, co-operating to constitute said small volume.

16. A device according to claim 1, wherein a pair of said close-together surfaces comprises a reservoir which defines a confinement volume operating by capillary action and interface tension between two close-together surfaces, at least one sector of the periphery of a liquid-retaining zone constituting extractor-forming means and at least one surface of the retaining zone being connected to liquid feed means.

17. A device according to claim 16, wherein the extractor-forming means is constituted by a liquid-retaining zone adjacent to a reservoir and is implemented by two close together parallel faces so as to produce capillary and surface tension action between them, said surface being provided with electrodes enabling an electric field to be created in said zone to extract calibrated quantities of liquid from the reservoir the width of said zone relative to the liquid displacement axis being substantially smaller than its length and more substantially smaller both than the width of the reservoir to which it is connected and that the width of the close-together surfaces of the displacement path for moving calibrated volumes of liquid to which it is connected.

18. A device according to claim 1, wherein the displacement path for moving calibrated volumes of liquid is constituted by a zone for retaining liquid by capillary and surface tension action between two close-together surfaces, such that the width of said retaining zone relative to the displacement path axis is of a dimension that is substantially greater than that of an extractor-forming pair of electrodes to which it is connected, the surfaces forming said zone being provided with electrodes that enable a distributable electric field to be created for receiving at least one calibrated quantity of liquid extracted from the reservoir by the action of the extractor.

19. A device according to claim 1, including at least two displacement paths enabling calibrated quantities of liquids to be extracted from at least two reservoirs and conveyed towards at least one other path internal to the device, the calibrated quantities optionally not having the same volume.

20. A device according to claim 1, wherein at least one reservoir can put into communication with the outside of the device so that liquid can be caused to penetrate therein.

21. A device according to claim 1, including at least two reservoirs arranged in such a manner as to enable the calibrated small volumes extracted from said reservoirs to be combined and mixed together, and at least one displacement path for conveying the combined volumes to a destination zone.

22. A device according to claim 1, wherein the at least one reservoir and each pair of close-together surfaces of said displacement path are configured to create relaxation of the perimeter of the liquid in the absence of an electric field so as to facilitate the passage of the liquid from one pair of surfaces to another.

23. A device according to claim 1, wherein at least one reservoir contains a rinsing liquid suitable for cleaning the at least one displacement path for moving calibrated small volumes of liquid.

24. A device according to claim 1, constructed and arranged to be fed from at least one extractable reservoir.

25. An assembly for diffusing liquid in the form of small volumes, comprising in a common package:

at least one device for forming, moving, and diffusing drops according to claim 1;

control electronics for generating electrical potentials for delivering control signals in programmable manner to the means for applying an electric field;

at least one reservoir of liquid to be diffused; and

an electrical power supply source.

26. An assembly according to claim 25, wherein the package is substantially planar, having the format of a smart card or credit card.