System for retrieving a gas phase sample from a gas stream containing entrained liquid, and sample conditioner assembly therefore

• US 6,904,816 B2
• Filed: 04/03/2003
• Issued: 06/14/2005
• Est. Priority Date: 08/22/1996
• Status: Expired due to Term

• Current Assignee: Mayeaux Holding, LLC
• Original Assignee: Donald P. Mayeaux
• Inventors: Mayeaux, Donald P.
• Primary Examiner(s): NOLAND, THOMAS
• Application Number:
  US10/408,026
• Publication Number:
  US 20030233890A1
• Time in Patent Office: 803 Days
• Field of Search: 7386311-86325, 738/63, 738/638.1, 738/638.5, 738/638.6, 73/290.1, 73/310.7
• US Class Current: 73/863.23
• CPC Class Codes: G01N 1/2035 by deviating part of a fluid stream, e.g. by drawing-off or tapping
• CPC Class Codes: G01N 1/2205 with filters
• CPC Class Codes: G01N 2035/00326 Analysers with modular structure
• CPC Class Codes: Y10T 137/0396 Involving pressure control
• CPC Class Codes: Y10T 137/598 With repair, tapping, assembly, or disassembly means

Abstract

A system for the retrieval and initial conditioning of sample gas for “on line” analyzers or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is highly susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches an assembly including a phase separation membrane and housing configured to facilitate the removal of entrained liquid from a sample gas stream. Accuracy of the sample is enhanced, and compositional changes are avoided by first extracting a sample from the process gas followed by removal of entrained liquid it may contain, with the entrained liquid removal being conducted at the prevailing process gas pressure and temperature. Thereafter the liquid free sample may be desaturated by lowering its pressure to reduce its susceptibility to condensation.

Claims

1. A method of conditioning a sample of gas derived from a fluid stream, comprising the steps of:

a. providing a fluid conduit having first and second ends, said first end of said fluid conduit communicating with said fluid stream;

b. providing an insertion assembly comprising a phase separation membrane having first and second sides;

c. providing a housing in communication with said fluid stream, said housing configured to receive said insertion assembly;

d. inserting said insertion assembly into said housing;

e. directing said sample of gas having liquid entrained therein to communicate with said phase separation membrane;

f. allowing the passage of gas from said sample of gas through said phase separation membrane, providing filtered gas, while preventing the passage of entrained liquid from said sample of gas and coalescing said entrained liquid from said sample of gas.

2. The method of claim 1, wherein there is provided the additional step after step “

e”

of draining said coalesced liquid from the vicinity of said phase separation membrane.

3. The method of claim 2, wherein said coalesced liquid is drained into said fluid stream.

4. The method of claim 2, wherein there is provided the additional step after step “

e”

of analyzing said filtered gas.

5. The method of claim 2, wherein said fluid stream and said sample of gas has a temperature and a pressure, and wherein there is further included the step of maintaining said pressure and temperature of said sample of gas at the same temperature and pressure of said fluid stream.

6. The method of claim 5, wherein there is provided the additional step of providing a housing assembly comprising thermal insulation means, and wherein said housing assembly is configured to envelope said fluid conduit, said sample of gas, and said phase separation membrane so as to maintain said temperature of said sample of gas at the same temperature of said fluid stream.

7. The method of claim 2, wherein there is further provided containment means for containing said fluid stream, and wherein said fluid conduit, said phase separation membrane, and said drainage means are situated within said containment means.

8. The method of claim 2, wherein after step “

e”

there is provided the additional step of measuring the amount of coalesced liquid emanating from said drainage means.

9. The method of claim 2, wherein there is further provided the steps, after step “

f”

of;

i. obtaining a representative sample of fluid from said fluid stream, said representative sample containing both gas phase and entrained liquid phase matter in equal proportion to said fluid stream;

ii. vaporizing said entrained liquid contained within said representative sample to a produce a homogenous vapor phase sample; and

iii. analyzing homogenous vapor phase sample, providing compositional data, and comparing same with said filtered gas analysis data, so as to discern differences therein.