Apparatus and method for self-calibration of mass flow controller

• US 6,948,508 B2
• Filed: 06/24/2002
• Issued: 09/27/2005
• Est. Priority Date: 06/24/2002
• Status: Expired due to Term

• Current Assignee: MKS Instruments Incorporated
• Original Assignee: MKS Instruments Incorporated
• Inventors: Shajii, Ali, Smith, John A., Ambrosina, Jesse, Kottenstette, Nicholas
• Primary Examiner(s): Scherbel, David A.
• Assistant Examiner(s): Krishnamurthy, Ramesh
• Application Number:
  US10/178,378
• Publication Number:
  US 20030234046A1
• Time in Patent Office: 1,191 Days
• Field of Search: 137/1, 137/486, 137/487.5, 73/11.6, 73/13.5, 732/025, 702/45, 702/100
• US Class Current: 137/1
• CPC Class Codes: G01F 1/684 Structural arrangements; Mounting of elements, e.g. in relation to fluid flow
• CPC Class Codes: G01F 1/6965 comprising means to store calibration data for flow signal calculation or correction
• CPC Class Codes: G01F 1/86 Indirect mass flowmeters, e.g. measuring volume flow and density, temperature or pressure
• CPC Class Codes: G01F 25/15 specially adapted for gas meters G01F25/11 - G01F25/14, G01F25/17 take precedence
• CPC Class Codes: G01F 5/00 Measuring a proportion of the volume flow
• CPC Class Codes: G05D 7/0635 by action on throttling means G05D7/0688, G05D7/0694 take precedence
• CPC Class Codes: Y10T 137/0318 Processes
• CPC Class Codes: Y10T 137/7759 Responsive to change in rate of fluid flow
• CPC Class Codes: Y10T 137/7761 Electrically actuated valve

Abstract

A mass flow controller includes a mass flow sensor and a calibrator configured to perform a self-calibration on the mass flow controller. The calibrator generates flow measurements that are used as “standards” and flow measurements from the mass flow sensor are correlated to flow measurements from the calibrator.

Claims

1. A self-calibrating mass flow controller, comprising:

a mass flow sensor configured to produce an electronic signal representative of mass flow in the mass flow controller as a function of the flow sensed by the sensor;

a mass flow calibrator operative to produce an independent electronic signal representative of mass flow in the mass flow controller as a function of the flow sensed by the calibrator, the mass flow calibrator includes a pressure sensor operative to measure pressure of gases within a receptacle of predetermined volume between a bypass included in the mass flow sensor and an outlet control valve; and

an electronic controller configured to correlate the mass flow signal from the mass flow sensor to the rate of flow indicated by the independent electronic signal from the mass flow calibrator.

2. The mass flow controller of claim 1 wherein the outlet control valve is

operative to control the flow of gas in the mass flow controller under control of the electronic controller.

3. The self-calibrating mass flow controller of claim 1 wherein the mass flow sensor is a thermal mass flow sensor.

4. The self-calibrating mass flow controller of claim 1 wherein the electronic controller is configured to employ the correlated mass flow sensor signal to control the outlet valve during non-calibration operation.

5. The self-calibrating mass flow controller of claim 1 wherein the electronic controller is configured to store the correlation between the mass flow sensor signal and the mass flow calibrator signal.

6. A mass flow controller as in claim 1 wherein the mass flow calibrator, comprises:

a variable flow gas source configured to provide proportionate flow to the mass flow sensor and to the receptacle; and

a pressure differentiator configured to produce an electronic signal representative of the time derivative of gas pressure within the receptacle of predetermined volume, said time derivative signal being proportional to the mass flow signal of the mass flow calibrator.

7. The mass flow controller of claim 6 wherein the gas flow source is configured to supply the same gas at the same flow rate to both the mass flow sensor and the receptacle of predetermined volume.

8. The mass flow controller of claim 6 wherein the gas flow source is configured to supply gas to the mass flow sensor and to the receptacle of predetermined volume in series.

9. The mass flow controller of claim 6 wherein the differentiator includes:

analog differentiator circuitry configured to produce an electronic signal that is representative of the time derivative of an electronic signal representative of the pressure within the receptacle produced by the pressure sensor; and

an analog to digital converter configured to convert one or more values of the analog time derivative signal to digital samples of the time derivative.

10. The mass flow controller of claim 9 further comprising:

storage for storing one or more samples of the signal representative of the time derivative of gas pressure.

11. The mass flow controller of claim 1 wherein the electronic controller is configured to correlate the mass flow signal from the mass flow sensor to that of the mass flow calibrator for a plurality of gas flows and to produce one or more compensation coefficients.

12. The mass flow controller of claim 11 wherein the mass flow controller is configured to store the one or more compensation coefficients.

13. The mass flow controller of claim 12 wherein the mass flow controller is configured to compute the mass flow of a gas using one or more of the stored compensation coefficients and the flow signal from the mass flow sensor.

14. The mass flow controller of claim 6 wherein the differentiator includes:

an analog to digital converter configured to convert one or more values of the electronic signal, produced by the pressure sensor, which is representative of the pressure within the receptacle into digital form; and

a digital differentiator configured to produce a plurality of digital values representative of the time derivative of the pressure signal.

15. The mass flow controller of claim 14 further comprising:

storage for storing one or more samples of the signal representative of the time derivative of gas pressure.

16. The mass flow controller of claim 6 wherein the gas source is configured to provide an exponentially variable flow gas.

17. The mass flow controller of claim 6 wherein the gas source is configured to provide an exponentially increasing gas flow.

18. The mass flow controller of claim 6 wherein the gas source is configured to provide an exponentially decreasing gas flow.

19. The mass flow controller of claim 6 wherein the gas source is configured to provide a patterned gas flow, the pattern including both increasing and decreasing gas flow.

20. A self-calibrating mass flow controller comprising:

a thermal mass flow sensor configured to sense the flow of gas in the mass flow controller and to produce an electronic signal representative of the sensed flow;

an electronic controller;

an outlet control valve operated by the controller to allow a predetermined flow of gas through the mass flow controller; and

a pressure sensor operative to measure the pressure of gas within the receptacle formed between the thermal mass flow sensor'"'"'s bypass and the outlet control valve, the receptacle thus-formed being of predetermined volume, the electronic controller configured to operate the outlet valve to vary the flow through the mass flow controller, to take the time derivative of the pressure signal, to normalize the time derivative signal, and to correlate the signal from the thermal mass flow sensor to the normalized time derivative signal.

21. The mass flow controller of claim 20 wherein the controller is configured to employ analog differentiator circuitry to take the derivative of the pressure signal.

22. The mass flow controller of claim 20 wherein the controller is configured to compute at least two pressure differences and divide the differences by corresponding time spans to create the derivative of the pressure signal.

23. The mass flow controller of claim 20 wherein the electronic controller is configured to correlate the mass flow signal from the mass flow sensor to that of the normalized time derivative for a plurality of gas flows and to produce one or more compensation coefficients relating the thermal mass flow signal of one gas flow to that of another.

24. The mass flow controller of claim 23 wherein the mass flow controller is configured to store the one or more compensation coefficients.

25. The mass flow controller of claim 24 wherein the mass flow controller is configured to compute the mass flow of a gas using one or more of the stored compensation coefficients and the flow signal from the mass flow sensor.

26. A method of self-calibrating a mass flow controller that includes a mass flow sensor, an electronic controller, and a mass flow calibrator, comprising the steps of:

a mass flow controller'"'"'s mass flow sensor producing an electronic signal representative of mass flow in the mass flow controller as a function of the flow sensed by the sensor;

the mass flow controller'"'"'s mass flow calibrator producing an independent electronic signal representative of mass flow in the mass flow controller as a function of the flow sensed by the calibrator, the mass flow calibrator includes a pressure sensor operative to measure pressure of gases within a receptacle of predetermined volume between a bypass of the mass flow sensor and an outlet control valve; and

the mass flow controller'"'"'s electronic controller correlating the mass flow signal produced by the mass flow sensor in response to its sensed flow within the mass flow controller to the flow indicated by the independent electronic signal produced by the mass flow calibrator in its sensing of flow in the mass flow controller.

27. The method of claim 26 further comprising the step of:

the mass flow controller'"'"'s electronic controller controlling the outlet control valve to control the flow of gas in the mass flow controller.

28. The method of claim 27 wherein a thermal mass flow sensor produces the mass flow electronic signal.

29. The method of claim 26 wherein the electronic controller employs the correlated mass flow sensor signal to control the outlet control valve during non-calibration operation.

30. The method of claim 26 wherein the electronic controller is configured to store the correlation between the mass flow sensor signal and the mass flow calibrator signal.

31. The method as in claim 26 wherein the mass flow calibrator comprises:

a variable flow gas source configured to provide proportionate flow to the mass flow sensor and to the receptacle; and

a pressure differentiator that produces an electronic signal representative of the time derivative of gas pressure within the receptacle of predetermined volume, said time derivative signal being proportional to the un-normalized mass flow signal of the mass flow calibrator.

32. The method of claim 31 wherein the gas flow source supplies the same gas at the same flow rate to both the mass flow sensor and the receptacle of predetermined volume.

33. The method of claim 31 wherein the gas flow source supplies gas to the mass flow sensor and to the receptacle of predetermined volume in series.

34. The method of claim 31 wherein the differentiator comprises:

analog differentiator circuitry that produces an electronic signal that is representative of the time derivative of an electronic signal, produced by the pressure sensor, which is representative of the pressure within the receptacle; and

an analog to digital converter that converts one or more values of the analog time derivative signal to digital samples of the time derivative.

35. The method of claim 34 further comprising the step of:

storing one or more samples of the signal representative of the time derivative of gas pressure.

36. The method of claim 26 wherein the electronic controller correlates the mass flow signal from the mass flow sensor to that of the mass flow calibrator for a plurality of gas flows and produces one or more compensation coefficients.

37. The method of claim 36 wherein the mass flow controller stores the one or more compensation coefficients.

38. The method of claim 37 wherein the mass flow controller computes the mass flow of a gas using one or more of the stored compensation coefficients and the flow signal from the mass flow sensor.

39. The method of claim 31 wherein the differentiator comprises:

an analog to digital converter that converts one or more values of an electronic signal, produced by the pressure sensor that is representative of the pressure within the receptacle, into digital form; and

a digital differentiator that produces a plurality of digital values representative of the time derivative of the pressure signal.

40. The method of claim 39 further comprising the step of:

storing one or more samples of the signal representative of the time derivative of gas pressure.

41. The method of claim 31 wherein the gas source provides an exponentially variable flow gas.

42. The method of claim 41 wherein the gas source provides an exponentially increasing gas flow.

43. The method of claim 40 wherein the gas source provides an exponentially decreasing gas flaw.

44. The method of claim 31 wherein the gas source provides a patterned gas flow, the pattern including both increasing and decreasing gas flow.

45. The method of claim 26 wherein the mass flow sensor and calibrator produce independent electronic signals representative of mass flow in situ.

46. The method of claim 26 wherein gas flow is restricted in order to differentiate the pressure over a greater period of time than would be available with unrestricted flow.

47. A method of calibrating a self-calibrating mass flow controller comprising the steps of:

a thermal mass flow sensor sensing the flow of gas in the mass flow controller and producing an electronic signal representative of the sensed flow;

an electronic controller operating an outlet control valve to allow a varied flow of gas through the mass flow controller; and

a pressure sensor measuring the pressure of gas within the receptacle formed between the thermal mass flow sensor'"'"'s bypass and the outlet control valve, the receptacle thus-formed being of predetermined volume;

the electronic controller taking the time derivative of the pressure signal, normalizing the time derivative signal, and correlating the signal from the thermal mass flow sensor to the normalized time derivative signal.

48. The method of claim 47 wherein analog differentiator circuitry takes the derivative of the pressure signal.

49. The method of claim 47 wherein the controller computes at least two pressure differences and divides the differences by corresponding time spans to create the derivative of the pressure signal.

50. The method of claim 47 wherein the electronic controller correlates the mass flow signal from the mass flow sensor to that of the normalized time derivative for a plurality of gas flows;

and

produces one or more compensation coefficients relating the thermal mass flow signal of one gas flow to that of another.

51. The method of claim 50 wherein the mass flow controller stores the one or more compensation coefficients.

52. The method of claim 51 wherein the mass flow controller computes the mass flow of a gas using one or more of the stored compensation coefficients in combination with the flow signal from the mass flow sensor.

53. The method of claim 47 wherein the thermal mass flow and pressure sensors measure in situ.

54. The method of claim 47 wherein gas flow is restricted in order to differentiate the pressure over a greater period of time than would be available with unrestricted flow.