Sample supplying device for a dry particle-size distribution measuring apparatus and method

• US 7,042,557 B2
• Filed: 12/18/2002
• Issued: 05/09/2006
• Est. Priority Date: 12/19/2001
• Status: Expired due to Fees

• Current Assignee: Horiba Limited
• Original Assignee: Horiba Limited
• Inventors: Yamaguchi, Tetsuji, Kitamura, Hiroyuki
• Primary Examiner(s): Toatley, Jr., Gregory J.
• Assistant Examiner(s): VALENTIN, JUAN D
• Application Number:
  US10/322,819
• Publication Number:
  US 20030147074A1
• Time in Patent Office: 1,238 Days
• Field of Search: 198/758, 198/533, 209/241, 221/179, 221/180
• US Class Current: 356/36
• CPC Class Codes: G01N 15/0205 by optical means
• CPC Class Codes: G01N 2015/0096 Investigating consistence of powders, dustability, dustiness

Abstract

A dry particle-size distribution measuring apparatus and method is provided for suspending a plurality of bristle members across a support surface of a dispensing trough with bristles being arranged to contact and disperse any clusters of particles to a primary state prior to releasing the particles to a sample flow cell. A source of light can irradiate the sample flow cell and a detector unit can measure any scattered and/or diffracted light to provide corresponding signals. A control unit can determine the size and distribution of particles from the corresponding signals. The bristle members can be mounted on a brush unit that is directly mounted on the trough and both the trough and the brush unit can be driven by the same vibrator unit.

Claims

1. In a sample supplying device for a dry particle-size distribution measuring apparatus which is configured by a trough that accommodates a sample, and a linear feeder that vibrates said trough, and in which the sample in said trough is dropped through a sample drop hole formed in said trough, by vibrating said trough, the improvement of an impacting member for separating any plurality of primary particles aggregated together comprising:

a brush unit positioned in said trough and operatively mounted to vibrate in a plane transverse to a surface of the trough by the vibration of the trough to contact and pulverize any aggregated groups of the sample to a primary particle state before being dropped by gravity through the sample drop hole.

2. The sample supply device of claim 1, wherein the sample contains particles of approximately 1 μ

m in size and the brush unit includes bristles that are spaced greater than 1 μ

m in distance apart.

3. The sample supply device of claim 2, wherein the brush unit includes a cylindrical base with bristles extending 360°

around the base.

4. The sample supply device of claim 1, further including a mounting unit for mounting the brush unit to provide both vertical and horizontal movement in said trough.

5. The sample supply device of claim 1, wherein the brush unit includes bristles that are progressively positioned closer to each other the closer to the sample drop hole.

6. The sample supply device of claim 1, wherein the brush unit includes bristles that are positioned in an elongated arrangement across said trough.

7. The sample supply device of claim 1, wherein the brush unit includes bristles arranged in rectangular pattern with center devoid of bristles.

8. A method of separating particles into a primary state of single particles in a particle-size distribution measuring apparatus, comprising the steps of:

supplying a sample of particles to a support surface;

vibrating the support surface to move the sample of particles along the support surface to a dispense position; and

contacting the sample of particles upstream of the dispense position with a plurality of bristles that vibrate relative to the support surface, the arrangement of bristles being spaced to assure impact contact with any cluster of particles attached together whereby the bristles will contact and disperse the cluster of particles to a primary state after impact with the bristles so that the sample of particles will be in a primary state after contact with the bristles.

9. The method of claim 8, wherein the sample of particles are approximately 1 μ

m in size and the bristles are spaced from each other at a distance approximately slightly greater than 1 μ

m.

10. The method of claim 8, wherein the bristles are vibrated in a vertical and horizontal direction relative to the support surface.

11. The method of claim 10, wherein the bristles are operatively mounted above the support surface and are vibrated by the vibration of the support surface to contact and pulverize the cluster of particles.

12. A device for separating particles into a primary state of single particles in a particle-size distribution measuring apparatus, comprising:

a support member for receiving sample particles;

means for supplying a sample of particles to a surface of the support member;

a vibrating unit operatively connected to the support member for moving the sample of particles by a vibratory movement to a release position on the support member; and

a plurality of bristles that vibrate relative to the support surface between the means for supply and the release position whereby the bristles will contact and disperse by breaking any clusters of sample particles into a primary state so that the sample of particles will be in a primary state after contact with the bristles.

13. The device of claim 12 wherein the support member is a trough with a substantially horizontal support surface that only moves by the vibratory movement.

14. The device of claim 13 wherein the support surface is tapered in a direction towards the release position.

15. The device of claim 14 wherein the support member is made of a synthetic resin.

16. The device of claim 12 wherein the vibrating unit includes a spring unit and an electromagnetic drive unit to provide a longitudinal vibration to the support member.

17. The device of claim 16 wherein the plurality of bristles are mounted on a holder that is attached to the support member to enable vertical and horizontal movement of the plurality of bristles relative to the support surface by the operation of the vibrating unit.

18. The device of claim 17 wherein individual bristles are spaced on the holder at a distance slightly greater than a diameter of the primary state of particle size.

19. The device of claim 18 wherein the bristles are formed of a synthetic resin.