Method and device for evaluating physical parameters of an underground reservoir from rock cuttings taken therefrom

• US 7,082,812 B2
• Filed: 03/26/2004
• Issued: 08/01/2006
• Est. Priority Date: 03/26/2003
• Status: Expired due to Fees

• Current Assignee: Institut Francais Du Petrole (IFP Energies Nouvelles)
• Original Assignee: Institut Francais Du Petrole (IFP Energies Nouvelles)
• Inventors: Templier, Arnaud, Egermann, Patrick, Lenormand, Roland
• Primary Examiner(s): Williams, Hezron
• Assistant Examiner(s): FITZGERALD, JOHN P
• Application Number:
  US10/809,895
• Publication Number:
  US 20040211252A1
• Time in Patent Office: 858 Days
• Field of Search: 73/38
• US Class Current: 73/38
• CPC Class Codes: G01N 15/0826 and measuring fluid flow rate, i.e. permeation rate or pressure change
• CPC Class Codes: G01N 15/088 Investigating volume, surface area, size or distribution of pores; Porosimetry
• CPC Class Codes: G01N 2015/0833 Pore surface area
• CPC Class Codes: G01N 2015/0873 Dynamic sorption, e.g. with flow control means

Abstract

Method and device for evaluating, simultaneously and with a single equipment, physical parameters such as the absolute permeability and the porosity of fragments taken from a fragmented artificial or natural porous medium.

The porosity of the fragments is measured by means of pressure tests using helium or any other gas, according to a protocol known in the art. Chamber (1) in which they are contained is communicated with a tank (11) of known volume containing helium at a known pressure. At pressure balance, the value of the solid volume can be deduced. The rock envelope volume and the mass in fragments are also measured. The porosity of the samples and the density of the rock are determined by combining these measurements. Their permeability is then measured by immersing them in a liquid and by communicating the chamber with a liquid initially at a predetermined pressure contained in an accumulator (9) so as to compress the gas trapped in the pores of the rock. The values of the physical parameters are determined by modelling the evolution of the volume of liquid injected in the chamber and by means of an iterative adjustment.

Applications: petrophysical measurements from drill cuttings or crushed cores for example.

Claims

1. A method for evaluating, with a single equipment, physical parameters of a fragmented porous medium from rock fragments taken in this medium, comprising a stage of immersing fragments contained in a containment chamber in a liquid and of intermittently communicating the chamber containing the fragments with a source of liquid under pressure comprising an accumulator containing an elastic volume of liquid, so as to compress the gas trapped in the pores of the rock, a stage of measuring the volume of liquid injected, a stage of modelling the evolution of the volume of liquid injected from a priori selected initial values at least for permeability and the residual gas saturation, and a stage of iterative adjustment of the value of the physical parameters of the rock fragments so as to obtain the best possible adjustment of the modelled evolution of the volume injected with the measured evolution of the volume injected in the chamber, characterized in that:

during the stage of immersion, in the liquid, of the fragments contained in the containment chamber, the volume of liquid injected is measured by measuring the concomitant pressure variation in said accumulator.

2. A method as claimed in claim 1, wherein the modelling stage is also carried out from a priori selected initial values for porosity.

3. A method as claimed in claim 1, comprising a prior stage of feeding the washed and dried rock fragments into containment chamber which is first communicated with a gas tank at a predetermined pressure, so as to determine the solid volume of said fragments, the envelope volume and the mass of the fragments are measured, and the porosity and the density of the rock fragments are deduced therefrom, the modelling stage comprising modelling the evolution of the volume of liquid injected from a priori selected initial values of permeability and of the residual gas saturation, and from the value measured for porosity.

4. A method as claimed in claim 1, wherein the stage of communicating the chamber with the accumulator is carried out so as to cause, during a first period, a fast pressure increase in the chamber and compression of the gas trapped in the pores of the rock, followed by a relaxation period after isolation of the chamber, and comprises measuring the evolution of the pressure in the chamber during the two periods.

5. A method as claimed in claim 1, wherein the containment chamber is filled with drill cuttings.

6. A method as claimed in claim 1, wherein the containment chamber is filled with rock fragments obtained by crushing cores taken in a well, notably cores obtained by sidewall coring of a well.

7. A method as claimed in claim 1, wherein the containment chamber is filled with rock fragments invaded by drilling fluids.

8. A method as claimed in claim 1, wherein the containment chamber is filled with previously cleaned rock fragments.

9. A device for evaluating physical parameters of a fragmented porous medium from fragments taken in this medium, comprising a processing system, a containment chamber for the fragments, an injection assembly for injecting a liquid into the chamber so as to fill the chamber containing the rock fragments, and for carrying out a cycle comprising a stage of liquid injection into the chamber, this assembly comprising an accumulator containing an elastic volume of liquid and means controlled by the processing system for controlling communication of the accumulator with the chamber containing the rock fragments, means for measuring the pressure in the chamber, the processing system being suited for modelling the evolution of the volume of liquid injected from initial values selected for the physical parameters of the rock fragments, and for adjusting iteratively the values to be given to these physical parameters so as to obtain the best possible adjustment between the modelled evolution of the physical quantity and the measured evolution of said quantity in the chamber, characterized in that it comprises pressure measuring means for measuring pressure variations in the accumulator and in that the processing system is suited for calculation of the volume of liquid injected in the chamber from the accumulator, from the pressure variation measured by the pressure measuring means.

10. A device as claimed in claim 9, comprising a gas tank that can be communicated with chamber by means of a valve, an instrument for measuring the envelope volume so as to determine the porosity of the fragments and means for measuring the mass of the fragments.

11. A device as claimed in claim 10, characterized in that the means for measuring the envelope volume of the fragments to be tested comprise a powder pycnometer.

12. A device as claimed in claim 10, wherein the elastic volume of liquid is delimited in said accumulator by a volume of gas, said relation being obtained by applying the gas law.

13. A device as claimed in claim 10, wherein the elastic volume of liquid is delimited in said accumulator by an elastic membrane or a moveable element, said relation being obtained by prior calibration of the deformations or of the displacements.

14. A device as claimed in claim 10, wherein the pressure measuring means for measuring pressure variations in the accumulator comprises a manometer connected to an outlet of the accumulator.