Slurry treatment and shipping method

• US 7,101,507 B1
• Filed: 05/27/1999
• Issued: 09/05/2006
• Est. Priority Date: 05/28/1998
• Status: Expired due to Fees

• Current Assignee: Mineral Assets, LLC
• Original Assignee: Paul E. Adler
• Inventors: Adler, Paul E.
• Primary Examiner(s): MCKANE, ELIZABETH L
• Application Number:
  US09/701,455
• Time in Patent Office: 2,658 Days
• Field of Search: 422/32, 422/38, 422/307, 422/308, 422/309, 422/1, 422/41, 241/23, 241/46.01, 241/65, 241/606, 165/66
• US Class Current: 422/1
• CPC Class Codes: A61L 2/04 Heat A61L2/08 takes precedence

Abstract

Aerobic and anaerobic contamination is removed from a slurry by a sterilizing process and apparatus (10). A slurry piping circuit (26, 28, 30, 32, 34) interconnects a supply tank (12), three serial heat exchangers (16, 18, 20) and a storage tank (14). The circuit and storage tank are sanitized by flushing with mist of hydrogen peroxide (44) and nitrogen (50). One heat exchanger (16) transfers heat from the sterilized slurry to the unsterilized slurry. A closed hot water piping circuit (60, 62, 64) interconnects a hot water boiler (22) and the other two heat exchangers (18, 20). The slurry is sterilized in an insulated manifold (24) interconnecting the other two heat exchangers (18, 20). Slurry is pumped through the piping and heated by hot water in the manifold to kill the bacteria, and is covered by a layer of nitrogen (54) in the storage tank (14). The storage tank may be transported to a distant terminus where it is unloaded and again sterilized, if necessary, or is used immediately in an industrial process.

Claims

1. A process for sterilizing a contaminatable slurry to preclude aerobic and anaerobic bacteria from the slurry, comprising the steps of

a. providing a sanitized oxygen-free fluid handling system,

b. pumping the slurry through the system at a predetermined pressure,

c. heating the slurry to a sterilizing temperature of about 210°

F.-290°

for a predetermined time to sterilize the slurry,

d. cooling the sterilized slurry by transferring heat to the unsterilized slurry entering the process, and

e. transferring the sterilized slurry to a sanitized fluid collection device.

2. The process of claim 1, including the step of flushing the fluid handling system with a mist of nitrogen and a sanitizing chemical to sanitize the system.

3. The process of claim 1, wherein the sterilizing temperature is about 230°

F.-270°

F. the predetermined time is greater than 5 seconds, and the cooling temperature is below 100°

F.

4. The process of claim 3, wherein the sterilizing temperature is about 250°

F. and the predetermined time is about 2 minutes.

5. The process of claim 1, wherein the sanitized fluid collection device is a storage tank, and including the steps of

f. flushing the fluid handling system with a mist of nitrogen and a sanitizing chemical to sanitize the system, and

g. excluding oxygen from the storage tank, and

h. transporting the storage tank to a terminus for offloading of the slurry.

6. The process of claim 5, including the further steps of

i. offloading the slurry, and

j. repeating steps a-e.

7. The process of claim 1, Including the steps of

f. flushing the fluid handling system with a mist of nitrogen and hydrogen peroxide to sanitize the system,

g. providing a tank as the fluid collection device, and

h. excluding oxygen from the tank by covering the sterilized slurry with a blanket of nitrogen.

8. The process of claim 1, wherein the fluid collection device is the supply system of a further industrial process.

9. The process of claim 1, wherein the slurry is kaolin or calcium carbonate.

10. The process of claim 1, including the step of mounting the fluid handling system on a mobile platform for transportability.

11. Fluid handling and sterilizing apparatus for sterilizing contaminatable slurries to preclude aerobic and anaerobic bacteria from the slurry, comprising

a sterilizing unit for heating slurry to a sterilizing temperature,

a heat exchanger for transferring heat from the sterilized slurry to the unsterilized slurry to preheat the unsterilized slurry and cool the sterilized slurry,

a piping circuit connecting the pump to the heat exchanger and connecting the heat exchanger to the sterilizing unit for handling the unsterilized slurry, and connecting the sterilizing unit to the heat exchanger and exiting the heat exchanger for handling the sterilized slurry, and

a pump for intaking unsterilized slurry and pumping slurry through the piping circuit at a predetermined pressure at a predetermined flow rate

wherein the sterilizing unit includes

a heating, unit,

a second heat exchanger for transferring heat from the heating unit to the unsterilized slurry to raise the temperature of the unsterilized slurry to a sterilizing temperature,

a manifold for containing the heated slurry at the sterilizing temperature, and

a third heat exchanger for transferring heat from the sterilized slurry to the heating unit to cool the sterilized slurry.

12. The fluid handling and sterilizing apparatus of claim 11, wherein the manifold is sized to maintain the slurry at the sterilizing temperature for a predetermined time sufficient to fully sterilize the slurry.

13. The fluid handling and sterilizing apparatus of claim 11, wherein the heating unit comprises

a hot water boiler for heating water to a second predetermined temperature,

a second piping circuit interconnecting the hot water boiler, the second heat exchanger, and the third heat exchanger, and

a second pump for pumping water through the second piping circuit at a second predetermined flow rate.

14. The fluid handling and sterilizing apparatus of claim 13, wherein the first predetermined flow rate is about 17 gpm, and the second predetermined flow rate is about 30 gpm.

15. The fluid handling and sterilizing apparatus of claim 11, including a source of contaminatable slurry in the form of kaolin or calcium carbonate.

16. The fluid handling and sterilizing apparatus of claim 11, where the pump is a peristaltic pump.

17. The fluid handling and sterilizing apparatus of claim 11, including a mobile platform mounting the apparatus to enable transportation to a variety of locations.