ITFM extraction of oil seeds

• US 7,156,981 B2
• Filed: 04/26/2002
• Issued: 01/02/2007
• Est. Priority Date: 01/25/1999
• Status: Expired due to Fees

• Current Assignee: Bio-Extraction Inc.
• Original Assignee: Bio-Extraction Inc.
• Inventors: Skinner, Ronald E., Ablett, Richard F., Wilde, Peter F.
• Primary Examiner(s): Nguyen; Tam M.
• Application Number:
  US10/133,020
• Publication Number:
  US 20020189976A1
• Time in Patent Office: 1,712 Days
• Field of Search: 208/311, 208/313, 208/315, 208/320, 208/340
• US Class Current: 208/311
• CPC Class Codes: A23D 9/00 Other edible oils or fats, e.g. shortenings, cooking oils
• CPC Class Codes: A23J 1/142 by extracting with organic solvents
• CPC Class Codes: A23J 1/144 Desolventization
• CPC Class Codes: B01D 11/0219 Fixed bed of solid material
• CPC Class Codes: B01D 11/0288 Applications, solvents
• CPC Class Codes: C10G 1/04 by extraction
• CPC Class Codes: C11B 1/10 by extracting
• CPC Class Codes: C11B 1/104 using super critical gases or vapours
• CPC Class Codes: C11B 9/025 Recovery by solvent extraction

Abstract

A process for the producing edible protein-containing meal for human and animal consumption and high quality food grade oils from oil seed using iodotrifluoromathane as the solvent is shown. The meal has a significantly improved level of dietary available (absorbable) protein. The process involves the preparation of protein isolates by a procedure which is conducted at room temperature, thus decreases protein degradation and denaturing which is caused by elevated temperatures. The process also provides for extraction of substantially all oils and fats, which interfere with the formation of the protein micelle, from the protein meal providing a cleaner, purer product with high levels of absorbable protein. Such protein isolates can then be used as such or added to formulated foods in order to increase the total protein content of that food. The protein produced and the oils recovered have compositions which are also unique and unobtainable by prior processing methods.

Claims

1. A process of preparing a protein containing meal comprising:

providing a protein source material in a form that will allow a liquid extraction solvent applied thereto to permeate said protein source material,

mixing the protein source material with the liquid extraction solvent comprising iodotrifluoromethane in combination with a cosolvent to dissolve solvent soluble constituents of the protein source material,

forming a liquid phase and a solid phase, such mixing being conducted in a closed pressurized vessel,

separating the liquid phase from the solid phase,

removing the solvent from the liquid phase to leave an oil based extract and

removing the solvent from the solid phase to leave a dry, protein containing meal.

2. The process of claim 1 wherein the protein source material is crushed, cracked, ground or otherwise comminuted to allow the solvent to permeate said protein source material.

3. The process of claim 1 wherein the solvent and protein source material are mixed together for a period of from about 1 minute to about 90 minutes at a temperature of from about −

20°

C. to about 45°

C.

4. The process of claim 3 wherein the solvent and protein source material are mixed together for a period of from about 5 minutes to about 50 minutes.

5. The process of claim 3 wherein the solvent and protein source material are mixed together for at a temperature of from about 15°

C. to about 35°

C.

6. The process of claim 1 wherein a first quantity of the solvent is mixed with the protein source material for a period of from about 1 to 3 minutes at a temperature of from about 17°

C. to about 18°

C., the liquid phase is separated from the solid phase, and one or more additional quantities of the solvent are mixed with the protein source material under substantially the same conditions, and the liquid phase so produced is removed and added to the first collected liquid phase.

7. The process of claim 1 wherein the pressure of the vessel during mixing is the vapor pressure of the solvent at the processing temperature, said pressure being adequate to maintain the solvent as a liquid.

8. The process of claim 1 wherein the solvent is removed from the liquid phase and the solid phase by placing each of the solid phase and the liquid phase in separate sealed containers, reducing the pressure above each of the liquid phase and the solid phase to cause the solvent to vaporize, and collecting the evaporated solvent by transferring said vaporized solvent to a refrigerated container, causing the vaporized solvent to condense into a liquid.

9. The process of claim 1 wherein the co-solvent is HFC-134a.

10. The process of claim 1 wherein the co-solvent is added to the liquid phase after separation of the liquid phase from the solid phase.

11. The process of claim 1 wherein the protein source material is rapeseed, canola, soy, barley or flax seed or bean.