Micro slit viscometer with monolithically integrated pressure sensors

• US 7,290,441 B2
• Filed: 03/11/2005
• Issued: 11/06/2007
• Est. Priority Date: 10/31/2001
• Status: Expired due to Term

• Current Assignee: RheoSense, Inc.
• Original Assignee: RheoSense, Inc.
• Inventors: Baek, Seong-Gi
• Primary Examiner(s): CYGAN, MICHAEL T
• Application Number:
  US11/078,015
• Publication Number:
  US 20050183496A1
• Time in Patent Office: 970 Days
• Field of Search: 73/540.9, 73/544.3, 73/543.9, 73/541.4, 73/541.6
• US Class Current: 73/54.09
• CPC Class Codes: G01N 11/08 by measuring pressure required to produce a known flow

Abstract

An improved micro slit viscometer includes a combined micrometer depth rectangular slit flow channel with monolithically integrated multiple pressure sensors in the flow channels and a pumping system that injects a test sample to the channel at a desired flow rate. Pressure sensing diaphragm of the monolithically integrated pressure sensors is smooth to minimize the flow disturbance thereby measuring accurate local pressures. With the measurement of the pressures at various locations of the channel the true viscosity of test sample can be calculated. The viscometer may consist of multiple flow channels and thus the true viscosity at multiple shear rates can be measured simultaneously for a given flow rate thereby obtaining a full viscosity curve as a function of shear rate of non-Newtonian liquids in a much faster manner. The viscometer needs only a miniscule amount of sample, which minimizes a waste of test material. The flow channels and the monolithically integrated pressure sensors are fabricated using microfabriaction processes on wafers and combined, which greatly reduce the production costs.

Claims

1. A slit rheometer for determining the viscosities of liquids comprising:

a monolithic sensor plate formed from a combination of a pressure sensor membrane and a pressure sensor substrate having at least two cavities formed in one or the other or both of the pressure sensor membrane and the pressure sensor substrate, a portion of the pressure sensor membrane extending over respective cavities of the at least two cavities whereby the portions of the pressure sensor membrane extending over the respective cavities will deflect into the respective cavities upon application of pressure to the portion of the pressure sensor membrane over a respective cavity, the amount of deflection being proportional to the pressure applied to the membrane over the respective cavity, and a pressure sensor formed in each of the plurality of cavities to provide the monolithic sensor plate with a substantially smooth surface and a plurality of independent pressure sensors in the monolithic sensor plate;

a channel substrate configured to form at least one flow channel therein when combined with the monolithic sensor plate with the at least one flow channel having a flow entrance and a flow exit; and

each of said at least one flow channel having at least two individual pressure sensors located therein and spaced sufficiently away from the liquid entrance and the liquid exit whereby a pressure drop of fully developed flow of liquid through the at least one flow channel can be measured.

2. A slit rheometer according to claim 1, additionally including means to force a liquid to flow through the at least one flow channel at a known volumetric flow rate.

3. A slit rheometer according to claim 1, wherein the at least one flow channel has a width and a depth and wherein the width of the flow channel is at least about ten times larger than the depth of the flow channel in each of the at least one flow channels.

4. A slit rheometer according to claim 1, wherein the sensor plate has at least one temperature sensor for each of the at least one flow channels located to measure the temperture of the liquid flowing through the flow channel.

5. A slit rheometer according to claim 1, wherein there are at least two flow channels connected in series.

6. A slit rheometer according to claim 5, wherein the at least two flow channels connected in series each have a channel width and a channel depth, and wherein the at least two flow channels connected in series are different in channel depth.

7. A slit rheometer according to claim 5, wherein the at least two flow channels connected in series each have a channel width and a channel depth, and wherein the at least two flow channels connected in series are different in channel width.

8. A slit rheometer according to claim 1, wherein there are at least two channels connected in parallel.

9. A slit rheometer according to claim 1, where the at least one channel is on the order of a micrometer in depth.

10. A slit rheometer according to claim 9, where the at least one channel is at least about ten micrometers in width.

11. A slit rheometer according to claim 10 where the at least one channel has a length of at least about one hundred micrometers.

12. A slit rheometer according to claim 1 where the pressure sensors are capacitive pressure sensors.

13. A slit rheometer according to claim 1, wherein the channel substrate is combined with the monolithic sensor plate along one surface of the channel substrate, and wherein the channel substrate has at least one channel cavity formed therein opening along the one surface of the channel substrate so that when the channel substrate is combined with the monolithic sensor plate, the monolithic sensor plate closes the at least one channel cavity along the one surface of the channel substrate to form the at least one flow channel.

14. A slit rheometer according to claim 13, wherein the at least one channel cavity has opposite ends and the flow entrance extends through the channel substrate to one end of the channel cavity and the flow exit extends through the channel substrate to the opposite end of the channel cavity.

15. A slit rheometer according to claim 13, wherein each of the at least one channel cavity includes three channel walls and wherein the monolithic sensor plate froms a fourth wall for each of the at least one channel cavity when the monolithic sensor plate is combined with the channel substrate to form the at least one flow channel.

16. A slit rheometer according to claim 1, wherein the channel substrate is at least a portion of a wafer of a material used in microfabrication processes.

17. A slit rheometer according to claim 1, wherein the pressure sensor membrane is at least a portion of a silicon wafer.

18. A slit rheometer according to claim 1, wherein the pressure sensor substrate is at least a portion of a wafer of a material used in microfabrication processes.

19. A slit rheometer according to claim 18, wherein the wafer of a material used in microfabrication processes is a borosilicate glass wafer.

20. A slit rheometer according to claim 1, wherein the pressure sensor formed in each of the plurality of cavities is a single sensor cooperable with the portion of the pressure sensor membrane extending over the respective cavity to sense the deflection of such portion and provide a signal indicative of a single deflection sensed for the respective cavity.

21. A method of manufacturing slit rheometers comprising:

forming at least two cavities in one or both of a pressure sensor membrane and a pressure sensor substrate;

combining the pressure sensor membrane with the pressure sensor substrate to create a pressure sensor plate with a portion of the pressure sensor membrane extending over respective cavities of the at least two cavities;

forming independent pressure sensors in the at least two cavities; and

combining the pressure sensor plate with a channel substrate to create at least one flow channel having a flow entrance and a flow exit through which liquid can flow, the flow channel passing over at least two of the at least two independent pressure sensors in the pressure sensor plate with the at least two independent pressure sensors spaced sufficiently away from the liquid entrance and the liquid exit whereby a pressure drop of fully developed flow of liquid through the at least one flow channel can be measured.

22. A method of manufacturing slit rheometers according to claim 21 where the at least two cavities formed in one or both of the pressure sensor membrane and the pressure sensor substrate are formed by etching using chemical etching.

23. A method of manufacturing slit rheometers according to claim 21 where the at least two cavities formed in one or both of the pressure sensor membrane and the pressure sensor substrate are formed by etching using plasma etching.

24. A method of manufacturing slit rheometers according to claim 21 where the at least two cavities formed in one or both of the pressure sensor membrane and the pressure sensor substrate are formed by etching using a combination of chemical and plasma etching.

25. A method of manufacturing slit rheometers according to claim 21 where the pressure sensors are capacitor type sensors.

26. A method of manufacturing slit rheometer according to claim 21 where the pressure sensors are piezoresistive type sensors.