Method and apparatus for downhole spectral analysis of fluids

• US 7,336,356 B2
• Filed: 01/26/2006
• Issued: 02/26/2008
• Est. Priority Date: 01/26/2006
• Status: Active Grant

• Current Assignee: Schlumberger Technology Corporation (Schlumberger NV)
• Original Assignee: Schlumberger Technology Corporation (Schlumberger NV)
• Inventors: Fujisawa, Go, Vannuffelen, Stephane, Yamate, Tsutomu, Indo, Kentaro, Terabayashi, Toru
• Primary Examiner(s): Toatley, Jr.; Gregory J.
• Assistant Examiner(s): Stock, Jr.; Gordon J.
• Application Number:
  US11/307,170
• Publication Number:
  US 20070171412A1
• Time in Patent Office: 761 Days
• Field of Search: None
• US Class Current: 356/326
• CPC Class Codes: G01J 3/0218 using optical fibers
• CPC Class Codes: G01J 3/0232 using shutters
• CPC Class Codes: G01J 3/0294 Multi-channel spectroscopy
• CPC Class Codes: G01J 3/10 Arrangements of light sources specially adapted for spectrometry or colorimetry
• CPC Class Codes: G01J 3/36 Investigating two or more bands of a spectrum by separate detectors
• CPC Class Codes: G01J 3/42 Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry beam switching arrangements G01J3/08
• CPC Class Codes: G01N 2021/317 Special constructive features
• CPC Class Codes: G01N 21/274 Calibration, base line adjustment, drift correction
• CPC Class Codes: G01N 21/31 Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry G01N21/72 takes precedence
• CPC Class Codes: G01N 2201/08 Optical fibres; light guides

Abstract

A downhole fluid analysis system comprises an input light signal that is directed through a fluid sample housed in a sample cell. The input light signal may originate from a plurality of light sources. A light signal output from the sample cell is then routed to two or more spectrometers for measurement of the represented wavelengths in the output light signal. The output of the spectrometers is then compared to known values for hydrocarbons typically encountered downhole. This provides insight into the composition of the sample fluid. Additionally, the input light can be routed directly to the two or more spectrometers to be used in calibration of the system in the high temperature and noise environment downhole.

Claims

1. A fluid analysis system configured to operate downhole in a well traversing a formation comprising:

at least one light source generating an input light across a wide, continuous spectral range;

a sample cell operable to receive a flowing sample fluid therein, said sample cell further comprising;

at least one input window allowing said input light to flow into said sample cell and through the flowing sample fluid to produce an output light;

at least one output window allowing said output light to flow out of said sample cell;

two or more downhole spectrometers configured to measure said output light and generate a plurality of measurement signals; and

an analysis device configured to receive said plurality of measurement signals and determine properties of the flowing sample fluid.

2. The fluid analysis system configured to operate downhole as defined in claim 1 further comprising:

a plurality of light sources wherein said plurality of light sources generate light across a wide spectral range.

3. The fluid analysis system configured to operate downhole as defined in claim 1, wherein

one of said two or more spectrometers comprises a filter array spectrometer.

4. The fluid analysis system configured to operate downhole as defined in claim 1, wherein

one of said two or more spectrometers comprises a grating spectrometer.

5. The fluid analysis system configured to operate downhole as defined in claim 1, wherein

said two or more spectrometers comprise at least one filter array spectrometer and at least one grating spectrometer.

6. The fluid analysis system configured to operate downhole as defined in claim 1, wherein

said at least one light source comprises a halogen lamp.

7. The fluid analysis system configured to operate downhole as defined in claim 1, wherein

said at least one light source comprises a light emitting diode (LED).

8. The fluid analysis system configured to operate downhole as defined in claim 1, wherein

said at least one light source comprises a laser.

9. The fluid analysis system configured to operate downhole as defined in claim 1 further comprising:

a plurality of light processing units for processing said input light and said output light.

10. The fluid analysis system configured to operate downhole as defined in claim 1 further comprising at least one of:

a first light collector positioned between said at least one light source and said sample cell; and

a second light collector positioned between said sample cell and said two or more spectrometers.

11. The fluid analysis system configured to operate downhole as defined in claim 10, wherein

said first and second light collectors further comprise a router configured to selectively route light to at least one of a specific input window, a specific spectrometer, and at a specific time.

12. The fluid analysis system configured to operate downhole as defined in claim 9, wherein

said plurality of processing units comprises at least one amplitude modulator.

13. The fluid analysis system configured to operate downhole as defined in claim 9, wherein

said plurality of processing units comprises at least one frequency modulator.

14. A fluid analysis system configured to operate downhole in a well traversing a formation comprising:

at least one light source generating an input light across a wide, continuous spectral range;

a sample cell operable to receive a sample fluid therein, said sample cell further comprising;

at least one input window allowing said input light to flow into said sample cell and through the sample fluid to produce an output light;

at least one output window allowing said output light to flow out of said sample cell;

two or more downhole spectrometers configured to measure said output light and generate a plurality of measurement signals;

an analysis device configured to receive said plurality of measurement signals and determine properties of the sample fluid; and

a reference light collector positioned between said at least one light source and said two or more spectrometers, said reference light collector operable to route said input light directly from said at least one light source to said two or more spectrometers for a reference measurement.

15. The fluid analysis system configured to operate downhole as defined in claim 14 further comprising:

one or more light processing units between said reference light collector and said two or more spectrometers.

16. A method for downhole fluid analysis comprising:

providing input light using at least one light source generating an input across a wide, continuous spectral range;

inserting a flowing sample fluid into a sample cell;

introducing said input light to an input window of said sample cell, said light traversing through said flowing sample fluid and producing an output light traversing through an output window in said sample cell;

receiving said output light at two or more downhole spectrometers;

generating a plurality of measurement signals by said two or more spectrometers based on said output light; and

analyzing said plurality of measurement signals to determine properties of said flowing sample fluid.

17. The method for downhole fluid analysis defined in claim 16 further comprising:

providing input light from a plurality of light sources wherein said plurality of light sources generate light across a wide spectral range.

18. The method for downhole fluid analysis defined in claim 16 further comprising:

processing said input light before introduction to said sample cell.

19. The method for downhole fluid analysis defined in claim 18, wherein

said processing comprises modulating the amplitude of said input light.

20. The method for downhole fluid analysis defined in claim 18, wherein

said processing comprises modulating the frequency of said input light.

21. A method for downhole fluid analysis comprising:

providing input light using at least one light source generating an input light across a wide, continuous spectral range;

inserting a sample fluid into a sample cell;

introducing said input light to an input window of said sample cell, said light traversing through said sample fluid and producing an output light traversing through an output window in said sample cell;

receiving said output light at two or more downhole spectrometers;

generating a plurality of measurement signals by said two or more spectrometers based on said output light; and

analyzing said plurality of measurement signals to determine properties of said sample fluid;

introducing said input light directly to said two or more spectrometers;

generating a plurality of reference signals from said two or more spectrometers;

calibrating said spectrometers using said plurality of reference signals.