Scalable continuous production system
First Claim
1. An automated continuous processing parallel chemical production system for automatically producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
- (a) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor comprising at least;
a first reactant inlet, a second reactant inlet, a reaction volume coupled in fluid communication with the first reactant inlet and the second reactant inlet, and a product outlet coupled in fluid communication with the reaction volume;
(b) a reactant feed apparatus including;
(i) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to selectively couple said first reactant inlet of each chemical reactor in fluid communication with the supply of the first reactant, so that each first reactant inlet of the plurality of chemical reactors is coupled in parallel, with the supply of the first reactant; and
(ii) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to selectively couple said second reactant inlet of each chemical reactor in fluid communication with the supply of the second reactant, so that each second reactant inlet of the plurality of chemical reactors is coupled in parallel, with the supply of the second reactant;
(c) a product collection assembly configured to be placed in fluid communication with a product receiver, and to selectively couple said product outlet of each chemical reactor in fluid communication with the product receiver; and
(d) a system controller controllably coupled with said first reactant feed assembly, said second reactant feed assembly, and said product collection assembly, the system controller monitoring and controlling production of the desired chemical product by said plurality of chemical reactors, and designating at least one of said plurality of chemical reactors as a backup reactor, such that the system controller causes;
(i) said first reactant feed assembly to isolate said first reactant inlet of the backup reactor from the supply of the first reactant, while coupling said first reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the first reactant, such that while the system is automatically producing the desired chemical product, the first reactant inlet of each reactor not designated as a backup reactor is coupled in fluid communication with the first reactant feed assembly, such that a first reactant fluid is simultaneously supplied to each reactor not designated as a backup reactor;
(ii) said second reactant feed assembly to isolate said second reactant inlet of the backup reactor from the supply of the second reactant, while coupling said second reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the second reactant, such that while the system is automatically producing the desired chemical product, the second reactant inlet of each reactor not designated as a backup reactor is coupled in fluid communication with the second reactant feed assembly, such that a second reactant fluid is simultaneously supplied to each reactor not designated as a backup reactor; and
(iii) said product collection assembly to isolate said product outlet of the backup reactor from said product receiver, while coupling the product outlet of each other chemical reactor in fluid communication with the product receiver.
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Accused Products
Abstract
A parallel chemical production system producing a desired product by operating a plurality of reactors in parallel. The fluidic properties of each of the reactors are identical to the properties of a test reactor employed to determine conditions for producing the product, to facilitate scaling up production. In one embodiment, the production system is configured such that at least one reactor is always offline for cleaning, servicing, and use as a backup. If sensors detect less than optimal conditions in any reactor, the reactor is taken offline and serviced, while a previously designated backup reactor is placed online to maintain continuous production. Another aspect involves arranging the reactors in a concentric configuration to facilitate equal fluid distribution.
80 Citations
51 Claims
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1. An automated continuous processing parallel chemical production system for automatically producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
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(a) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor comprising at least;
a first reactant inlet, a second reactant inlet, a reaction volume coupled in fluid communication with the first reactant inlet and the second reactant inlet, and a product outlet coupled in fluid communication with the reaction volume;(b) a reactant feed apparatus including; (i) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to selectively couple said first reactant inlet of each chemical reactor in fluid communication with the supply of the first reactant, so that each first reactant inlet of the plurality of chemical reactors is coupled in parallel, with the supply of the first reactant; and (ii) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to selectively couple said second reactant inlet of each chemical reactor in fluid communication with the supply of the second reactant, so that each second reactant inlet of the plurality of chemical reactors is coupled in parallel, with the supply of the second reactant; (c) a product collection assembly configured to be placed in fluid communication with a product receiver, and to selectively couple said product outlet of each chemical reactor in fluid communication with the product receiver; and (d) a system controller controllably coupled with said first reactant feed assembly, said second reactant feed assembly, and said product collection assembly, the system controller monitoring and controlling production of the desired chemical product by said plurality of chemical reactors, and designating at least one of said plurality of chemical reactors as a backup reactor, such that the system controller causes; (i) said first reactant feed assembly to isolate said first reactant inlet of the backup reactor from the supply of the first reactant, while coupling said first reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the first reactant, such that while the system is automatically producing the desired chemical product, the first reactant inlet of each reactor not designated as a backup reactor is coupled in fluid communication with the first reactant feed assembly, such that a first reactant fluid is simultaneously supplied to each reactor not designated as a backup reactor; (ii) said second reactant feed assembly to isolate said second reactant inlet of the backup reactor from the supply of the second reactant, while coupling said second reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the second reactant, such that while the system is automatically producing the desired chemical product, the second reactant inlet of each reactor not designated as a backup reactor is coupled in fluid communication with the second reactant feed assembly, such that a second reactant fluid is simultaneously supplied to each reactor not designated as a backup reactor; and (iii) said product collection assembly to isolate said product outlet of the backup reactor from said product receiver, while coupling the product outlet of each other chemical reactor in fluid communication with the product receiver. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17, 18, 19, 20, 21, 22, 23, 24, 25)
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26. A concentrically parallel chemical production system for producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
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(a) a first stage including; (i) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor of the plurality of chemical reactors having at least;
a first reactant inlet, a second reactant inlet, a reaction volume coupled in fluid communication with the first reactant inlet and the second reactant inlet, and a product outlet, the plurality of chemical reactors being arranged in a generally concentric configuration, such that each reactor comprises an inner end and an outer end, each inner end being disposed relatively closer to a center of a circle defined by the plurality of chemical reactors than each outer end, the first reactant inlet and the second reactant inlet for each chemical reactor being disposed proximate the inner end of that reactor;(ii) a reactant feed apparatus including; (1) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to couple said first reactant inlet of each chemical reactor in parallel fluid communication with the supply of the first reactant; and (2) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to couple said second reactant inlet of each chemical reactor in parallel fluid communication with the supply of the second reactant; and (iii) a product collection assembly configured to be placed in fluid communication with a product receiver, and to couple said product outlet of each chemical reactor in fluid communication with the product receiver; and (b) a second stage including; (i) a plurality of additional chemical reactors, each additional chemical reactor in the second stage including at least an inlet and a second stage product outlet; and (ii) a second stage feed assembly configured to be placed in fluid communication with the product receiver, and to selectively couple the inlet of each additional chemical reactor in fluid communication with the product receiver, so that each additional chemical reactor is coupled in parallel with the product receiver, to enable the product collected from the first stage to be introduced as a reactant in the second stage. - View Dependent Claims (27, 28, 29, 30, 31, 32, 33, 34, 35, 36)
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37. A concentrically parallel chemical production system for producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
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(a) a first stage including; (i) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor of the plurality of chemical reactors having at least;
a first reactant inlet, a second reactant inlet, a reaction volume coupled in fluid communication with the first reactant inlet and the second reactant inlet, and a product outlet, the plurality of chemical reactors being arranged in a generally concentric configuration, such that each reactor comprises an inner end and an outer end, each inner end being disposed relatively closer to a center of a circle defined by the plurality of chemical reactors than each outer end, the first reactant inlet and the second reactant inlet for each chemical reactor being disposed proximate the inner end of that reactor;(ii) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to couple said first reactant inlet of each chemical reactor in parallel fluid communication with the supply of the first reactant; and (iii) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to couple said second reactant inlet of each chemical reactor in parallel fluid communication with the supply of the second reactant; (b) a final product collection assembly configured to couple in fluid communication with a product receiver; and (c) at least one additional stage, each additional stage including a plurality of chemical reactors arranged in a generally concentric configuration, such that; (i) a number of the plurality of chemical reactors in each additional stage is equal to a number of the plurality of reactors in the first stage, and each chemical reactor in each additional stage includes at least an inlet and a product outlet; (ii) the inlet of each chemical reactor in each additional stage is coupled in fluid communication with one of the product outlet of a corresponding chemical reactor in the first stage or the product outlet of a corresponding chemical reactor in a preceding additional stage; and (iii) the outlet of each chemical reactor in each additional stage is coupled in fluid communication with one of the inlet of a corresponding chemical reactor in a subsequent additional stage, and the final product collection assembly. - View Dependent Claims (38, 39, 40, 41, 42)
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43. An automated continuous processing parallel chemical production system for automatically producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
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(a) a first stage including; (i) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor of the plurality of chemical reactors having at least;
a first reactant inlet, a second reactant inlet, and a product outlet;(ii) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to couple the first reactant inlet of each chemical reactor in parallel fluid communication with the supply of the first reactant; and (iii) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to couple the second reactant inlet of each chemical reactor in parallel fluid communication with the supply of the second reactant; (b) a product collection assembly configured to couple in fluid communication with a product receiver; (c) at least one additional stage, each additional stage including a plurality of additional chemical reactors, such that; (i) a number of the additional chemical reactors in each additional stage is equal to a number of the plurality of reactors in the first stage, and each additional chemical reactor includes at least an inlet and a product outlet; (ii) the inlet of each additional chemical reactor in each additional stage is coupled in fluid communication with one of the product outlet of a corresponding chemical reactor in the first stage or the product outlet of a corresponding chemical reactor in a preceding additional stage; and (iii) the outlet of each additional chemical reactor in each additional stage is coupled in fluid communication with one of the inlet of a corresponding chemical reactor in a subsequent additional stage, or the product collection assembly, the product collection assembly being further configured to selectively couple each product outlet of each additional chemical reactor in a final additional stage in fluid communication with a product receiver; and (d) a system controller controllably coupled with the first reactant feed assembly, the second reactant feed assembly, and the product collection assembly, the system controller monitoring and controlling production of the desired chemical product by the plurality of chemical reactors, and designating at least one of the plurality of chemical reactors in the first stage as a backup reactor, and at least one of the plurality of additional chemical reactors in each additional stage as a backup reactor, such that the system controller causes; (i) the first reactant feed assembly to isolate the first reactant inlet of the backup reactor from the supply of the first reactant, while continuing to couple the first reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the first reactant; (ii) the second reactant feed assembly to isolate the second reactant inlet of the backup reactor from the supply of the second reactant, while continuing to couple the second reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the second reactant; and (iii) the product collection assembly to isolate the product outlet of each additional chemical reactor in the final additional stage that is designated as a backup reactor from a product receiver, while continuing to couple the product outlet of each other additional chemical reactor in the final additional stage in fluid communication with a product receiver.
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44. An automated continuous processing parallel chemical production system for automatically producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
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(a) a first stage including; (i) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor of the plurality of chemical reactors having at least;
a first reactant inlet, a second reactant inlet, and a product outlet;(ii) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to couple the first reactant inlet of each chemical reactor in parallel fluid communication with the supply of the first reactant; and (iii) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to couple the second reactant inlet of each chemical reactor in parallel fluid communication with the supply of the second reactant; (b) a second stage including a plurality of additional chemical reactors, such that; (i) there are at least as many additional chemical reactors in the second stage as there are chemical reactors in the first stage; and (ii) each additional chemical reactor in the second stage includes at least;
an inlet and a second stage product outlet, each additional chemical reactor inlet being configured to receive a product produced in the first stage and to use the product as a reactant to produce a second stage product;(c) a product collection assembly configured to couple the second stage product outlet of each chemical reactor in the second stage in fluid communication with a product receiver; and (d) a system controller controllably coupled with the first reactant feed assembly, the second reactant feed assembly, and the product collection assembly, the system controller monitoring and controlling production of the desired chemical product by the plurality of chemical reactors, and designating at least one of the plurality of chemical reactors in the first stage as a backup reactor, and at least one of the plurality of additional chemical reactors in the second stage as a backup reactor, such that the system controller causes; (i) the first reactant feed assembly to isolate the first reactant inlet of the backup reactor from the supply of the first reactant, while continuing to couple the first reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the first reactant; (ii) the second reactant feed assembly to isolate the second reactant inlet of the backup reactor from the supply of the second reactant, while continuing to couple the second reactant inlet of each other chemical reactor in parallel fluid communication with the supply of the second reactant; and (iii) the product collection assembly to isolate the second stage product outlet of the second stage backup reactor from the product receiver, while continuing to couple the second stage product outlet of each other additional chemical reactor in the second stage in fluid communication with the product receiver. - View Dependent Claims (45, 46, 47, 48, 49)
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50. A concentrically parallel chemical production system for producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
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(a) a first stage including; (i) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor of the plurality of chemical reactors having at least;
a first reactant inlet, a second reactant inlet, a reaction volume coupled in fluid communication with the first reactant inlet and the second reactant inlet, and a product outlet, the plurality of chemical reactors being arranged in a generally concentric configuration, such that each reactor comprises an inner end and an outer end, each inner end being disposed relatively closer to a center of a circle defined by the plurality of chemical reactors than each outer end, the first reactant inlet and the second reactant inlet for each chemical reactor being disposed proximate the inner end of that reactor; and(ii) a reactant feed apparatus including; (1) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to couple said first reactant inlet of each chemical reactor in parallel fluid communication with the supply of the first reactant; and (2) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to couple said second reactant inlet of each chemical reactor in parallel fluid communication with the supply of the second reactant; and (b) a second stage including a plurality of additional chemical reactors and a product collection assembly, the plurality of additional chemical reactors and the product collection assembly being configured such that; (i) a number of the additional chemical reactors in the second stage is equal to a number of the plurality of reactors in the first stage; (ii) each additional chemical reactor in the second stage includes at least;
an inlet, and a second stage product outlet;(iii) the product collection assembly is configured to be placed in fluid communication with a product receiver, and to couple the second stage product outlet of each chemical reactor in the second stage in fluid communication with the product receiver; and (iv) each product outlet of each chemical reactor in the first stage is coupled to the inlet of a different one of the additional chemical reactors in the second stage, such that each additional chemical reactor in the second stage is coupled with only one chemical reactor in the first stage.
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51. A concentrically parallel chemical production system for producing a desired chemical product by combining at least two reactants, the chemical production system comprising:
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(a) a first stage including; (i) a plurality of chemical reactors, each chemical reactor being configured to produce a quantity of the desired chemical product, each chemical reactor of the plurality of chemical reactors having at least;
a first reactant inlet, a second reactant inlet, a reaction volume coupled in fluid communication with the first reactant inlet and the second reactant inlet, and a product outlet, the plurality of chemical reactors being arranged in a generally concentric configuration, such that each reactor comprises an inner end and an outer end, each inner end being disposed relatively closer to a center of a circle defined by the plurality of chemical reactors than each outer end, the first reactant inlet and the second reactant inlet for each chemical reactor being disposed proximate the inner end of that reactor; and(ii) a reactant feed apparatus including; (1) a first reactant feed assembly configured to be placed in fluid communication with a supply of a first reactant, and to couple said first reactant inlet of each chemical reactor in parallel fluid communication with the supply of the first reactant; and (2) a second reactant feed assembly configured to be placed in fluid communication with a supply of a second reactant, and to couple said second reactant inlet of each chemical reactor in parallel fluid communication with the supply of the second reactant; (b) a second stage including a plurality of additional chemical reactors and a product collection assembly, the plurality of additional chemical reactors and the product collection assembly being configured such that; (i) a number of the additional chemical reactors in the second stage is equal to a number of the plurality of reactors in the first stage; (ii) each additional chemical reactor in the second stage includes at least;
an inlet, and a second stage product outlet;(iii) the product collection assembly is configured to be placed in fluid communication with a product receiver, and to couple the second stage product outlet of each chemical reactor in the second stage in fluid communication with the product receiver; and (iv) each product outlet of each chemical reactor in the first stage is coupled to the inlet of a different one of the additional chemical reactors in the second stage, such that each additional chemical reactor in the second stage is coupled with only one chemical reactor in the first stage; and (c) a valve system disposed in fluid communication with the outlet of each of the plurality of chemical reactors in the first stage, and the inlet of each of the plurality of additional chemical reactors in the second stage, the valve system enabling the selective coupling of the product outlet of each chemical reactor in the first stage to the inlet of a selected additional chemical reactor in the second stage.
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Specification