Microstructured optical fibers and methods

• US 7,450,806 B2
• Filed: 10/18/2006
• Issued: 11/11/2008
• Est. Priority Date: 11/08/2005
• Status: Expired due to Fees

• Current Assignee: Corning Incorporated
• Original Assignee: Corning Incorporated
• Inventors: Li, Ming-Jun, Bookbinder, Dana Craig, Tandon, Pushkar, Fiacco, Richard Michael, Murtagh, Michael Thomas
• Primary Examiner(s): Healy; Brian
• Assistant Examiner(s): Anderson; Guy G
• Application Number:
  US11/583,098
• Publication Number:
  US 20070104437A1
• Time in Patent Office: 755 Days
• Field of Search: 385123-128, 385/28, 385/11, 385/164, 398/164
• US Class Current: 385/125
• CPC Class Codes: C03B 2201/02 Pure silica glass, e.g. pure fused quartz
• CPC Class Codes: C03B 2201/31 doped with germanium
• CPC Class Codes: C03B 2203/14 Non-solid, i.e. hollow products, e.g. hollow clad or with core-clad interface
• CPC Class Codes: C03B 2203/42 Photonic crystal fibres, e.g. fibres using the photonic bandgap PBG effect, microstructured or holey optical fibres
• CPC Class Codes: C03B 37/01446 Thermal after-treatment of preforms, e.g. dehydrating, consolidating, sintering C03B37/01853 takes precedence
• CPC Class Codes: C03B 37/02781 Hollow fibres, e.g. holey fibres
• CPC Class Codes: C03C 13/00 Fibre or filament compositions manufacture of fibres or filaments C03B37/00
• CPC Class Codes: C03C 13/04 Fibre optics, e.g. core and clad fibre compositions light guides G02B6/00
• CPC Class Codes: G02B 1/048 characterised by the cladding material
• CPC Class Codes: G02B 6/02333 Core having higher refractive index than cladding, e.g. solid core, effective index guiding
• CPC Class Codes: G02B 6/02357 Property of longitudinal structures or background material varies radially and/or azimuthally in the cladding, e.g. size, spacing, periodicity, shape, refractive index, graded index, quasiperiodic, quasicrystals

Abstract

Microstructured optical fiber and method of making. Glass soot is deposited and then consolidated under conditions which are effective to trap a portion of the consolidation gases in the glass to thereby produce a non-periodic array of voids which may then be used to form a void containing cladding region in an optical fiber. Preferred void producing consolidation gases include nitrogen, argon, CO₂, oxygen, chlorine, CF₄, CO, SO₂ and mixtures thereof.

Claims

1. A microstructured optical fiber comprising:

a core region having a first refractive index and a cladding region having a second refractive index which is lower than that of the core region such that the light which is to be transmitted through the fiber is retained generally within the core, wherein the cladding comprises at least one region in the cladding comprised of a plurality of non-periodically located closed voids, such that when viewed in cross section said voids are distributed across said cross section, greater than 95 percent of the voids having a maximum diameter of 1550 nm or less, said fiber exhibiting an attenuation at at least one wavelength between 600 and 1550 nm which is less than 500 dB/km, wherein cross sections of said fiber taken at different points along the length of the fiber will exhibit different randomly oriented void patterns and different randomly oriented void sizes.

2. The microstructured optical fiber of claim 1, wherein said fiber is single moded at 1550 nm and greater than 95 percent of the voids in said fiber have a maximum diameter of 775 nm or less.

3. The optical fiber of claim 1, wherein said fiber exhibits an attenuation of less than 200 dB/km at 1550.

4. The optical fiber of claim 3, wherein the entire void containing region in the cladding of said fiber exhibits a regional void area percent of greater than about 0.5 percent and less than about 20 percent.

5. The optical fiber of claim 1, wherein said voids are contained only in said cladding, and region containing non-periodically distributed holes is spaced apart from the core.

6. The optical fiber of claim 3, wherein at least a portion of the cladding of said fiber within a 10 micron distance from said core exhibits a regional void area percent greater than about 1.0 percent.

7. The optical fiber of claim 1, wherein said core comprises germanium.

8. The optical fiber of claim 3, wherein said core comprises germanium.

9. The microstructured optical fiber of claim 7, wherein said fiber exhibits an increase in attenuation at 1550 nm when bent around a 10 mm diameter mandrel, which is less than 20 dB/turn.

10. The microstructured optical fiber of claim 1, wherein the maximum diameter of each one of said voids is less than 375 nm.

32. The microstructed optical fiber of claim 1, wherein said fiber exhibits different cross-sectional patterns of said voids at different points along the length of the fiber.

33. The microstructured optical fiber of claim 1, wherein at least some of the voids extend less than a few meters along the length of the fiber.

34. The microstructured optical fiber of claim 1, wherein said fiber exhibits less than 500 of said non-periodically located voids when viewed in cross section.

35. The microstructured optical fiber of claim 1, wherein said voids do not extend the entire length of said fiber.

36. The microstructured optical fiber of claim 1, wherein substantially all of the voids in the fiber cross-section are non-periodically located with respect to the other of said voids.

37. The microstructured optical fiber of claim 1, wherein said fiber exhibits an attenuation less than 0.2 dB/km at 1550 nm.

38. The microstructured optical fiber of claim 1, wherein said voids comprise krypton gas therein.

39. The microstructured optical fiber of claim 1, wherein said fiber exhibits a total fiber void area less than 5 percent.

11. A microstructured optical fiber comprising:

a core region having a first refractive index and a cladding region having a second refractive index which is lower than that of the core region such that the light which is to be transmitted through the fiber is retained generally within the core region, wherein said cladding comprises a void containing region in the cladding which when viewed in cross section is comprised of a plurality of non-periodically located voids distributed within said cladding, wherein said fiber exhibits different cross-sectional patterns of said voids at different points along the length of the fiber, and wherein at least 95% of the voids in said void containing region have a maximum diameter of 1550 nm or less, wherein the fiber exhibits a total fiber void area percent which is greater than 0.01 percent.

12. The microstructured optical fiber of claim 11, said region having a width of less than 40 microns and comprised of closed voids, wherein said fiber is single moded at 1550 nm and exhibits a total fiber void area percent which is less than 10 percent, and the relative void area percent is maintained consistently along the length of the fiber.

13. The microstructured optical fiber of claim 11, wherein the voids in said void containing region exhibit a mean diameter of less than 1550 nm, and a standard deviation of said holes is less than 1 micron and the fiber exhibits a total fiber void area percent less than 5 percent.

14. The microstructured optical fiber of claim 11, wherein said fiber exhibits an increase in attenuation at 1550 nm when bent around a 10 mm diameter mandrel, which is less than 20 dB/turn.

15. The microstructured optical fiber of claim 12, wherein said void containing region is spaced apart from said core.

16. The microstructured optical fiber of claim 11, wherein said void containing region comprises at least 25 holes, and the mean diameter of the holes in said void containing region is less than 2000 nm.

17. The microstructured optical fiber of claim 11, wherein said void containing region comprises at least 25 holes, and the mean diameter of the holes in said void containing region is less than 775 nm.

40. The microstructured optical fiber of claim 11, wherein said fiber exhibits less than 500 of said non-periodically located voids when viewed in cross section.

41. The microstructured optical fiber of claim 11, wherein substantially all of the voids in the fiber cross-section are non-periodically located with respect to the other of said voids.

42. The microstructured optical fiber of claim 11, wherein said fiber exhibits an attenuation less than 0.2 dB/km at 1550 nm.

43. The microstructured optical fiber of claim 11, wherein said voids comprise krypton gas therein.

18. A microstructured optical fiber comprising:

a core region having a first refractive index and a cladding region having a second refractive index which is lower than that of the core region such that the light which is to be transmitted through the fiber is retained generally within the core region, wherein said cladding comprises a region in the cladding which surrounds the core region and when said fiber is viewed in cross-section said region is comprised of non-periodically distributed voids which do not extend the length of the fiber, said voids contain gas which was trapped during a fiber preform soot consolidation step used to manufacture said fiber, said voids having a mean diameter less than about 2000 nm and a standard deviation less than about 750 nm, wherein said void containing region is spaced apart from the core region of said fiber, and wherein said fiber exhibits a total fiber void area percent less than 5 percent.

19. The microstructured optical fiber of claim 18, wherein said hole containing region comprises between about 25 and 200 holes.

20. The microstructured optical fiber of claim 18, wherein the mean diameter of the holes in said hole containing region is less than 775 nm.

21. The microstructured optical fiber of claim 18, wherein said fiber is single moded at 1550 nm and exhibits an increase in attenuation at 1550 nm when bent around a 10 mm diameter mandrel, which is less than 20 dB/turn.

22. The microstructured optical fiber of claim 18, wherein said fiber exhibits an increase in attenuation at 1550 nm when bent around a 10 mm diameter mandrel, which is less than 15 dB/turn.

23. A microstructured optical fiber which is multimoded at 1550 nm, said fiber comprising;

a core region having a first refractive index and a cladding region having a second refractive index which is lower than that of the core region such that the light which is to be transmitted through the fiber is retained generally within the core, wherein the cladding comprises at least one region in the cladding which is comprised of a plurality of non-periodically located voids, said fiber is multimoded at 1550 nm and exhibits an increase in attenuation at 1550 nm, when said fiber is wrapped once around a mandrel having a radius of 5 mm, which is less than 1 dB/turn, wherein different cross-sectiontaken along the length of the fiber exhibit different randomly oriented patterns of said voids.

24. The microstructured optical fiber of claim 23, whereinsaid region comprises 85 or more holes when viewed in cross-section.

25. The microstructured optical fiber of claim 23, wherein at least some of the voids extend less than a few meters along the length of the fiber.

26. The microstructured optical fiber of claim 23, wherein said fiber exhibits less than 500 of said non-periodically located voids when viewed in cross section.

27. The microstructured optical fiber of claim 23, wherein said voids do not extend the entire length of said fiber.

28. The microstructured optical fiber of claim 23, wherein substantially all of the voids in the fiber cross-section are non-periodically located with respect to the other of said voids.

29. The microstructured optical fiber of claim 23, wherein said fiber exhibits an attenuation less than 0.2 dB/km at 1550 nm.

30. The microstructured optical fiber of claim 23, wherein said voids comprise krypton gas therein.

31. The microstructured optical fiber of claim 23, wherein said fiber exhibits a total fiber void area less than 5 percent.

44. The microstructured optical fiber of claim 23, wherein said fiber exhibits a total fiber void area less than 5 percent.

45. A microstructured optical fiber comprising:

a solid glass core region having a first refractive index and a cladding region having a second refractive index which is lower than that of the core region such that the light which is to be transmitted through the fiber is retained generally within the core, wherein the cladding comprises at least one region in the cladding comprised of a plurality of non-periodically located closed voids, said voids containing krypton gas therein.