NMR Probe

• US 7,456,631 B1
• Filed: 08/20/2007
• Issued: 11/25/2008
• Est. Priority Date: 08/14/2007
• Status: Active Grant

• Current Assignee: JEOL Limited
• Original Assignee: JEOL Limited
• Inventors: Shino, Hideo
• Primary Examiner(s): Vargas; Dixomara
• Application Number:
  US11/841,318
• Time in Patent Office: 463 Days
• Field of Search: 324300-322, 600410-435, 333219-235, 343825-831, 343/844
• US Class Current: 324/322
• CPC Class Codes: G01R 33/34046 Volume type coils, e.g. bird-cage coils; Quadrature bird-cage coils; Circularly polarised coils
• CPC Class Codes: G01R 33/34053 Solenoid coils; Toroidal coils
• CPC Class Codes: G01R 33/34069 Saddle coils
• CPC Class Codes: G01R 33/34092 RF coils specially adapted for NMR spectrometers
• CPC Class Codes: G01R 33/3628 Tuning/matching of the transmit/receive coil

Abstract

An NMR (nuclear magnetic resonance) probe is offered which produces a magnetic field strength adapted for producing an NMR signal within a sample coil. The probe has a resonant circuit including a sample coil, a first transmission line, and a second transmission line. The resonant circuit is designed taking account of the transmission line length L_s of the coil, the transmission line length L_a of the first line, and the transmission line length L_b of the second line. The coil is placed in a position where the magnetic field strength is maximized. Where the electrical characteristics of the resonant circuit are varied by connection of the coil and transmission lines, the transmission line lengths are corrected according to the variations.

Claims

1. An NMR probe comprising:

a resonant circuit resonating with first RF waves, the resonant circuit including a sample coil having a first and a second ends, a first transmission line having a first end and a second end grounded, and a second transmission line having a first end and a second end grounded, the sample coil being made of a conductor, the first end of the first transmission line being connected with the first end of the sample coil, the first end of the second transmission line being connected with the second end of the sample coil;

a first connector for entering and extracting the first RF waves; and

a first matching circuit connected between the first connector and the resonant circuit;

wherein the total transmission line length of the conductor of the sample coil, the first transmission line, and the second transmission line is set to a value at which standing waves given by

λ

+(n−

1)×

λ

/2

are produced, where % is the wavelength of the first RF waves applied to the resonant circuit and n is a positive integer; and

wherein the sample coil is placed at a position where the strength of a produced magnetic field is maximized.

5. An NMR probe as set forth in any one of claims 1, 2, and 4, further including a first impedance circuit, and wherein said second end of said first transmission line is grounded via the first impedance circuit.

6. An NMR probe as set forth in claim 5, further including a second impedance circuit, and wherein said second end of said second transmission line is grounded via the second impedance circuit.

7. An NMR probe as set forth in any one of claims 1 to 4, further including a first and a second coupling circuits, wherein said first coupling circuit couples said first end of the sample coil to said first end of the first transmission line and said second coupling circuit couples said second end of the sample coil to said first end of the second transmission line.

8. An NMR probe as set forth in any one of claims 1 to 4, wherein at least one of said first and second transmission lines includes reactance elements.

9. An NMR probe as set forth in any one of claims 1 to 4, further including a second connector for entering and extracting second RF waves and a second matching circuit connected between the second connector and said resonant circuit.

10. An NMR probe as set forth in any one of claims 1 to 4, further including a third connector for entering and extracting third RF waves and a third matching circuit connected between the third connector and said resonant circuit.

11. An NMR probe as set forth in any one of claims 1 to 4, wherein at least one of said first and second transmission lines is a coaxial cable having an outer conductor layer.

12. An NMR probe as set forth in any one of claims 1 to 4, wherein there is provided a coaxial cable having an inner conductor and an outer conductor layer, and wherein one of said first and second transmission lines is said inner conductor, while the other is said outer conductor layer.

2. An NMR probe comprising:

a resonant circuit resonating with first RF waves, the resonant circuit including a sample coil having a first and a second ends, a first transmission line having a first end and a second end grounded, and a second transmission line having a first end and a second end electrically opened, the sample coil being made of a conductor, the first end of the first transmission line being connected with the first end of the sample coil, the first end of the second transmission line being connected with the second end of the sample coil;

a first connector for entering and extracting the first RF waves; and

a first matching circuit connected between the first connector and the resonant circuit;

wherein the total transmission line length of the conductor of the sample coil, the first transmission line, and the second transmission line is set to a value at which standing waves given by

(¾

)λ

+(n−

1)×

λ

/2

are produced, where λ

is the wavelength of the first RF waves applied to the resonant circuit and n is a positive integer; and

wherein the sample coil is placed at a position where the strength of a produced magnetic field is maximized.

3. An NMR probe comprising:

a resonant circuit resonating with first RF waves, the resonant circuit including a sample coil having a first and a second ends, a first transmission line having a first end and a second end electrically opened, and a second transmission line having a first end and a second end electrically opened, the sample coil being made of a conductor, the first end of the first transmission line being connected with the first end of the sample coil, the first end of the second transmission line being connected with the second end of the sample coil;

a first connector for entering and extracting the first RF waves; and

a first matching circuit connected between the first connector and the resonant circuit;

wherein the total transmission line length of the conductor of the sample coil, the first transmission line, and the second transmission line is set to a value at which standing waves given by (n/2)λ

are produced, where λ

is the wavelength of the first RF waves applied to the resonant circuit and n is a positive integer; and

wherein the sample coil is placed at a position where the strength of a produced magnetic field is maximized.

4. An NMR probe comprising:

a resonant circuit resonating with first RF waves, the resonant circuit including a sample coil having a first and a second ends, a first transmission line having a first end connected with the first end of the sample coil, and a second transmission line having a first end connected with the second end of the sample coil, the sample coil being made of a conductor, second ends of the first and second transmission lines being connected together;

a first connector for entering and extracting the first RF waves; and

a first matching circuit connected between the first connector and the resonant circuit;

wherein the total transmission line length of the conductor of the sample coil, the first transmission line, and the second transmission line is set to a value at which standing waves given by nλ

are produced, where λ

is the wavelength of the first RF waves applied to the resonant circuit and n is a positive integer; and

wherein the sample coil is placed at a position where the strength of a produced magnetic field is maximized.