Process for the extraction and preparation of bast fibers, bast fibers obtained therefrom and their use

• US 7,481,843 B2
• Filed: 10/31/2006
• Issued: 01/27/2009
• Est. Priority Date: 11/01/2005
• Status: Active Grant

• Current Assignee: Meirong Xu
• Original Assignee: Meirong Xu
• Inventors: Xu, Meirong
• Primary Examiner(s): Sample; David R
• Assistant Examiner(s): HAMMER, KATIE L
• Application Number:
  US11/555,134
• Publication Number:
  US 20070094810A1
• Time in Patent Office: 819 Days
• Field of Search: 811/551, 810/1, 810/7, 810/81, 810/9, 811/1, 536/2, 435/275, 435/277, 435/278, 435/279, 435/917
• US Class Current: 8/116.1
• CPC Class Codes: D01C 1/02 by chemical methods to obtain bast fibres
• CPC Class Codes: D06L 4/70 Multi-step processes
• CPC Class Codes: Y10T 428/298 Physical dimension

Abstract

The present invention generally relates to a process for the extraction and preparation of bast fibers with high quality and high counts. The process is suitable for ramie, hemp and flax. The present invention also relates to bast fibers with high counts produced according to the process, as well as pure yarns and mixed, blended yarns made from said bast fibers.

Claims

1. A process for the extraction and preparation of bast fibers, comprises ramie, hemp or flax is subjected to two times of bleaching, two times of alkali boiling, and a step of high-temperature loosening, wherein the two times of bleaching are chlorine bleaching and oxygen bleaching respectively, and in the chlorine bleaching, sodium hypochlorite having a concentration of 3-8 g/L is used, the temperature is 35-45°

C., and the duration is 40-80 minutes;

in the oxygen bleaching, hydrogen peroxide of 4-6 g/L is used, the temperature is 80-100°

C., and the duration is 40-80 minutes;

in the alkali boilings, the first alkali boiling is performed by use of caustic soda;

high-temperature loosening is performed after the bleaching and boiling, and in the high-temperature loosening, soda of 100-140 g/L is used, the temperature is 100-140°

C., and the duration is 1.5-2.5 hours.

2. The process as claimed in claim 1, wherein said bast fibers are ramie fibers, said process comprises the following steps in order:

pickling→

washing with water→

boiling for the first time→

washing with water→

bleaching for the first time→

washing with acid→

boiling for the second time→

washing with water→

bleaching for the second time→

loosening at high temperature→

washing with water→

oiling→

dehydrating→

drying;

wherein,

in pickling, sulfuric acid is used and controlled to have a concentration of 2-10 g/L, the temperature is 40-60°

C., and the duration is 1-2 hours;

both the first boiling and the second boiling are alkali boiling with the same conditions which are 50-150 g/L of caustic soda, 1.5-2 hours of duration and 90-140°

C. of temperature;

bleaching is performed twice, and in the first bleaching, sodium hypochlorite having a concentration of 3-8 g/L is used, the temperature is 35-45°

C., and the duration is 40-80 minutes;

in the second bleaching, hydrogen peroxide of 4-6 g/L is used, the temperature is 80-100°

C., and the duration is 40-80 minutes;

in the high-temperature loosening, soda of 100-140 g/L is used, the temperature is 100-140°

C., and the duration is 1.5-2.5 hours;

oiling is performed with vegetable oil in an amount of 1-2% by weight of fiber mass;

the technical bath ratio in the above steps is 1;

10-20.

3. The process as claimed in claim 2, characterized in that,

in pickling, the concentration of sulfuric acid is controlled to be 4-8 g/L, the temperature is controlled to be 45-55°

C., and the duration is controlled to be 75-110 minutes;

the conditions of alkali boiling are controlled to be 70-120 g/L of caustic soda, 100-115 minutes of duration and 110-130°

C. of temperature;

in the first bleaching, sodium hypochlorite having a concentration of 4-7 g/L is used, the temperature is 35-45°

C., and the duration is 50-70 minutes;

in the second bleaching, hydrogen peroxide of 4-6 g/L is used, the temperature is 80-100°

C., and the duration is 55-75 minutes;

in the high-temperature loosening, soda of 110-130 g/L is used, the temperature is 110-135°

C., and the duration is 100-140 minutes.

4. The process as claimed in claim 1, wherein said bast fibers are flax or hemp fibers, said process comprises the following steps in order:

purification→

pickling→

washing with water→

bleaching for the first time→

boiling for the first time→

washing with water→

bleaching for the second time→

boiling for the second time→

loosening at high temperature→

washing with water→

oiling→

dehydrating→

drying;

wherein,

in pickling and purification, 2-10 g/L of sulfuric acid is used, the temperature is 40-60°

C., and the duration is 1-2 hours;

both the first boiling and the second boiling are alkali boiling with the conditions of the first boiling to be 25-100 g/L of caustic soda, 1-1.5 hours of duration and 60-90°

C. of temperature;

bleaching is performed twice, and in the first bleaching, sodium hypochlorite having a concentration of 3-8 g/L is used, the temperature is 35-45°

C., and the duration is 40-80 minutes;

in the second boiling, 60-90 g/L of soda is used, the duration is 1-1.5 hours, and the temperature is 100-130°

C.;

in the second bleaching, hydrogen peroxide of 4-6 g/L is used, the temperature is 80-100°

C., and the duration is 40-80 minutes;

in the high-temperature loosening, soda of 100-140 g/L is used, the temperature is 100-140°

C., and the duration is 1.5-2.5 hours;

oiling is performed with vegetable oil in an amount of 1-2% by weight of fiber mass;

the technical bath ratio in the above steps is 1;

10-20.

5. The process as claimed in claim 4, characterized in that,

the conditions of the first boiling are controlled to be 40-80 g/L of caustic soda, 70-85 minutes of duration and 70-85°

C. of temperature;

in the first bleaching, sodium hypochlorite having a concentration of 4-7 g/L is used, the temperature is 35-45°

C., and the duration is 50-70 minutes;

in the second bleaching, hydrogen peroxide of 4-6 g/L is used, the temperature is 80-100°

C., and the duration is 55-75 minutes;

in the second boiling, soda is used in an amount of 70-85 g/L, the duration is 70-85 minutes, and the temperature is 110-130°

C.;

in the high-temperature loosening, soda of 110-130 g/L is used, the temperature is 110-135°

C., and the duration is 100-140 minutes.