Method and system for corn fractionation

• US 7,569,671 B2
• Filed: 01/06/2006
• Issued: 08/04/2009
• Est. Priority Date: 01/06/2005
• Status: Active Grant

• Current Assignee: Board of Trustees of The University of Illinois
• Original Assignee: Board of Trustees of The University of Illinois
• Inventors: Cheryan, Munir
• Primary Examiner(s): Monshipouri; Maryam
• Assistant Examiner(s): Tsay; Marsha M
• Application Number:
  US11/327,166
• Publication Number:
  US 20060173169A1
• Time in Patent Office: 1,306 Days
• Field of Search: 530/373, 426/601
• US Class Current: 530/376
• CPC Class Codes: A23K 20/147 Polymeric derivatives, e.g. peptides or proteins
• CPC Class Codes: A23L 7/115 Cereal fibre products, e.g. bran, husk
• CPC Class Codes: C08B 30/044 from corn or maize
• CPC Class Codes: C11B 1/10 by extracting
• CPC Class Codes: C11B 1/108 after-treatment, e.g. of miscellae

Abstract

Methods and apparatus for processing corn into one or more corn products. Oil is extracted from corn or corn products or by-products with a solvent. The corn-solvent mixture is separated into streams, one of which preferably includes an extract containing at least oil and solvent, and another containing de-oiled corn solids and adsorbed solvent. The solvent is separated from oil, and the de-oiled, desolventized corn solids are processed to provide one or more corn products.

Claims

1. A process for fractionation of corn, the process comprising the steps of:

preparing the corn for extraction;

without separating germ from the prepared corn, extracting oil from the prepared corn with a solvent to provide an extracted corn-solvent mixture;

separating the extracted corn-solvent mixture into at least two streams, one including an extract comprising the oil and the solvent, and the other comprising de-oiled corn solids and adsorbed solvent;

membrane processing the extract to separate the solvent from the oil;

desolventizing the de-oiled corn solids from the other stream to substantially remove the solvent and provide-deoiled, desolventized corn solids;

resuspending said de-oiled, desolventized corn solids in water; and

separating one or more of fiber, starch and protein from the suspended de-oiled, desolventized corn solids to produce one or more corn products.

2. The process of claim 1 wherein the solvent comprises at least one of a hydrocarbon, an alcohol, hydrocarbon combined with water, and an alcohol combined with water.

3. The process of claim 1 wherein said separating the extracted corn-solvent mixture comprises at least one of centrifugation, filtration, and membrane filtration.

4. The process of claim 1

wherein the extract comprising the oil and solvent is pretreated with an ultrafiltration membrane, and

wherein the process further comprises nanofiltering a permeate from the ultrafiltration membrane to recover oil and solvent.

5. The process of claim 1 further comprising:

separating fiber from the resuspended desolventized, de-oiled corn solids; and

washing the separated fiber.

6. The process of claim 5 further comprising:

dewatering and drying the separated and washed fiber.

7. The process of claim 6 wherein the wash water from said fiber dewatering is membrane filtered to recover protein and starch.

8. The process of claim 6

wherein the de-oiled, desolventized corn solids after said fiber separating comprise a suspension including substantially starch and protein in water, and

wherein the process further comprises dewatering and thickening the separated fiber by at least one of a centrifuge, a membrane microfilter, and a membrane ultrafilter.

9. The process of claim 8 wherein the suspension is separated into crude starch and protein fractions.

10. The process of claim 9 further comprising:

washing and purifying the crude starch using water.

11. The process of claim 10 wherein said washing and purifying uses at least one of a hydrocyclone and a membrane microfilter.

12. The process of claim 11, further comprising:

passing the wash water from said starch purifying through at least one of a membrane, a reverse osmosis membrane, a nanofiltration membrane, an ultrafiltration membrane and a microfiltration membrane, to recover clean water and permeate and concentrated solids.

13. The process of claim 12 wherein the clean water permeate from said passing is recycled to upstream operations.

14. The process of claim 13 further comprising:

recycling retained solids from said passing to upstream operations to recover the solids.

15. The process of claim 9 further comprising:

thickening the separated protein fraction in a gluten thickener;

wherein the gluten thickener includes at least one of a centrifuge, a membrane microfilter, and an ultrafilter designed to retain substantially all proteins and starch.

16. The process of claim 15 wherein said thickening uses a centrifuge, and wherein the overflow from the centrifuge is sent to at least one of a membrane microfilter, an ultrafilter, and a nanofilter to recover substantially all the protein.

17. The process of claim 15

wherein said thickening uses a gluten filter;

and

wherein the process further comprises membrane processing a filtrate from the gluten filter using at least one of reverse osmosis, nanofiltration, ultrafiltration, and microfiltration to recover protein.

18. The process of claim 1

wherein said preparing comprises reducing a particle size of the corn;

wherein the prepared corn is not steeped before said extracting oil.