Mass transfer apparatus and method

• US 7,628,924 B2
• Filed: 10/21/2005
• Issued: 12/08/2009
• Est. Priority Date: 10/22/2004
• Status: Expired due to Fees

• Current Assignee: Muddy River Technologies, Inc.
• Original Assignee: Muddy River Technologies, Inc., Nels Robert Ladouceur
• Inventors: Ladouceur, Nels Robert, Jack, Peter Douglas
• Primary Examiner(s): Lithgow; Thomas M
• Application Number:
  US11/254,809
• Publication Number:
  US 20060086669A1
• Time in Patent Office: 1,509 Days
• Field of Search: 210/703, 210/706, 210/760, 210/750, 210/741, 210/221.2, 210/188, 261/79.2
• US Class Current: 210/703
• CPC Class Codes: B01F 23/2319 Methods of introducing gases into liquid media
• CPC Class Codes: B01F 23/232 using flow-mixing means for introducing the gases, e.g. baffles
• CPC Class Codes: B01F 23/29 Mixing systems, i.e. flow charts or diagrams
• CPC Class Codes: B01F 25/10 Mixing by creating a vortex flow, e.g. by tangential introduction of flow components
• CPC Class Codes: C02F 1/24 by flotation C02F1/465 takes precedence
• CPC Class Codes: C02F 1/38 by centrifugal separation
• CPC Class Codes: C02F 1/727 using pure oxygen or oxygen rich gas
• CPC Class Codes: C02F 1/78 with ozone C02F1/4672 takes precedence
• CPC Class Codes: C02F 2201/784 Diffusers or nozzles for ozonation
• CPC Class Codes: C02F 2209/005 Processes using a programmable logic controller [PLC]
• CPC Class Codes: C02F 2209/03 Pressure

Abstract

The invention relates to an apparatus and method for more effectively dissolving a gas into a liquid stream. A gas is introduced into a liquid stream, at atmospheric pressure, to create a mixed/dissolved stream. The mixed/dissolved stream is then pressurized to an elevated pressure and directed into a hydrocyclone where the gas is further dissolved and more thoroughly distributed in the liquid thereby creating a more intimately mixed/dissolved stream. The intimately mixed/dissolved stream is then directed to a pressure retention vessel where the liquid is held at a predetermined pressure for a predetermined time period for effectively treating, disinfecting and/or clarifying said intimately mixed/dissolved stream. The treated intimately mixed/dissolved stream can then be directed to further processing steps.

Claims

1. A mass transfer apparatus for dissolving a gas into a liquid stream, comprising:

means for introducing a gas into a liquid stream to create a mixed stream;

a pump having an inlet for receiving the mixed stream of liquid and gas, and an outlet;

for discharging said mixed stream at an elevated pressure;

at least one hydrocyclone connected downstream from said pump outlet;

for shearing and more thoroughly mixing and dissolving said gas into said mixed/dissolved stream creating a more intimately mixed/dissolved stream, said at least one hydrocyclone having at least one inlet for receiving said pressurized mixed stream, and an outlet;

for discharging said more intimately mixed/dissolved stream;

a pressure retention vessel connected downstream from said hydrocyclone for holding said intimately mixed/dissolved stream at a predetermined pressure for a predetermined time period for effectively treating, disinfecting and/or clarifying said intimately mixed/dissolved stream, thereby creating a treated stream, said pressure retention vessel having an inlet for receiving said intimately mixed/dissolved stream from said hydrocyclone, a first outlet;

for discharging said treated stream, and a second outlet;

for discharging residual gas;

pressure control means in communication with said at least one hydrocyclone and said pressure retention vessel for adjusting the pressure of said mixed and intimately mixed/dissolved streams to ensure effective dissolution of said gas within said liquid stream; and

means, in communication with said pressure retention vessel, for reducing the pressure downstream from said pressure retention vessel as said treated stream is released therefrom;

wherein said at least one hydrocyclone comprises;

a housing vessel equipped with said at least one hydrocyclone inlet and said hydrocyclone outlet;

a hydrocyclone liner contained in said housing vessel, said liner having an upper neck portion and a lower outlet portion, said lower outlet portion being in communication with said outlet of said housing vessel, and said liner having a internal diameter that reduces from said upper neck portion towards said lower outlet portion; and

a spin inducer attached to the upper neck portion of said hydrocyclone liner and in communication with the at least one inlet of said hydrocyclone for inducing circular flow to the mixed stream as it enters said hydrocyclone.

2. A method for dissolving a gas into a liquid stream;

comprising the steps of;

injecting a gas at atmospheric pressure via a gas feed line into a liquid stream to create a mixed stream;

pressurizing said mixed stream;

to a predetermined level;

directing said mixed stream;

into a hydrocyclone to create a more intimately mixed/dissolved stream;

directing said intimately mixed/dissolved stream;

from the hydrocyclone to a pressure retention vessel, and holding said intimately mixed/dissolved stream;

in said pressure retention vessel at a predetermined pressure for a predetermined time period for effectively treating, disinfecting and/or clarifying said intimately mixed/dissolved stream thereby creating a treated stream;

wherein said hydrocyclone comprises;

a housing vessel equipped with at least one hydrocyclone inlet and outlet;

a hydrocyclone liner contained in said housing vessel, said liner having an upper neck portion and a lower outlet portion, said lower outlet portion being in communication with said outlet of said housing vessel, and said liner having a internal diameter that reduces from said upper neck portion towards said lower outlet portion; and

a spin inducer attached to the upper neck portion of said hydrocyclone liner and in communication with the at least one inlet of said hydrocyclone for inducing circular flow to the mixed stream as it enters said hydrocyclone.

3. The method according to claim 2, wherein said mixed stream;

is pressurized to between about 80-150 psig.

4. The method according to claim 2, wherein said gas is ozone, and said mixed stream;

is pressurized to about 150 psig.

5. The method according to claim any one of claims 3, further comprising the steps of:

reducing the pressure downstream of the pressure retention vessel; and

directing said treated stream;

from said pressure retention vessel under reduced pressure downstream of the pressure retention vessel to a dissolved air flotation system for further treatment thereof.

6. The method according to claim 2, wherein said gas is ozone and said mixed/dissolved stream;

is pressurized to about 150 psig, said method further comprising the steps of;

reducing the pressure downstream of the pressure retention vessel;

directing said treated stream;

from the pressure retention vessel to a degassing vessel;

directing a first output stream;

of residual ozone gas from said degassing vessel to an ozone destruct chamber; and

retrieving a disinfected, clean effluent stream;

of the remaining treated/disinfected liquid from said degassing vessel as a second output thereof.

7. The method according to claims 2, wherein said gas is ozone and said mixed/dissolved stream;

Is pressurized to about 150 psig, said method further comprising the steps of;

reducing the pressure downstream of the pressure retention vessel;

directing said treated intimately mixed/dissolved stream;

under reduced pressure from the pressure retention vessel to a dissolved air flotation system for further treatment thereof;

directing a purified stream;

from said dissolved air flotation system to a degassing vessel;

directing a first output stream;

of residual ozone gas from said degassing vessel to an ozone destruct chamber; and

retrieving a disinfected, clean effluent stream;

of the remaining treated/disinfected liquid from said degassing vessel as a second output thereof.

8. The method according to claim 2, further comprising the step of recycling any residual gas that collects in said pressure retention vessel through a vapour-return line to the gas feed line.

9. A method for dissolving a gas into a liquid stream;

comprising the steps of;

injecting a gas at atmospheric pressure via a gas feed line into a liquid stream;

to create a mixed stream;

pressurizing said mixed stream;

to about 80-150 psig;

directing said mixed stream;

into a hydrocyclone to create a more intimately mixed/dissolved stream;

directing said intimately mixed/dissolved stream;

from the hydrocyclone to a pressure retention vessel, and holding said intimately mixed/dissolved stream;

in said pressure retention vessel at a predetermined pressure for a predetermined time period for effectively treating, disinfecting and/or clarifying said intimately mixed/dissolved stream, thereby creating a treated stream;

reducing the pressure downstream of the pressure retention vessel; and

directing said treated stream;

from said pressure retention vessel under reduced pressure from the pressure retention vessel to a dissolved air flotation system for further treatment thereof; and

recycling any residual gas that collects in said pressure retention vessel through a vapour-return line to the liquid feed line thereby creating a treated stream,

wherein said hydrocyclone comprises;

a housing vessel equipped with said at least one hydrocyclone inlet and said hydrocyclone outlet;

a hydrocyclone liner contained in said housing vessel, said liner having an upper neck portion and a lower outlet portion, said lower outlet portion being in communication with said outlet of said housing vessel, and said liner having a internal diameter that reduces from said upper neck portion towards said lower outlet portion; and

a spin inducer attached to the upper neck portion of said hydrocyclone liner and in communication with the at least one inlet of said hydrocyclone for inducing circular flow to the mixed stream as it enters said hydrocyclone.